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Potassium peroxymonosulfate

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Potassium peroxymonosulfate Basic information

Product Name:
Potassium peroxymonosulfate
Synonyms:
  • Potassium peroxymonosulfate,Active Oxygen≥4.5%
  • Potassium hydrogen monopersulfate
  • Potassium peroxymonosulfate joyce
  • OXONE, MONOPERSULFATE COMPOUNDOXONE, MONOPERSULFATE COMPOUNDOXONE, MONOPERSULFATE COMPOUND
  • Potassiumhydrogenperoxymonosulfate
  • PotassiuM 3-sulfotrioxidan-1-ide
  • PotassiuM Monopersulfate coMpound
  • Oxone , potassium monopersulfate
CAS:
70693-62-8
MF:
H3K5O18S4
MW:
614.74
EINECS:
274-778-7
Product Categories:
  • Inorganics
  • 70693-62-8
Mol File:
70693-62-8.mol
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Potassium peroxymonosulfate Chemical Properties

Density 
1.15
storage temp. 
Store at <= 20°C.
solubility 
250-300g/l soluble
form 
solid
Specific Gravity
1.12-1.20
color 
white
PH
2-3 (10g/l, H2O, 20℃)
Water Solubility 
Soluble in water (100 mg/ml).
Sensitive 
Hygroscopic
Exposure limits
ACGIH: TWA 0.1 mg/m3
Stability:
Stable. Oxidizer. Incompatible with combustible materials, bases.
InChIKey
HVAHYVDBVDILBL-UHFFFAOYSA-M
LogP
-3.9 at 25℃
CAS DataBase Reference
70693-62-8(CAS DataBase Reference)
EPA Substance Registry System
Potassium peroxymonosulfate sulfate (K5[HSO3(O2)][SO3(O2)](HSO4)2) (70693-62-8)
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Safety Information

Hazard Codes 
O,C
Risk Statements 
8-22-34-42/43-37-35
Safety Statements 
22-26-36/37/39-45
RIDADR 
UN 3260 8/PG 2
WGK Germany 
1
TSCA 
Yes
HS Code 
2833 40 00
HazardClass 
5.1
PackingGroup 
III
Toxicity
LD50 orally in Rabbit: > 2000 mg/kg
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Potassium peroxymonosulfate Usage And Synthesis

Reactions

  1. Reagent for the catalytic asymmetric Shi epoxidation
  2. Reagent for the synthesis of nitro heteroaromatics in water
  3. Reagent for the syntheses of benzoxazoles and benzothiazoles using aryl iodides via C-H functionalization and C-O/S bond formation
  4. Reagent used for bromolactonization in the asymmetric total synthesis of (+)-Dubiusamine C
  5. Reagent for the benzofuran oxidative dearomatization cascade in the total synthesis of Integrastatin B

Chemical Properties

white crystalline powder

Uses

PCB metal surface treatment chemical and water treatment etc.

Uses

Oxone is used for halogenation of a,b-unsaturated carbonyl compounds and catalytic generation of hypervalent iodine reagents for alcohol oxidation. It is a used for rapid, and good synthesis of oxaziridines.

General Description

OXONE?, monopersulfate compound is a potassium triple salt mainly used as a stable, easy to handle and nontoxic oxidant.

Flammability and Explosibility

Non flammable

Purification Methods

This is a stable form of Caro's acid and should contain >4.7% of active oxygen. It can be used in EtOH/H2O and EtOH/AcOH/H2O solutions. If active oxygen is too low. it is best to prepare it afresh from 1mole of KHSO5, 0.5mole of KHSO4 and 0.5mole of K2SO4. [Kennedy & Stock J Org Chem 25 1901 1960, Stephenson US Patent 2,802,722 1957.] A rapid preparation of Caro's acid is made by stirring finely powdered potassium persulfate (M 270.3) into ice-cold conc H2SO4 (7mL) and when homogeneous add ice (40-50g). It is stable for several days if kept cold. Keep away from organic matter as it is a STRONG OXIDANT. A detailed preparation of Caro's acid (hypersulfuric acid, H2SO5) in crystalline form m ~45o from H2O2 and chlorosulfonic acid was described by Fehér in Handbook of Preparative Inorganic Chemistry (Ed. Brauer) Academic Press Vol I p 388 1963.

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