ChemicalBook > CAS DataBase List > 2-Bromo-3-fluoronitrobenzene

2-Bromo-3-fluoronitrobenzene

Product Name
2-Bromo-3-fluoronitrobenzene
CAS No.
59255-94-6
Chemical Name
2-Bromo-3-fluoronitrobenzene
Synonyms
2-Bromo-1-fluoro-3-nitrobenzene;2-broMo-3-fluorobroMobezene;2-BROMO-3-FLUORONITROBENZENE;1-Bromo-2-fluoro-6-nitrobenzene;Benzene, 2-bromo-1-fluoro-3-nitro-;2-Bromo-3-fluoronitrobenzene ISO 9001:2015 REACH
CBNumber
CB9783955
Molecular Formula
C6H3BrFNO2
Formula Weight
220
MOL File
59255-94-6.mol
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2-Bromo-3-fluoronitrobenzene Property

Melting point:
42.0-44.0 °C(Solv: ethyl acetate (141-78-6); hexane (110-54-3))
Boiling point:
222.3±20.0 °C(Predicted)
Density 
1.808±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
color 
yellow
CAS DataBase Reference
59255-94-6(CAS DataBase Reference)
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Safety

Hazard Codes 
T
HazardClass 
IRRITANT
HS Code 
2904990090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
B688653
Product name
2-Bromo-1-fluoro-3-nitrobenzene
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
B688653
Product name
2-Bromo-1-fluoro-3-nitrobenzene
Packaging
500mg
Price
$65
Updated
2021/12/16
TRC
Product number
B688653
Product name
2-Bromo-1-fluoro-3-nitrobenzene
Packaging
1g
Price
$75
Updated
2021/12/16
Apolloscientific
Product number
PC5083
Product name
2-Bromo-3-fluoronitrobenzene
Packaging
5g
Price
$76
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-B-X4
Product name
2-Bromo-3-fluoronitrobenzene
Packaging
5G
Price
$90
Updated
2021/12/16
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2-Bromo-3-fluoronitrobenzene Chemical Properties,Usage,Production

Synthesis

Preparation method of 2-bromo-3-fluoronitrobenzene: Add 21.6g (0.1mol) 2-bromo-3-nitroaniline, 12.5ml (0.15mol) concentrated hydrochloric acid, and 12.5ml water into a reaction bottle, and reduce the temperature to 15°C; dissolve 8.3g (0.12mol) sodium nitrite in 14.5ml water and slowly add dropwise to the above system, then add 11.4g (0.13mol) fluoroboric acid, keep warm at 15°C and stir for 2 hours, track the reaction by HPLC until the reaction of 2-bromo-3-nitroaniline is complete; filter, rinse the filter cake with methanol, and dry to obtain 25.8g of intermediate IV. Add 30 ml of toluene to the reaction flask, heat to 100 ° C, slowly add 10 g (31.7 mmol) of intermediate IV, keep warm and stir for 1 hour, track the reaction by HPLC until the intermediate IV reacts completely: concentrate, recrystallize from ethyl acetate and n-hexane to obtain 5.7 g of 2-Bromo-3-fluoronitrobenzene, with a molar yield of 83%.

2-Bromo-3-fluoronitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Bromo-3-fluoronitrobenzene Suppliers

J & K SCIENTIFIC LTD.
Tel
010-82848833 400-666-7788
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
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China
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96815
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3B Pharmachem (Wuhan) International Co.,Ltd.
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821-50328103-801 18930552037
Fax
86-21-50328109
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3bsc@sina.com
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China
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Energy Chemical
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021-021-58432009 400-005-6266
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021-58436166
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sales8178@energy-chemical.com
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China
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Wuhan Chemwish Technology Co., Ltd
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86-027-67849912
Fax
86-027-87531808
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sales@chemwish.com
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China
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Capot Chemical Co., Ltd
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+86 (0) 571 85 58 67 18
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0086-571-85864795
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sales@capotchem.com
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Beijing Ouhe Technology Co., Ltd
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010-82967028 13552068683
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+86-10-82967029
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2355560935@qq.com
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China
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JinYan Chemicals(ShangHai) Co.,Ltd.
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13817811078
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86-021-50426522,50426273
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sales@jingyan-chemical.com
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China
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Adamas Reagent, Ltd.
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400-6009262 16621234537
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021-64823266
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chenyj@titansci.com
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China
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Accela ChemBio Co.,Ltd.
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021-50795510 4000665055
Fax
021-50795055
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sales@accelachem.com
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China
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11655
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Shanghai Harvest Chemical Industrial Co., Ltd.
Tel
21-31038972 15721252604
Fax
+86-21-51385350
Email
ammyzuo@harvest-chem.com
Country
China
ProdList
2540
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View Lastest Price from 2-Bromo-3-fluoronitrobenzene manufacturers

Hebei Weibang Biotechnology Co., Ltd
Product
2-Bromo-3-fluoronitrobenzene 59255-94-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2023-04-26
Hebei Weibang Biotechnology Co., Ltd
Product
2-Bromo-3-fluoronitrobenzene 59255-94-6
Price
US $10.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2023-04-27
Hebei Xinsheng New Material Technology Co., LTD.
Product
2-Bromo-3-fluoronitrobenzene 59255-94-6
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-11-13