1H-Indole, 4-broMo-5-Methyl-
- Product Name
- 1H-Indole, 4-broMo-5-Methyl-
- CAS No.
- 610794-15-5
- Chemical Name
- 1H-Indole, 4-broMo-5-Methyl-
- Synonyms
- 4-BroMo-5-Methylindole;4-BroMo-5-Methyl-1H-indole;1H-Indole, 4-broMo-5-Methyl-
- CBNumber
- CB02606480
- Molecular Formula
- C9H8BrN
- Formula Weight
- 210.07
- MOL File
- 610794-15-5.mol
1H-Indole, 4-broMo-5-Methyl- Property
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Off-white to light yellow Solid
- InChI
- InChI=1S/C9H8BrN/c1-6-2-3-8-7(9(6)10)4-5-11-8/h2-5,11H,1H3
- InChIKey
- DVCLJDAZHYRZHZ-UHFFFAOYSA-N
- SMILES
- N1C2=C(C(Br)=C(C)C=C2)C=C1
N-Bromosuccinimide Price
- Product number
- B814620
- Product name
- 4-bromo-5-methyl-1H-indole
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FB141531
- Product name
- 4-Bromo-5-methyl-1H-indole
- Packaging
- 10mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FB141531
- Product name
- 4-Bromo-5-methyl-1H-indole
- Packaging
- 25mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- FB141531
- Product name
- 4-Bromo-5-methyl-1H-indole
- Packaging
- 50mg
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 9141AB
- Product name
- 4-Bromo-5-methyl-1H-indole
- Packaging
- 100mg
- Price
- $202.4
- Updated
- 2021/12/16
1H-Indole, 4-broMo-5-Methyl- Chemical Properties,Usage,Production
Synthesis
60956-25-4
4637-24-5
610794-15-5
Under nitrogen protection, 2-bromo-1,3-dimethyl-4-nitrobenzene (3.0 g, 13.04 mmol), pyrrolidine (926 mg, 13.04 mmol), and N,N-dimethylformamide dimethyl acetal (7.76 g, 65.22 mmol) were dissolved in 1,4-dioxane (20 mL) and the reaction was carried out for 18 hr at 100 °C. After completion of the reaction, the mixture was concentrated to dryness under reduced pressure. To the residue was added iron powder (3.65 g, 65.22 mmol) and acetic acid (40 mL) and heated at 110°C for 4 hours. The reaction solution was cooled to room temperature and filtered, and the filtrate was concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using petroleum ether/ethyl acetate (10:1) as eluent to afford 4-bromo-5-methyl-1H-indole (150 mg, 5.5% yield) as a yellow solid. Mass spectrum (ESI) m/z = 210.1 ([M+H]+).
References
[1] Patent: WO2013/26914, 2013, A1. Location in patent: Page/Page column 170
1H-Indole, 4-broMo-5-Methyl- Preparation Products And Raw materials
Raw materials
Preparation Products
1H-Indole, 4-broMo-5-Methyl- Suppliers
- Tel
- +1-858-6993322
- Fax
- (+1)-858-876-1948
- info@accelachem.com
- Country
- United States
- ProdList
- 21193
- Advantage
- 58
- Tel
- tp@aladdinsci.com
- Country
- United States
- ProdList
- 52923
- Advantage
- 58
- Tel
- --
- Fax
- --
- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
- 58
View Lastest Price from 1H-Indole, 4-broMo-5-Methyl- manufacturers
- Product
- 1H-Indole, 4-broMo-5-Methyl- 610794-15-5
- Price
- US $9.80/KG
- Min. Order
- 1g
- Purity
- ≥99%
- Supply Ability
- 100kg
- Release date
- 2020-01-14