N-BENZOYLIMIDAZOLE Chemical Properties

Melting point:

19-20 °C(Solv: ligroine (8032-32-4))

Boiling point:

120 °C

Density 

1.15±0.1 g/cm3(Predicted)

Flash point:

120-121°C/0.8mm

storage temp. 

Inert atmosphere,2-8°C

solubility 

Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)

form 

Oil

pka

3.65±0.10(Predicted)

color 

Pale Yellow to Yellow

Sensitive 

Moisture Sensitive

BRN 

125881

CAS DataBase Reference

10364-94-0(CAS DataBase Reference)

Safety Information

Hazard Codes 

Xi

Risk Statements 

36/38

Safety Statements 

26-36/37/39

HazardClass 

IRRITANT, MOISTURE SENSITIVE, KEEP COLD

MSDS

• Language:English Provider:ALFA

N-BENZOYLIMIDAZOLE Usage And Synthesis

Chemical Properties

Slightly Coloured Oil

Synthesis Reference(s)

The Journal of Organic Chemistry, 54, p. 5620, 1989 DOI: 10.1021/jo00284a043
Tetrahedron, 36, p. 2409, 1980 DOI: 10.1016/0040-4020(80)80219-5

Synthesis

A suspension of imidazole (4.54 g, 0.0668 mol) in anhydrous benzene (200 mL) in a flask fitted with a drying apparatus was treated at 8??C with a solution of benzoyl chloride (4.69 ) in benzene (20 mL). g, 0.0333 mol) in benzene (20 mL). The mixture was allowed to warm to room temperature and stirred for 16 hours. The precipitated imidazole hydrochloride was removed by filtration through a funnel and the clarified filtrate was concentrated under reduced pressure to give N-benzoyl imidazolylide as a viscous, hygroscopic oil in a yield of 5.78 g. It was stored at 0??C in a tightly closed container.

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