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3,4-Methylenedioxyacetophenone

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3,4-Methylenedioxyacetophenone Basic information

Product Name:
3,4-Methylenedioxyacetophenone
Synonyms:
  • 1-(1,3-Benzodioxol-5-yl)ethanone
  • 3,4-Methylen-dioxy-acetophenon
  • Methyl (1,3-benzodioxole-5-yl) ketone
  • Moskachan A
  • 3,4-Methylenedioxyacetophenone,98%
  • 3,4-Methylenedioxyac
  • 3,4-Methylenedioxyacetophenone, 98% 5GR
  • 3',4'-(Methylenedioxy)acetophenone 98%
CAS:
3162-29-6
MF:
C9H8O3
MW:
164.16
EINECS:
221-613-1
Product Categories:
  • Adehydes, Acetals & Ketones
  • C9
  • Aromatic Acetophenones & Derivatives (substituted)
  • Carbonyl Compounds
  • Ketones
Mol File:
3162-29-6.mol
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3,4-Methylenedioxyacetophenone Chemical Properties

Melting point:
87-89 °C(lit.)
Boiling point:
152-155°C 15mm
Density 
1.2132 (rough estimate)
refractive index 
1.5260 (estimate)
Flash point:
152-155°C/15mm
storage temp. 
Inert atmosphere,Room Temperature
form 
Crystalline Powder
color 
Beige
Odor
Heavy, sweet-floral and warm-herbaceous odor
Water Solubility 
Slightly soluble in water.
BRN 
139669
CAS DataBase Reference
3162-29-6(CAS DataBase Reference)
NIST Chemistry Reference
3',4'-(Methylenedioxy)acetophenone(3162-29-6)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
37/39-26-36-24/25
WGK Germany 
3
Hazard Note 
Irritant
HS Code 
29329990

MSDS

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3,4-Methylenedioxyacetophenone Usage And Synthesis

Chemical Properties

Colorless or white crystals. M.P. 89℃. Almost insoluble in water, soluble in alcohol and oils.

Uses

3?,4?-(Methylenedioxy)acetophenone is used in the synthesis of N-ethyl-1-(3,4-methylenedioxyphenyl)ethylamine.

Uses

3′,4′-(Methylenedioxy)acetophenone was used in the synthesis of N-ethyl-1-(3,4-methylenedioxyphenyl)ethylamine.

Definition

ChEBI: 3,4-Methylenedioxyacetophenone is a member of benzodioxoles.

Synthesis Reference(s)

Journal of the American Chemical Society, 79, p. 4507, 1957 DOI: 10.1021/ja01573a069

Synthesis

3,4-Methylenedioxyacetophenone's synthesis method: 1) from Piperonylic acid plus Acetic acid vapors at high temperature over catalyst (Thoria, e.g.). 2) from alpha-Methylpiperonylic acid by oxidation.

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