METHYL 2-CHLOROISONICOTINATE
- Product Name
- METHYL 2-CHLOROISONICOTINATE
- CAS No.
- 58481-11-1
- Chemical Name
- METHYL 2-CHLOROISONICOTINATE
- Synonyms
- BUTTPARK 91\04-05;METHYL 2-CHLOROISONICOTINATE;Methyl 2-chloroisonicotin...;. methyl-2-chloroisonicotiate;Methyl2-Chloroisonicotinate>3-chloro-4-iodo-2-methylbenzoate;Methyl 2-chloroisonicotinate ,98%;Methyl 2-chloropyidine-4-carboxylate;METHYL 2-CHLORO-4-PYRIDINECARBOXYLATE;METHYL 2-CHLOROPYRIDINE-4-CARBOXYLATE
- CBNumber
- CB9777334
- Molecular Formula
- C7H6ClNO2
- Formula Weight
- 171.58
- MOL File
- 58481-11-1.mol
METHYL 2-CHLOROISONICOTINATE Property
- Melting point:
- 32-36 °C
- Boiling point:
- 70°C/0.1mmHg(lit.)
- Density
- 1.294±0.06 g/cm3(Predicted)
- Flash point:
- >230 °F
- storage temp.
- Inert atmosphere,2-8°C
- pka
- -1.15±0.10(Predicted)
- form
- powder to lump to clear liquid
- color
- White or Colorless to Yellow
- CAS DataBase Reference
- 58481-11-1(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H315Causes skin irritation
H318Causes serious eye damage
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 660604
- Product name
- Methyl 2-chloropyridine-4-carboxylate
- Purity
- 97%
- Packaging
- 5g
- Price
- $60.6
- Updated
- 2023/06/20
- Product number
- M2164
- Product name
- Methyl 2-Chloroisonicotinate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $18
- Updated
- 2025/07/31
- Product number
- M2164
- Product name
- Methyl 2-Chloroisonicotinate
- Purity
- >98.0%(GC)
- Packaging
- 25g
- Price
- $69
- Updated
- 2025/07/31
- Product number
- M295658
- Product name
- Methyl 2-Chloroisonicotinate
- Packaging
- 5g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- M295658
- Product name
- Methyl 2-Chloroisonicotinate
- Packaging
- 2.5g
- Price
- $65
- Updated
- 2021/12/16
METHYL 2-CHLOROISONICOTINATE Chemical Properties,Usage,Production
Chemical Properties
White to light brown solid
Synthesis
67-56-1
6313-54-8
58481-11-1
2-Chloroisonicotinic acid (5.10 g, 32.38 mmol) was dissolved in methanol (150 mL) and thionyl chloride (12 mL) was added slowly. The reaction mixture was stirred at 70 °C for 5 h. After completion of the reaction, the reaction solution was concentrated under reduced pressure by rotary evaporator. The concentrated residue was dissolved in dichloromethane (250 mL), washed sequentially with 10% aqueous potassium carbonate (2×150 mL), dried over anhydrous magnesium sulfate, filtered, and the filtrate was concentrated by rotary evaporation to afford methyl 2-chloropyridine-4-carboxylate (SLA 07150) as a yellow solid (5.06 g, 91% yield).The molecular weight of SRA 07150 was 171.58; melting point was 33.0 °C; thin layer chromatography (TLC) Rf value was 0.80 (unfolding reagent ratio methanol:dichloromethane=10:90).1H-NMR (CDCl3, δ): 3.98 (s, 3H, CH3), 7.78 (dd, 1H, J=5.1 Hz, J=1.3 Hz, ArH), 7.89 (d, 1H, J= 0.6 Hz, ArH), 8.55 (dd, 1H, J=5.1 Hz, J=0.6 Hz, ArH).
References
[1] Patent: WO2008/11478, 2008, A2. Location in patent: Page/Page column 76
[2] Patent: WO2016/154241, 2016, A1. Location in patent: Paragraph 578; 579
[3] Patent: US2008/167321, 2008, A1. Location in patent: Page/Page column 14
[4] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988, p. 2785 - 2790
[5] Patent: EP1754706, 2007, A1. Location in patent: Page/Page column 76
METHYL 2-CHLOROISONICOTINATE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from METHYL 2-CHLOROISONICOTINATE manufacturers
- Product
- Methyl 2-chloroisonicotinate 58481-11-1
- Price
- US $0.00-0.00/Kg/Drum
- Min. Order
- 1KG
- Purity
- 98%min
- Supply Ability
- 500KGS
- Release date
- 2021-07-14
- Product
- METHYL 2-CHLOROISONICOTINATE 58481-11-1
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 Tons
- Release date
- 2021-10-15
- Product
- METHYL 2-CHLOROISONICOTINATE 58481-11-1
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-10-22