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LIDOFLAZINE, 98.5%

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LIDOFLAZINE, 98.5% Basic information

Product Name:
LIDOFLAZINE, 98.5%
Synonyms:
  • 6’-xylidide,4-(4,4-bis(p-fluorophenyl)butyl)-1-piperazineaceto-2
  • clinium
  • corflazine
  • klinium
  • lidoflazin
  • lidoflazina
  • lidoflazinum
  • mcn-jr7904
CAS:
3416-26-0
MF:
C30H35F2N3O
MW:
491.62
EINECS:
222-312-8
Mol File:
3416-26-0.mol
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LIDOFLAZINE, 98.5% Chemical Properties

Melting point:
159-161°
Boiling point:
632.6±55.0 °C(Predicted)
Density 
1.1322 (estimate)
storage temp. 
2-8°C
solubility 
DMSO: ≥10mg/mL
pka
14.62±0.70(Predicted)
form 
powder
color 
white
CAS DataBase Reference
3416-26-0
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Safety Information

Hazard Codes 
Xn
Risk Statements 
22
Safety Statements 
36
WGK Germany 
3
RTECS 
TK7910000
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LIDOFLAZINE, 98.5% Usage And Synthesis

Chemical Properties

WHITE TO ALMOST WHITE POWDER

Originator

Clinium,Janssen,W. Germany,1969

Uses

Coronary vasodilatator;Ca++ channel activator

Uses

Lidoflazine is a L-type Ca2+ channel antagonist.Also, it is derived from 1,1''-(4-Chlorobutylidene)bis(4-fluorobenzene) (C364775), which is a derivative of Zerumbone with potential anti-tumor effects towards HeLa cancer cells.

Definition

ChEBI: 2-[4-[4,4-bis(4-fluorophenyl)butyl]-1-piperazinyl]-N-(2,6-dimethylphenyl)acetamide is a diarylmethane.

Manufacturing Process

A mixture of 6.6 parts 1-[4,4-di-(4-fluoro-phenyl)butyl]-piperazine, 4.33 parts N-(2-chloro-acetyl)-2,6-dimethyl-aniline, 3.2 parts sodium carbonate, a few crystals of potassium iodide in 200 parts 4-methyl-2-pentanone is stirred and refluxed for 70 hours. After cooling there are added 70 parts water. The organic layer is separated, dried over potassium carbonate, filtered and evaporated. The oily residue is dissolved in 80 parts diisopropylether and the solution is filtered hot. After cooling the filtrate at 0°C. the formed solid is filtered off and recystallired from 80 parts ether, yielding 1-[4,4-di-(4-fluorophenyl)butyl]-4-[(2,6-dimethylanilino-carbonyl)-methyl]-piperazine; MP 159°C to 161°C.

brand name

Angex (Janssen); Clinium (Ortho-McNeil).

Therapeutic Function

Coronary vasodilator

LIDOFLAZINE, 98.5%Supplier

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