Dichloroacetyl chloride

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Dichloroacetyl chloride

Product Name: Dichloroacetyl chloride
CAS No.: 79-36-7
Chemical Name: Dichloroacetyl chloride
Synonyms: 2,2-DICHLOROACETYL CHLORIDE;CHCl2COCl;2,2-dichloroac;2,2-dichloroacetyl;Dichloroacetyl chlor;Dichloracetylchlorid;DichloroacetylChoride;DICHLORACETYL CHLORIDE;dichloro-acetylchlorid;DICHLOROACETYL CHLORIDE
CBNumber: CB0153797
Molecular Formula: C2HCl3O
Formula Weight: 147.39
MOL File: 79-36-7.mol

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Dichloroacetyl chloride Property

Melting point:: <25 °C
Boiling point:: 107-108 °C (lit.)
Density: 1.532 g/mL at 25 °C (lit.)
refractive index: n20/D 1.46(lit.)
Flash point:: 66 °C
storage temp.: 2-8°C
solubility: Chloroform, Hexanes
form: Liquid
color: Clear colorless to light yellow
Specific Gravity: 1.537 (20/4℃)
Water Solubility: MAY DECOMPOSE
Sensitive: Moisture Sensitive
Merck: 14,3053
BRN: 1209426
Stability:: Stable. Combustible. Incompatible with water, alcohols and oxidizing agents. Fumes in air.
InChIKey: FBCCMZVIWNDFMO-UHFFFAOYSA-N
CAS DataBase Reference: 79-36-7(CAS DataBase Reference)
NIST Chemistry Reference: Acetyl chloride, dichloro-(79-36-7)
EPA Substance Registry System: Dichloroacetyl chloride (79-36-7)

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Safety

Hazard Codes: C,N
Risk Statements: 35-50
Safety Statements: 9-26-45-61
RIDADR: UN 1765 8/PG 2
WGK Germany: 2
RTECS: AO6650000
F: 19-21
Hazard Note: Corrosive/Moisture Sensitive
TSCA: Yes
HazardClass: 8
PackingGroup: II
HS Code: 29159000
Hazardous Substances Data: 79-36-7(Hazardous Substances Data)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H350May cause cancer

H400Very toxic to aquatic life

Precautionary statements

P202Do not handle until all safety precautions have been read and understood.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: D55008
Product name: Dichloroacetyl chloride
Purity: 98%
Packaging: 100g
Price: $71
Updated: 2024/03/01

Sigma-Aldrich

Product number: D55008
Product name: Dichloroacetyl chloride
Purity: 98%
Packaging: 5g
Price: $37
Updated: 2023/06/20

TCI Chemical

Product number: D0313
Product name: Dichloroacetyl Chloride
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $28
Updated: 2024/03/01

TCI Chemical

Product number: D0313
Product name: Dichloroacetyl Chloride
Purity: >98.0%(GC)(T)
Packaging: 500g
Price: $91
Updated: 2024/03/01

Alfa Aesar

Product number: B22296
Product name: Dichloroacetyl chloride, 97%
Packaging: 100g
Price: $31.65
Updated: 2024/03/01

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Dichloroacetyl chloride Chemical Properties,Usage,Production

Chemical Properties

Dichloroacetyl chloride (DCAC) is a colourless to light yellow fuming liquid with an acrid, penetrating odor. It is irritating to the eyes and mucous membranes (HSDB 2003b). DCAC is insoluble in water, but decomposes quickly to form HCl and dichloroacetic acid (t1/2 of hydrolysis of 0.0023 seconds in water at 25°C, and 0.2 seconds in 89.1:10.9 water-acetone at -20°C (Prager et al. 2001, Ugi and Beck 1961).

Uses

Dichloroacetyl Chloride is a reagent used in the synthesis of substituted benzothiazoles exhibiting antitumor and anticancer activity.

Preparation

Dichloroacetyl chloride can be synthesized by the reaction of dichloroacetic acid and chlorosulfonic acid. Or from the oxidation of trichloroethylene. Trichloroethylene and azobisisobutyronitrile (catalyst) were heated to 100°C, and oxygen was introduced to react under 0.6MPa pressure, maintaining the oil bath temperature at 110°C, and reacted for 10h, The product dichloroacetyl chloride is distilled off under normal pressure.

Definition

ChEBI: Dichloroacetyl chloride is the acyl chloride obtained by displacement of the hydroxy group of dichloroacetic acid by chloride. It has a role as a hapten. It derives from a dichloroacetic acid.

General Description

Dichloroacetyl chloride is a colorless liquid with a pungent odor. Flash point 151°F Boiling point 107-108°F. Vapors are irritating to the eyes and mucous membranes. Corrosive to metals and tissue.

Air & Water Reactions

Fumes in air. Decomposed by water to dichloroacetic acid and hydrochloric acid, both corrosive, with release of heat. (NIP).

Reactivity Profile

Solutions in acetone are stable for less than two hours and fresh solution should be prepared before each use (NIP). May react vigorously or explosively if mixed with diisopropyl ether or other ethers in the presence of trace amounts of metal salts [J. Haz. Mat., 1981, 4, 291].

Health Hazard

TOXIC; inhalation, ingestion or contact (skin, eyes) with vapors, dusts or substance may cause severe injury, burns or death. Contact with molten substance may cause severe burns to skin and eyes. Reaction with water or moist air will release toxic, corrosive or flammable gases. Reaction with water may generate much heat that will increase the concentration of fumes in the air. Fire will produce irritating, corrosive and/or toxic gases. Runoff from fire control or dilution water may be corrosive and/or toxic and cause pollution.

Fire Hazard

Combustible material: may burn but does not ignite readily. Substance will react with water (some violently) releasing flammable, toxic or corrosive gases and runoff. When heated, vapors may form explosive mixtures with air: indoors, outdoors and sewers explosion hazards. Most vapors are heavier than air. They will spread along ground and collect in low or confined areas (sewers, basements, tanks). Vapors may travel to source of ignition and flash back. Contact with metals may evolve flammable hydrogen gas. Containers may explode when heated or if contaminated with water.

Safety Profile

Questionable carcinogen with experimental tumorigenic data. Moderately toxic by ingestion, inhalation, and skin contact. Corrosive to the skin, eyes, and mucous membranes. Combustible when exposed to heat or flame. When heated to decomposition it emits toxic fumes of Cl-. See also CHLORIDES.

Dichloroacetyl chloride Preparation Products And Raw materials

Raw materials

2,2'-Azobis(2-methylpropionitrile) Oxygen Trichloroethylene Dichloroacetic acid Aluminum chloride Chlorosulfonic acid

Preparation Products

Tetrachlorvinphos HEPTENOPHOS Fluorochloridone Trichloroacetyl chloride 4'-Hydroxy-3'-methylacetophenone

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View Lastest Price from Dichloroacetyl chloride manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: Dichloroacetyl chloride 79-36-7
Price: US $9.90/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5tons
Release date: 2024-12-05

Hebei Chuanghai Biotechnology Co,.LTD

Product: Isoamyl acetate 79-36-7
Price: US $10.70/kg
Min. Order: 10kg
Purity: 99%
Supply Ability: 10000kg
Release date: 2024-08-20

Henan Fengda Chemical Co., Ltd

Product: Dichloroacetyl chloride 79-36-7
Price: US $50.00-1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2023-12-22

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DICHLOROACETYL CHLORIDE FOR SYNTHESIS

Dichloroacetyl chlor

Dichloroacetyl chloride, 97% 100ML

Dichloroacetyl chloride, 97% 500ML

2,2-dichloroac

Twochloroacetyl chloride

chlorurededichloracetyle

chlorurededichloracetyle[french][qr]

dichloro-acetylchlorid

dichloroethanoylchloride[qr]

Dichloroacetylchloride,97%

DichloroacetylChoride

Dichloracetylchlorid

Dichloroacetyl Chloride &gt

Dichloroacetyl Chloride (DCAC)

Vildagliptin Impurity 47

79-36-7

73-36-7

Cl2CHCOCl

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