2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
- Product Name
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
- CAS No.
- 63897-12-1
- Chemical Name
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
- Synonyms
- Zinc02559133;AURORA KA-3220;2,4-Dichloro-6-methyl-3-nitropyidine;2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE;2,4-Dichloro-6-Mehtyl-3-nitro-pyridine;Pyridine,2,4-dichloro-6-Methyl-3-nitro-;2,4-Dichloro-6-methyl-3-nitropyridine 98%;2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE ISO 9001：2015 REACH
- CBNumber
- CB0298506
- Molecular Formula
- C6H4Cl2N2O2
- Formula Weight
- 207.01
- MOL File
- 63897-12-1.mol
2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Property
- Melting point:
- 75 °C
- Boiling point:
- 310.0±37.0 °C(Predicted)
- Density
- 1.537±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- -1.47±0.10(Predicted)
- Appearance
- Gray to brown Solid
- InChI
- InChI=1S/C6H4Cl2N2O2/c1-3-2-4(7)5(10(11)12)6(8)9-3/h2H,1H3
- InChIKey
- MTGIKTMXZFIZLS-UHFFFAOYSA-N
- SMILES
- C1(Cl)=NC(C)=CC(Cl)=C1[N+]([O-])=O
N-Bromosuccinimide Price
- Product number
- D482838
- Product name
- 2,4-dichloro-6-methyl-3-nitropyridine
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 118838
- Product name
- 2,4-Dichloro-6-methyl-3-nitropyridine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $432
- Updated
- 2021/12/16
- Product number
- COR0001564
- Product name
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $691.27
- Updated
- 2021/12/16
- Product number
- 4H54-5-3H
- Product name
- 2,4-Dichloro-6-methyl-3-nitropyridine
- Packaging
- 1g
- Price
- $122
- Updated
- 2021/12/16
- Product number
- V2378
- Product name
- 2,4-Dichloro-6-methyl-3-nitropyridine
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Chemical Properties,Usage,Production
Synthesis
4966-90-9
63897-12-1
General procedure for the synthesis of 2,4-dichloro-6-methyl-3-nitropyridine from 4-hydroxy-6-methyl-3-nitro-2-pyridone: (1) 4-hydroxy-6-methyl-3-nitro-2-pyridone (1.7 g, 10 mmol) was dissolved in 10 mL of phosphorus oxychloride (POCl3), heated to 95 °C, and the reaction was stirred for 1.5 hours. Upon completion of the reaction, excess POCl3 was removed by centrifugation.Subsequently, the reaction was quenched by slow addition of 100 mL of ice water. The reaction mixture was extracted with ethyl acetate (80 mL x 3). The organic phases were combined, washed with saturated sodium chloride solution, dried over anhydrous sodium sulfate, and concentrated under reduced pressure to give 1.773 g of yellow powdery product in 85.7% yield.
References
[1] Journal of Medicinal Chemistry, 2005, vol. 48, # 16, p. 5104 - 5107
[2] Patent: US2012/289497, 2012, A1. Location in patent: Page/Page column 40
[3] Patent: EP2524917, 2012, A1. Location in patent: Page/Page column 43-44
[4] Patent: WO2008/119713, 2008, A1. Location in patent: Page/Page column 65
[5] Journal of Medicinal Chemistry, 2008, vol. 51, # 22, p. 7273 - 7286
2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE Suppliers
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- Country
- India
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View Lastest Price from 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE manufacturers
- Product
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-18
- Product
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons min
- Release date
- 2021-09-07
- Product
- 2,4-DICHLORO-6-METHYL-3-NITROPYRIDINE 63897-12-1
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-03