ChemicalBook > CAS DataBase List > 3-Bromo-2-methoxypyridine

3-Bromo-2-methoxypyridine

Product Name
3-Bromo-2-methoxypyridine
CAS No.
13472-59-8
Chemical Name
3-Bromo-2-methoxypyridine
Synonyms
2-METHOXY-3-BROMOPYRIDINE;3-BROWN-2-METHOXYPYRIDINE;3-BROMO-2-METHOXYPYRIDINE;Pyridine, 3-bromo-2-methoxy-;3-Bromo-2-methoxypyridine >3-BROMO-2-METHOXYPYRIDINE ,98%;3-BroMo-2-Methoxypyridine, 95+%;3-Bromo-2-methoxypyridine ISO 9001：2015 REACH
CBNumber
CB0194569
Molecular Formula
C6H6BrNO
Formula Weight
188.02
MOL File
13472-59-8.mol
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3-Bromo-2-methoxypyridine Property

Boiling point:
87 °C(Press: 16 Torr)
Density 
1.5856 g/mL at 25 °C
refractive index 
1.566
Flash point:
93 °C
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
pka
1.04±0.10(Predicted)
form 
clear liquid
color 
Colorless to Light yellow
Water Solubility 
Not miscible or difficult to mix in water.
Sensitive 
Moisture Sensitive/Light Sensitive
InChIKey
PORGLLGXCAQORO-UHFFFAOYSA-N
CAS DataBase Reference
13472-59-8(CAS DataBase Reference)
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Safety

Hazard Codes 
Xn
Risk Statements 
22-37/38-41
Safety Statements 
26-36/37/39
WGK Germany 
3
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
687413
Product name
3-Bromo-2-methoxypyridine
Purity
96%
Packaging
1g
Price
$124
Updated
2023/01/07
TCI Chemical
Product number
B3737
Product name
3-Bromo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$39
Updated
2025/07/31
TCI Chemical
Product number
B3737
Product name
3-Bromo-2-methoxypyridine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$124
Updated
2025/07/31
TRC
Product number
B696878
Product name
3-Bromo-2-methoxypyridine
Packaging
1g
Price
$75
Updated
2021/12/16
Matrix Scientific
Product number
074014
Product name
3-Bromo-2-methoxypyridine
Purity
95+%
Packaging
1g
Price
$36
Updated
2021/12/16
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3-Bromo-2-methoxypyridine Chemical Properties,Usage,Production

Uses

It is employed in the facile synthesis of 2-unsubstituted benzofuran-3-carboxylates using diazo(trimethylsilyl)methyl magnesium bromide.

Synthesis

52200-48-3

124-41-4

13472-59-8

A) 3-bromo-2-chloropyridine (4.76 g) was dissolved in N,N-dimethylformamide (DMF, 30 mL) under argon protection. Subsequently, a methanolic solution of 28% sodium methanol (5.73 g) was added to this solution. The reaction mixture was stirred at 80°C for 30 minutes. After completion of the reaction, the mixture was cooled to room temperature and the reaction was quenched by the addition of water. The reaction mixture was extracted with ethyl acetate and the organic phases were combined. The organic phase was washed sequentially with water and saturated sodium chloride solution and dried over anhydrous magnesium sulfate. The solvent was removed by concentration under reduced pressure to give the crude product 3-bromo-2-methoxypyridine (4.43 g) as a light yellow oil.

References

[1] Patent: EP2816023, 2014, A1. Location in patent: Paragraph 0393; 0394

3-Bromo-2-methoxypyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Bromo-2-methoxypyridine manufacturers

Hebei Fengjia New Material Co., Ltd
Product
3-Bromo-2-methoxypyridine 13472-59-8
Price
US $3.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
100000
Release date
2024-08-19
Hebei Chuanghai Biotechnology Co., Ltd
Product
3-Bromo-2-methoxypyridine 13472-59-8
Price
US $9.90/KG
Min. Order
100KG
Purity
99%
Supply Ability
100 mt
Release date
2024-12-02
Dideu Industries Group Limited
Product
3-Bromo-2-methoxypyridine 13472-59-8
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-10-25

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