PROPYL LAURATE
PROPYL LAURATE Basic information
- Product Name:
- PROPYL LAURATE
- Synonyms:
-
- PROPYL LAURATE
- Dodecanoic acid, propyl ester
- dodecanoicacidpropylester
- lauricacidpropylester
- Propyl dodecanoate
- Lauric acid propyl ester, Propyl laurate
- CAS:
- 3681-78-5
- MF:
- C15H30O2
- MW:
- 242.4
- EINECS:
- 222-961-7
- Mol File:
- 3681-78-5.mol
PROPYL LAURATE Chemical Properties
- Melting point:
- 4.2°C (estimate)
- Boiling point:
- 285.23°C (estimate)
- Density
- 0.86 g/mL at 25 °C(lit.)
- refractive index
- 1.4335
- storage temp.
- Sealed in dry,Room Temperature
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- Oil
- color
- Colourless
- LogP
- 6.110
- CAS DataBase Reference
- 3681-78-5
PROPYL LAURATE Usage And Synthesis
Uses
Propyl dodecanoate is an ester product.
Synthesis
71-23-8
2146-71-6
3681-78-5
The general procedure for the synthesis of propyl dodecanoate from n-propanol and vinyl laurate is as follows: enzymatic synthesis in a 50 mL high pressure reactor. The reactor was equipped with a pressure reading controller and a JASCO-PU-2080-CO2 plus regulator. First, a predetermined amount of vinyl laurate was added to the reactor, followed by a predetermined amount of n-propanol. Next, a fixed amount of PVA/CHI lipase was added to initiate the reaction, followed by sealing the reactor and assembling it into an SC-CO2 high pressure reaction system. Liquid SC-CO2 was pumped into the reactor at a flow rate of 3.5 mL/min. The reaction was carried out for a predetermined time at a specific pressure (MPa) and temperature (°C) set by the RSM software. Upon completion of the reaction, the SC-CO2 pressure was slowly released through a 50°C thermostatic limiter to allow the residual material inside the reactor to flow out with the CO2. The reaction products were subsequently analyzed by Perkin-Elmer Clarus-400 gas chromatography (GC) equipped with a flame ionization detector (FID) and a capillary column.The oven temperature program for the GC was to maintain an initial temperature of 90 °C for 4 min, and then increase the temperature at a rate of 10 °C/min to 240 °C. The GC was then operated at a constant temperature of 50 °C, and the temperature was increased by a Shimadzu QC. In addition, the products were further confirmed by gas chromatography-mass spectrometry (GC-MS) on a Shimadzu QP-2010 instrument.
References
[1] Process Biochemistry, 2015, vol. 50, # 8, p. 1224 - 1236
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PROPYL LAURATE(3681-78-5)Related Product Information
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- ZINC LAURATE
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- METHYL LAURATE
- Ethyl laurate
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