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NITROCYCLOPENTANE

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NITROCYCLOPENTANE Basic information

Product Name:
NITROCYCLOPENTANE
Synonyms:
  • NITROCYCLOPENTANE
  • NITROCYCLOPENTANE, 97+%
  • 1-Nitrocyclopentane
  • nitro-cyclopentan
  • (1S,2S)-Methyl 2-aMinocyclopropanecarboxylate
  • Nitrocyclopentane (NCyP)
  • Cyclopentane, nitro-
  • NITROCYCLOPENTANE ISO 9001:2015 REACH
CAS:
2562-38-1
MF:
C5H9NO2
MW:
115.13
EINECS:
219-884-6
Product Categories:
  • Nitro Compounds
  • Nitrogen Compounds
  • Organic Building Blocks
  • Building Blocks
  • Chemical Synthesis
  • Nitro Compounds
  • Nitrogen Compounds
  • Organic Building Blocks
Mol File:
2562-38-1.mol
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NITROCYCLOPENTANE Chemical Properties

Melting point:
143-144 °C
Boiling point:
180 °C (lit.)
Density 
1.086 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.454(lit.)
Flash point:
153 °F
pka
8.46±0.20(Predicted)
BRN 
907079
CAS DataBase Reference
2562-38-1
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36/37/39
RIDADR 
2810
WGK Germany 
3
RTECS 
GY4657500
HazardClass 
6.1
PackingGroup 
III
HS Code 
29042000

MSDS

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NITROCYCLOPENTANE Usage And Synthesis

Chemical Properties

Clear pale yellow liquid

Preparation

Bromocyclopentane (22.0 g, 0.15 mol) was added to a soln of NaNO2 (18 g, 0.26 mol) in dry DMSO (100 mL) at 15 ℃ and the mixture was stirred at this temperature for 3 h. The mixture was poured into ice water (250 mL) and extracted with petroleum ether (bp 35-37 ℃; 4 × 50 mL). The combined organic extracts were washed with H2O (4× 50 mL), dried (MgSO4), and concentrated under reduced pressure. The residue was distilled to give Nitrocyclopentane; yield: 9.9 g (58%); bp 62 ℃/8 Torr; nD/20 1.4538.

Synthesis of Nitrocyclopentane

Synthesis Reference(s)

Tetrahedron Letters, 21, p. 1117, 1980 DOI: 10.1016/S0040-4039(01)83928-9

NITROCYCLOPENTANESupplier

Meryer (Shanghai) Chemical Technology Co., Ltd.
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