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9-Bromoanthracene

Basic information Description References Safety Related Supplier
9-Bromoanthracene Basic information
9-Bromoanthracene Chemical Properties
  • Melting point:97-100 °C(lit.)
  • Boiling point:303.85°C (rough estimate)
  • Density 1.4251 (rough estimate)
  • refractive index 1.6404 (estimate)
  • storage temp.  0-6°C
  • form Powder
  • color Yellow
  • Water Solubility Insoluble in water.
  • BRN 1869747
  • InChIKeyZIRVQSRSPDUEOJ-UHFFFAOYSA-N
  • CAS DataBase Reference1564-64-3(CAS DataBase Reference)
  • NIST Chemistry Reference9-Bromoanthracene(1564-64-3)
Safety Information
  • Hazard Codes Xi
  • Safety Statements 22-24/25
  • WGK Germany 3
  • Hazard Note Irritant
  • HS Code 29049090
MSDS
9-Bromoanthracene Usage And Synthesis
  • Description9-bromoanthracene is a kind of bromine-derived anthracene. It is known to be able to reversibly photodimerize in a head-to tail fashion upon irradiation by long-wavelength ultraviolet light. The photodimers of 9-bromoanthracene are suitable to be used as alkyl halide initiators in the atom transfer radical polymerization (ATRP) reactions. It is also used as the intermediate for the preparation of the 9-substitued form of the polycyclic aromatic hydrocarbon (PAH) anthracene.
  • ReferencesCohen, Nicole A., et al. Macromolecular Chemistry and Physics 210.3 ‐4 (2009): 263-268.
    Xu, Xiaoming, Wenzhe Lu, and Richard B. Cole. Analytical chemistry 68.23 (1996): 4244-4253.
    Dang, Hung, and Miguel A. Garcia-Garibay. Journal of the American Chemical Society 123.2 (2001): 355-356.
  • Chemical Propertieswhite to light yellow crystal powder
  • Purification MethodsCrystallise 9-bromoanthracene from MeOH or EtOH followed by sublimation in vacuo. [Masnori et al. J Am Chem Soc 108 126 1986, Beilstein 5 IV 2295.]
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