Basic information Safety Supplier Related

ETHYL (DIPHENYLMETHYLSILYL)ACETATE

Basic information Safety Supplier Related

ETHYL (DIPHENYLMETHYLSILYL)ACETATE Basic information

Product Name:
ETHYL (DIPHENYLMETHYLSILYL)ACETATE
Synonyms:
  • ETHYL (DIPHENYLMETHYLSILYL)ACETATE
  • ethyl (methyldiphenylsilyl)acetate
  • 2-(Methyldiphenylsilyl)acetic acid ethyl ester
CAS:
13950-57-7
MF:
C17H20O2Si
MW:
284.425
Mol File:
13950-57-7.mol
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ETHYL (DIPHENYLMETHYLSILYL)ACETATE Usage And Synthesis

Physical properties

clear to light yellow liquids.

Uses

vinyl 1,1-dication synthetic equivalent in reactions with Grignard reagents; reagent for Peterson synthesis of α,β-un saturated esters.

Preparation

whereas the direct silylation of the lithium enolate of an ester normally results in the formation of a mixture of the α-silyl ester and the corresponding silyl ketene acetal, the same reaction with methyldiphenylchlorosilane gives exclusively the α-methyldiphenylsilyl ester. This direct C-silylation is the best general route to α-silyl esters.

ETHYL (DIPHENYLMETHYLSILYL)ACETATESupplier

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