Diisopropyl succinate
Diisopropyl succinate Basic information
- Product Name:
- Diisopropyl succinate
- Synonyms:
-
- BUTANEDIOIC ACID, BIS(1-METHYL-ETHYL) ESTER
- DIPS
- DIISOPROPYL SUCCINATE
- SUCCINIC ACID DIISOPROPYL ESTER
- Bis(1-methylethyl)butanedioate
- dipropan-2-yl butanedioate
- Diisopropyl Succinate, 99.0%(GC)
- Butanedioic acid, 1,4-bis(1-methylethyl) ester
- CAS:
- 924-88-9
- MF:
- C10H18O4
- MW:
- 202.25
- EINECS:
- 213-110-0
- Mol File:
- 924-88-9.mol
Diisopropyl succinate Chemical Properties
- Melting point:
- 263.0 °C
- Boiling point:
- 228 °C
- Density
- 0,99 g/cm3
- vapor pressure
- 12.2Pa at 25℃
- refractive index
- 1.4170 to 1.4190
- storage temp.
- Sealed in dry,Room Temperature
- form
- solid
- color
- Colorless to Almost colorless
- LogP
- 2.2
- CAS DataBase Reference
- 924-88-9(CAS DataBase Reference)
- NIST Chemistry Reference
- Succinic acid diisopropyl ester(924-88-9)
- EPA Substance Registry System
- Butanedioic acid, bis(1-methylethyl) ester (924-88-9)
Safety Information
- Risk Statements
- 36/37/38-52/53
- Safety Statements
- 26-36/37/39
- HS Code
- 2917.19.1700
Diisopropyl succinate Usage And Synthesis
Uses
Diisopropyl Succinate is used in preparation of Heterocyclic Pyrrolopyrrole Diketone quaternary Ammonium Salt as Copper electroplating leveling agent.
Synthesis
110-15-6
67-63-0
924-88-9
In a typical reaction, butanedioic acid (1 mol), isopropanol (1.5-2 mol) and AMA 2:3 (332 g, 0.6 mol) were mixed in a reaction glass tube equipped with a screw cap and a magnetic stirrer until a homogeneous wet mixture was formed. The reaction mixture was placed in a microwave reactor (Anton Parr Monowave 300) and irradiated at 80 °C for 8 min or at 120 °C for 20 min. Upon completion of the reaction, the mixture was cooled, diluted with dichloromethane (41 mL), filtered by gravity and the filtrate was washed with dichloromethane. Subsequently, the filtrate was washed sequentially with saturated sodium carbonate solution (Na2CO3) and water. The organic layer was separated, dried with anhydrous sodium sulfate (Na2SO4), filtered and concentrated under reduced pressure to give diisopropyl succinate.
References
[1] Synthetic Communications, 2014, vol. 44, # 16, p. 2386 - 2392
[2] Phosphorus, Sulfur and Silicon and the Related Elements, 2004, vol. 179, # 6, p. 1187 - 1191
[3] Journal of Organic Chemistry, 1983, vol. 48, # 18, p. 3106 - 3108
[4] Journal of the Chemical Society, 1948, p. 631
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Diisopropyl succinate(924-88-9)Related Product Information
- 6alpha-Methylprednisolone sodium succinate
- Succinic anhydride
- Diisopropyl phosphite
- Diisopropyl ether
- Isopropyl palmitate
- 2,3-Dimethylbutane
- Diisopropyl adipate
- Triisopropyl borate
- Isopropyl myristate
- Diisobutyl succinate
- Tris(trimethylsilyl)phosphate
- Diethyl phthalate
- Titanium tetraisopropanolate
- Diisopropyl malonate
- Succinic acid
- Methyl acrylate
- Diisopropyl azodicarboxylate
- Disodium succinate