ChemicalBook > CAS DataBase List > 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE

2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE

Product Name: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
CAS No.: 63897-12-1
Chemical Name: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
Synonyms: Zinc02559133;AURORA KA-3220;2,4-Dichloro-6-methyl-3-nitropyidine;2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE;2,4-Dichloro-6-Mehtyl-3-nitro-pyridine;Pyridine,2,4-dichloro-6-Methyl-3-nitro-;2,4-Dichloro-6-methyl-3-nitropyridine 98%;2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE ISO 9001：2015 REACH
CBNumber: CB0298506
Molecular Formula: C6H4Cl2N2O2
Formula Weight: 207.01
MOL File: 63897-12-1.mol

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2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Property

Melting point:: 75 °C
Boiling point:: 310.0±37.0 °C(Predicted)
Density: 1.537±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: -1.47±0.10(Predicted)
Appearance: Gray to brown Solid
InChI: InChI=1S/C6H4Cl2N2O2/c1-3-2-4(7)5(10(11)12)6(8)9-3/h2H,1H3
InChIKey: MTGIKTMXZFIZLS-UHFFFAOYSA-N
SMILES: C1(Cl)=NC(C)=CC(Cl)=C1[N+]([O-])=O

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Safety

Hazard Codes: Xn
Risk Statements: 22-41
Safety Statements: 26-39
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: D482838
Product name: 2,4-dichloro-6-methyl-3-nitropyridine
Packaging: 100mg
Price: $65
Updated: 2021/12/16

Matrix Scientific

Product number: 118838
Product name: 2,4-Dichloro-6-methyl-3-nitropyridine
Purity: 95+%
Packaging: 1g
Price: $432
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: COR0001564
Product name: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
Purity: 95.00%
Packaging: 1G
Price: $691.27
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H54-5-3H
Product name: 2,4-Dichloro-6-methyl-3-nitropyridine
Packaging: 1g
Price: $122
Updated: 2021/12/16

AK Scientific

Product number: V2378
Product name: 2,4-Dichloro-6-methyl-3-nitropyridine
Packaging: 1g
Price: $125
Updated: 2021/12/16

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2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Chemical Properties,Usage,Production

Synthesis

4966-90-9

63897-12-1

General procedure for the synthesis of 2,4-dichloro-6-methyl-3-nitropyridine from 4-hydroxy-6-methyl-3-nitro-2-pyridone: (1) 4-hydroxy-6-methyl-3-nitro-2-pyridone (1.7 g, 10 mmol) was dissolved in 10 mL of phosphorus oxychloride (POCl3), heated to 95 °C, and the reaction was stirred for 1.5 hours. Upon completion of the reaction, excess POCl3 was removed by centrifugation.Subsequently, the reaction was quenched by slow addition of 100 mL of ice water. The reaction mixture was extracted with ethyl acetate (80 mL x 3). The organic phases were combined, washed with saturated sodium chloride solution, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to give 1.773 g of yellow powdery product in 85.7% yield.

References

[1] Journal of Medicinal Chemistry, 2005, vol. 48, # 16, p. 5104 - 5107
[2] Patent: US2012/289497, 2012, A1. Location in patent: Page/Page column 40
[3] Patent: EP2524917, 2012, A1. Location in patent: Page/Page column 43-44
[4] Patent: WO2008/119713, 2008, A1. Location in patent: Page/Page column 65
[5] Journal of Medicinal Chemistry, 2008, vol. 51, # 22, p. 7273 - 7286

2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Suppliers

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View Lastest Price from 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-18

Dideu Industries Group Limited

Product: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-07

Career Henan Chemical Co

Product: 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-03

63897-12-1, 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINERelated Search:

2,4-DICHLORO-5-ISOPROPOXYANILINE 4-Chloro-3-nitropyridine hydrochloride 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 4-Chloro-3-nitropyridine 3-AMINO-2-CHLOROPYRIDINE 5-Amino-2-methylpyridine 2-CHLORO-3-NITROPYRIDINE 2,4-Dichloro-3-nitropyridine 3-Amino-4-chloropyridine 4-Chloro-2-picoline 2-Chloro-3-nitro-6-methylpyridine 2-Methyl-5-nitropyridine 3-AMINO-2-CHLORO-6-PICOLINE 2,6-Dichloro-4-methyl-3-nitropyridine 2,4-Dichloro-6-picoline Pyridine,2,4-dichloro-5,6-dimethyl-3-nitro- CHEMPACIFIC 38112 2,4-DICHLORO-3-AMINOPYRIDINE

2,4-Dichloro-6-methyl-3-nitropyridine 98%

AURORA KA-3220

2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE

2,4-Dichloro-6-methyl-3-nitropyidine

Zinc02559133

Pyridine,2,4-dichloro-6-Methyl-3-nitro-

2,4-Dichloro-6-Mehtyl-3-nitro-pyridine

2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE ISO 9001：2015 REACH

63897-12-1

Heterocycle-Pyridine series

Pyridine