1-Boc-5-hydroxyindole

Product Name: 1-Boc-5-hydroxyindole
CAS No.: 434958-85-7
Chemical Name: 1-Boc-5-hydroxyindole
Synonyms: 1-Boc-1H-indol-5-ol;5-AMINOPHTHALIC ACID;1-BOC-5-HYDROXYINDOLE;N-BOC-5-HYDROXYINDOLE;5-hydroxy-1-indolecarboxylate;5-hydroxy-1H-indole-1-carboxylate;tert-butyl 5-hydroxyindole-1-carboxylate;tert-butyl 5-hydroxy-1H-indole-1-carboxylate;1H-Indole-1-carboxylic acid, 5-hydroxy-,1,1-diMethylethyl ester
CBNumber: CB0275347
Molecular Formula: C13H15NO3
Formula Weight: 233.26
MOL File: 434958-85-7.mol

More

Less

1-Boc-5-hydroxyindole Property

Boiling point:: 374.5±34.0 °C(Predicted)
Density: 1.16±0.1 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 9.55±0.40(Predicted)
Appearance: White to off-white Solid
CAS DataBase Reference: 434958-85-7(CAS DataBase Reference)

More

Less

Safety

HS Code: 2933998090

More

Less

Hazard and Precautionary Statements (GHS)

More

Less

N-Bromosuccinimide Price

TRC

Product number: B656693
Product name: N-Boc-5-Hydroxyindole
Packaging: 500mg
Price: $130
Updated: 2021/12/16

Matrix Scientific

Product number: 072860
Product name: N-Boc-5-Hydroxyindole
Purity: 95+%
Packaging: 1g
Price: $163
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140244
Product name: tert-Butyl 5-hydroxy-1H-indole-1-carboxylate
Packaging: 5G
Price: $363
Updated: 2021/12/16

AK Scientific

Product number: W6280
Product name: N-Boc-5-Hydroxyindole
Packaging: 10g
Price: $537
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140244
Product name: tert-Butyl 5-hydroxy-1H-indole-1-carboxylate
Packaging: 10g
Price: $631.3
Updated: 2021/12/16

More

Less

1-Boc-5-hydroxyindole Chemical Properties,Usage,Production

Synthesis

170147-29-2

434958-85-7

General procedure for the synthesis of N-Boc-5-hydroxyindole from tert-butyl 5-(benzyloxy)-1H-indole-1-carboxylate: the product of Example 93A (680 mg, 2.103 mmol) was dissolved in ethanol (20 mL) under nitrogen protection, and 10% palladium carbon (68 mg) and ammonium formate (265 mg, 4.205 mmol) were added. After stirring the reaction for 1 h at room temperature, the reaction mixture was filtered through a 0.45 μm PTFE membrane and the catalyst was washed with methanol. The filtrate was concentrated by rotary evaporator and the resulting residue was dissolved in ethyl acetate (50 mL) and washed sequentially with water (2 × 25 mL) and saturated saline (25 mL). The organic phase was dried over anhydrous sodium sulfate, filtered and concentrated in vacuum to give N-Boc-5-hydroxyindole (475 mg, 96% yield) as a white solid.

References

[1] Patent: WO2007/76034, 2007, A2. Location in patent: Page/Page column 127
[2] Patent: WO2005/51957, 2005, A1. Location in patent: Page/Page column 57

1-Boc-5-hydroxyindole Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

1-Boc-5-hydroxyindole Suppliers

China 95 Germany 1 India 2 United Kingdom 3 United States 15 Global 116

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

JinYan Chemicals(ShangHai) Co.,Ltd.

Tel: 13817811078
Fax: 86-021-50426522,50426273
Email: sales@jingyan-chemical.com
Country: China
ProdList: 9976
Advantage: 60

China DongFan Chemical Co.,LTD

Tel: 86-0571-85151182
Fax: 86-0571-85151182
Country: China
ProdList: 5691
Advantage: 66

Shanghai AmasPharm Co., Ltd.

Tel: 021-54540637 18621091017
Fax: 021-34978309
Email: sales@amaspharm.com
Country: China
ProdList: 781
Advantage: 62

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
ProdList: 8669
Advantage: 57

Nanjing Vital Chemical Co., Ltd.

Tel: Please Send Email 18652950785
Fax: 025-87193546
Email: chemweiao@163.com
Country: China
ProdList: 4378
Advantage: 65

Sphinx Scientific Laboratory (Tianjin) Co., Ltd.

Tel: 022-66211289-843 13672102692
Fax: QQ：2377893365
Email: contact@sphinxpharm.com
Country: China
ProdList: 361
Advantage: 62

Hangzhou Yuhao Chemical Technology Co., Ltd

Tel: 0571-82693216
Fax: +86-571-82880190
Email: info@yuhaochemical.com
Country: China
ProdList: 6387
Advantage: 52

ZhengZhou HuaWen Chemical Co.Ltd

Tel: 0370-2785118 17550508557
Fax: QQ：3470079902
Email: 675141927@qq.com
Country: China
ProdList: 3199
Advantage: 55

T&W GROUP

Tel: 021-61551611 13296011611
Fax: ＋86 21-50676805
Email: contact@trustwe.com
Country: China
ProdList: 9895
Advantage: 58

More

Less

View Lastest Price from 1-Boc-5-hydroxyindole manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1-Boc-5-hydroxyindole 434958-85-7
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1-Boc-5-hydroxyindole 434958-85-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95%
Supply Ability: 500kg
Release date: 2018-08-19

434958-85-7, 1-Boc-5-hydroxyindoleRelated Search:

Indometacin Chrysin Indole-3-butyric acid Indole-3-acetic acid tert-Butyl acrylate tert-Butyl methacrylate TERT-BUTYL PROPIONATE 5-Hydroxyindole Butylparaben tert-Butyl bromoacetate tert-Butyl acetoacetate 1-BOC-5-METHOXYINDOLE 1-Boc-5-aminoindole t-butyl chloroformate 5-BENZYLOXY-1-BOC-INDOLE-2-BORONIC ACID 5-(TERT-BUTYLDIMETHYLSILYLOXY)-1H-INDOLE-2-BORONIC ACID, N-BOC PROTECTED 98 1-(TERT-BUTOXYCARBONYL)-5-METHOXY-1H-INDOL-2-YLBORONIC ACID 5-METHOXY-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

N-BOC-5-HYDROXYINDOLE

1-BOC-5-HYDROXYINDOLE

5-AMINOPHTHALIC ACID

1H-Indole-1-carboxylic acid, 5-hydroxy-,1,1-diMethylethyl ester

tert-butyl 5-hydroxy-1H-indole-1-carboxylate

5-hydroxy-1H-indole-1-carboxylate

5-hydroxy-1-indolecarboxylate

tert-butyl 5-hydroxyindole-1-carboxylate

1-Boc-1H-indol-5-ol

434958-85-7