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4-Aminobenzonitrile

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4-Aminobenzonitrile Basic information

Product Name:
4-Aminobenzonitrile
Synonyms:
  • 4-CyanobenzenaMine
  • 4-CyanobenzeneaMine
  • 4-CyanophenylaMine
  • NSC 7625
  • p-CyanophenylaMine
  • 4-AMinobenonitrile
  • 4-AMinobenzonitirle
  • 4-AMINOBENZONITRILE FOR SYNTHESIS
CAS:
873-74-5
MF:
C7H6N2
MW:
118.14
EINECS:
212-850-1
Product Categories:
  • FINE Chemical & INTERMEDIATES
  • Aromatic Nitriles
  • Nitriles
  • Benzonitriles (Building Blocks for Liquid Crystals)
  • Building Blocks for Liquid Crystals
  • Functional Materials
Mol File:
873-74-5.mol
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4-Aminobenzonitrile Chemical Properties

Melting point:
83-85 °C(lit.)
Boiling point:
167 °C / 1mmHg
Density 
1.1151 (rough estimate)
vapor pressure 
0.002-0.005Pa at 20-25℃
refractive index 
1.5500 (estimate)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form 
Crystalline Powder Chunks
pka
1.74(at 25℃)
color 
Off-white or beige to orange-yellow
Water Solubility 
Soluble in ethyl acetate, dichloromethane and chloroform. Insoluble in water.
BRN 
774507
Stability:
Toxic
InChIKey
YBAZINRZQSAIAY-UHFFFAOYSA-N
LogP
1 at 20℃ and pH7
CAS DataBase Reference
873-74-5(CAS DataBase Reference)
NIST Chemistry Reference
Benzonitrile, 4-amino-(873-74-5)
EPA Substance Registry System
Benzonitrile, 4-amino- (873-74-5)
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Safety Information

Hazard Codes 
Xn,Xi
Risk Statements 
22-36-36/37/38-20/21/22
Safety Statements 
26-36
RIDADR 
UN 2811 6.1/PG 3
WGK Germany 
3
RTECS 
BX2320000
Hazard Note 
Harmful
TSCA 
T
HazardClass 
6.1
PackingGroup 
III
HS Code 
29269095

MSDS

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4-Aminobenzonitrile Usage And Synthesis

Chemical Properties

off-white or beige to orange-yellow crystalline

Uses

4-Aminobenzonitrile is used as an amino substituted benzonitrile with hypotensive activity and as a radioprotective agent. It is also used as a derivatization reagent in the capillary zone electrophoretic analysis of aldoses, ketoses and uronic acid. Further, it is used in the preparation of methacrylic monomers containing pendant azobenzene structures and polythiophenes containing an azobenzene moiety in the side-chain.

Synthesis

Mixing the nitrobenzene substituent with ammonia gas and a second gas, and reacting in the presence of a catalyst to obtain the p-aminobenzonitrile, wherein the second gas is air, oxygen or inert gas.

Purification Methods

It crystallises from water, 5% aqueous EtOH or EtOH and is dried over P2O5 or dried in vacuo for 6hours at 40o. [Moore et al. J Am Chem Soc 108 2257 1986, Edidin et al. J Am Chem Soc 109 3945 1987, Beilstein 14 IV 1158.]

4-Aminobenzonitrile Preparation Products And Raw materials

Preparation Products

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