(-)-Isopinocampheol Chemical Properties

Melting point:

52-55 °C

alpha 

-34 º (c=20, EtOH)

Boiling point:

219 °C(lit.)

Density 

0.8389 (rough estimate)

refractive index 

1.4710 (estimate)

Flash point:

200 °F

pka

15.35±0.60(Predicted)

optical activity

[α]22/D 34°, c = 20 in ethanol

BRN 

2038100

LogP

2.720 (est)

Safety Information

Safety Statements 

22-24/25

WGK Germany 

3

MSDS

• Language:English Provider:SigmaAldrich

(-)-Isopinocampheol Usage And Synthesis

Purification Methods

Dissolve it in Et2O, dry over MgSO4, filter, evaporate, then recrystallise it from pet ether. Also recrystallise it from aqueous EtOH and distil it in a vacuum. [Kergomard & Geneix Bull Soc Chim Fr 394 1958, Zweifel & Brown J Am Chem Soc 86 393 1964.] The 3,4-dinitrobenzoyl derivative has m 100-101o, the phenylcarbamoyl derivative has m 137-138o and the acid -phthalate has m 125-126o. [Beilstein 6 III 282, 283.]

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