2-Bromo-3-fluoronitrobenzene
- Product Name
- 2-Bromo-3-fluoronitrobenzene
- CAS No.
- 59255-94-6
- Chemical Name
- 2-Bromo-3-fluoronitrobenzene
- Synonyms
- 2-Bromo-1-fluoro-3-nitrobenzene;2-broMo-3-fluorobroMobezene;2-BROMO-3-FLUORONITROBENZENE;1-Bromo-2-fluoro-6-nitrobenzene;Benzene, 2-bromo-1-fluoro-3-nitro-;2-Bromo-3-fluoronitrobenzene ISO 9001:2015 REACH
- CBNumber
- CB9783955
- Molecular Formula
- C6H3BrFNO2
- Formula Weight
- 220
- MOL File
- 59255-94-6.mol
2-Bromo-3-fluoronitrobenzene Property
- Melting point:
- 42.0-44.0 °C(Solv: ethyl acetate (141-78-6); hexane (110-54-3))
- Boiling point:
- 222.3±20.0 °C(Predicted)
- Density
- 1.808±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- color
- yellow
- CAS DataBase Reference
- 59255-94-6(CAS DataBase Reference)
Safety
- Hazard Codes
- T
- HazardClass
- IRRITANT
- HS Code
- 2904990090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B688653
- Product name
- 2-Bromo-1-fluoro-3-nitrobenzene
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- B688653
- Product name
- 2-Bromo-1-fluoro-3-nitrobenzene
- Packaging
- 500mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- B688653
- Product name
- 2-Bromo-1-fluoro-3-nitrobenzene
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
- Product number
- PC5083
- Product name
- 2-Bromo-3-fluoronitrobenzene
- Packaging
- 5g
- Price
- $76
- Updated
- 2021/12/16
- Product number
- 4654-B-X4
- Product name
- 2-Bromo-3-fluoronitrobenzene
- Packaging
- 5G
- Price
- $90
- Updated
- 2021/12/16
2-Bromo-3-fluoronitrobenzene Chemical Properties,Usage,Production
Synthesis
Preparation method of 2-bromo-3-fluoronitrobenzene: Add 21.6g (0.1mol) 2-bromo-3-nitroaniline, 12.5ml (0.15mol) concentrated hydrochloric acid, and 12.5ml water into a reaction bottle, and reduce the temperature to 15°C; dissolve 8.3g (0.12mol) sodium nitrite in 14.5ml water and slowly add dropwise to the above system, then add 11.4g (0.13mol) fluoroboric acid, keep warm at 15°C and stir for 2 hours, track the reaction by HPLC until the reaction of 2-bromo-3-nitroaniline is complete; filter, rinse the filter cake with methanol, and dry to obtain 25.8g of intermediate IV. Add 30 ml of toluene to the reaction flask, heat to 100 ° C, slowly add 10 g (31.7 mmol) of intermediate IV, keep warm and stir for 1 hour, track the reaction by HPLC until the intermediate IV reacts completely: concentrate, recrystallize from ethyl acetate and n-hexane to obtain 5.7 g of 2-Bromo-3-fluoronitrobenzene, with a molar yield of 83%.
2-Bromo-3-fluoronitrobenzene Preparation Products And Raw materials
Raw materials
Preparation Products
2-Bromo-3-fluoronitrobenzene Suppliers
- Tel
- 010-82848833 400-666-7788
- Fax
- 86-10-82849933
- jkinfo@jkchemical.com
- Country
- China
- ProdList
- 96815
- Advantage
- 76
- Tel
- 821-50328103-801 18930552037
- Fax
- 86-21-50328109
- 3bsc@sina.com
- Country
- China
- ProdList
- 15839
- Advantage
- 69
- Tel
- 021-021-58432009 400-005-6266
- Fax
- 021-58436166
- sales8178@energy-chemical.com
- Country
- China
- ProdList
- 44688
- Advantage
- 61
- Tel
- 86-027-67849912
- Fax
- 86-027-87531808
- sales@chemwish.com
- Country
- China
- ProdList
- 35896
- Advantage
- 56
- Tel
- +86 (0) 571 85 58 67 18
- Fax
- 0086-571-85864795
- sales@capotchem.com
- Country
- China
- ProdList
- 18207
- Advantage
- 66
- Tel
- 010-82967028 13552068683
- Fax
- +86-10-82967029
- 2355560935@qq.com
- Country
- China
- ProdList
- 12390
- Advantage
- 60
- Tel
- 13817811078
- Fax
- 86-021-50426522,50426273
- sales@jingyan-chemical.com
- Country
- China
- ProdList
- 9976
- Advantage
- 60
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14103
- Advantage
- 59
- Tel
- 021-50795510 4000665055
- Fax
- 021-50795055
- sales@accelachem.com
- Country
- China
- ProdList
- 11655
- Advantage
- 64
- Tel
- 21-31038972 15721252604
- Fax
- +86-21-51385350
- ammyzuo@harvest-chem.com
- Country
- China
- ProdList
- 2540
- Advantage
- 64
View Lastest Price from 2-Bromo-3-fluoronitrobenzene manufacturers
- Product
- 2-Bromo-3-fluoronitrobenzene 59255-94-6
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2023-04-26
- Product
- 2-Bromo-3-fluoronitrobenzene 59255-94-6
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2023-04-27
- Product
- 2-Bromo-3-fluoronitrobenzene 59255-94-6
- Price
- US $35.00-25.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 20 Ton
- Release date
- 2023-11-13