4'-n-Amylacetophenone Chemical Properties

Boiling point:

132-133°C 4mm

Density 

0,95 g/cm³

refractive index 

1.5140 to 1.5160

Flash point:

132-133°C/4mm

storage temp. 

Sealed in dry,Room Temperature

form 

clear liquid

color 

Colorless to Light yellow

Specific Gravity

0.95

InChI

InChI=1S/C13H18O/c1-3-4-5-6-12-7-9-13(10-8-12)11(2)14/h7-10H,3-6H2,1-2H3

InChIKey

KBKGPMDADJLBEM-UHFFFAOYSA-N

SMILES

C(=O)(C1=CC=C(CCCCC)C=C1)C

CAS DataBase Reference

37593-02-5(CAS DataBase Reference)

NIST Chemistry Reference

p-Pentylacetophenone(37593-02-5)

EPA Substance Registry System

Ethanone, 1-(4-pentylphenyl)- (37593-02-5)

Safety Information

TSCA 

Yes

HS Code 

2914390090

MSDS

• Language:English Provider:ALFA

4'-n-Amylacetophenone Usage And Synthesis

Chemical Properties

Light yellow transparent liquid

Uses

Intermediates of Liquid Crystals

Synthesis

GENERAL PROCEDURE: The reaction was carried out in a magnetically stirred circular three-necked flask equipped with a condenser, which was placed in a thermostatic oil bath. To a well stirred mixed solution of 4-pentylphenylacetylene (2 mmol) and H2O (8 mmol) was added zeolite (H-type, 100 mg) and the reaction mixture was stirred and reacted at 100 °C. The reaction progress was monitored by TLC and after complete disappearance of 4-pentylphenylacetylene or for a predetermined time, the reaction mixture was cooled to room temperature and diluted with ethyl acetate. The catalyst was separated by filtration and the solvent was subsequently evaporated under reduced pressure to give the crude product. The crude product was further purified by silica gel column chromatography (100-200 mesh) to give pure p-pentyl acetophenone. The structures of all the products were confirmed by 1H NMR and 13C NMR spectral data.

References

[1] Applied Catalysis A: General, 2015, vol. 505, p. 213 - 216
[2] European Journal of Organic Chemistry, 2018, vol. 2018, # 29, p. 3974 - 3981
[3] Tetrahedron Letters, 2013, vol. 54, # 33, p. 4414 - 4417
[4] Catalysis Communications, 2015, vol. 65, p. 102 - 104
[5] Applied Organometallic Chemistry, 2012, vol. 26, # 12, p. 722 - 726

4'-n-Amylacetophenone(37593-02-5)Related Product Information

• 4'-Hydroxyacetophenone
• 4-Nitroacetophenone
• 4'-Bromoacetophenone
• Acetophenone
• 2-Bromoacetophenone
• 4-Fluoroacetophenone
• 4'-Methylacetophenone
• 3-Nitroacetophenone
• 4'-(Trifluoromethyl)acetophenone
• 3-(4-CYCLOHEXYLBENZOYL)ACRYLIC ACID
• 4'-CYCLOHEXYLACETOPHENONE
• Adriamycin
• 4-N-NONYLACETOPHENONE
• 4'-N-HEPTYLACETOPHENONE
• NOGALAMYCIN
• 4'-N-OCTYLACETOPHENONE
• Phenylpentane
• 4'-N-HEXYLACETOPHENONE