ChemicalBook > CAS DataBase List > 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE

2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE

Product Name: 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE
CAS No.: 426463-09-4
Chemical Name: 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE
Synonyms: 2-Chloro-5-iodopyridin-3-aMine;2-chloro-5-iodo-3-pyridinamine;3-AMINO-2-CHLORO-5-IODOPYRIDINE;2-Chloro-3-amino--5-iodopyridine;3-PyridinaMine, 2-chloro-5-iodo-;2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE;2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE ISO 9001：2015 REACH
CBNumber: CB0681601
Molecular Formula: C5H4ClIN2
Formula Weight: 254.46
MOL File: 426463-09-4.mol

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2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE Property

Melting point:: 128-133°C
Boiling point:: 352.5±42.0 °C(Predicted)
Density: 2.139±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
form: solid
pka: 0.27±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xn
Risk Statements: 22-41
Safety Statements: 26-39
WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H318Causes serious eye damage

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 720372
Product name: 3-Amino-2-chloro-5-iodopyridine
Purity: 97%
Packaging: 1g
Price: $108
Updated: 2023/01/07

Ark Pharm

Product number: AK113412
Product name: 2-Chloro-5-iodopyridin-3-amine
Purity: 97%
Packaging: 25g
Price: $665
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0066602
Product name: 3-AMINO-2-CHLORO-5-IODOPYRIDINE
Purity: 95.00%
Packaging: 1G
Price: $720.98
Updated: 2021/12/16

AK Scientific

Product number: 5887AB
Product name: 2-Chloro-5-iodopyridin-3-amine
Packaging: 250mg
Price: $81
Updated: 2021/12/16

Crysdot

Product number: CD11125252
Product name: 2-Chloro-5-iodopyridin-3-amine
Purity: 95+%
Packaging: 1g
Price: $100
Updated: 2021/12/16

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2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE Chemical Properties,Usage,Production

Synthesis

426463-05-0

426463-09-4

General procedure for the synthesis of 3-amino-2-chloro-5-iodopyridine from 2-chloro-5-iodo-3-nitropyridine: 5-iodo-3-nitro-2-chloropyridine (230 mg, 0.809 mmol), ethanol (1 mL), water (6 drops), and concentrated hydrochloric acid (0.020 mL) were stirred at room temperature for 10 minutes. Subsequently, iron powder (500 mg, 8.95 mmol) was added in small portions and the reaction mixture was heated in an oil bath at 100 °C for 20 min. After completion of the reaction, the iron powder was removed by filtration and the filtrate was washed with ethanol. The ethanol layers were combined and concentrated under reduced pressure. The crude product was purified by fast chromatography using 9:1 hexane:ethyl acetate as eluent to afford 5-iodo-3-amino-2-chloropyridine (190 mg, 92% yield) as a colorless solid with a melting point of 129 °C. 1H NMR (CDCl3) δ (ppm): 4.15 (broad single peak, 2H), 7.34 (double peak, J = 2.0 Hz, 1H), and 7.96 (double peaks, J = 2.0 Hz, 1H); 13C NMR (CDCl3) δ (ppm): 91.41, 129.67, 136.31, 140.77, 143.90. Calculated values for elemental analysis (C5H4N2Cl): C, 23.60; H, 1.58; N, 11.01; Measured values: C, 23.66; H 1.52; N, 10.98.

References

[1] Journal of Organic Chemistry, 2011, vol. 76, # 23, p. 9841 - 9844
[2] Journal of Medicinal Chemistry, 2002, vol. 45, # 21, p. 4755 - 4761
[3] Patent: US6538010, 2003, B1
[4] Bioorganic & Medicinal Chemistry Letters, 2003, vol. 13, # 3, p. 525 - 528

2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE manufacturers

Dideu Industries Group Limited

Product: 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE 426463-09-4
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons min
Release date: 2021-09-01

426463-09-4, 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINERelated Search:

3-aMino-5-broMo-4-chloropyridine 3-Amino-6-trifluoromethyl-pyridin-2-ol 3-AMINO-6-IODOPYRAZINE-2-CARBOXYLIC ACID METHYL ESTER 3-amino-6-chloropyrazine-2-carboxylic acid 3-AMINO-4-METHOXYPYRIDINE 3-AMINO-3-(4-CYANOPHENYL)PROPANOIC ACID 3-Amino-5-chloropyridin-2-ol HCl (3-aminopyrazin-2-yl)methanol 3-Amino-3-(4-methoxyphenyl)propionic acid 3-PYRIDINAMINE, 6-(1-METHYLETHYL)- 3-AMINO-5-HYDROXYBENZOIC ACID 2-CHLORO-5-(TRIFLUOROMETHYL)-3-PYRIDINAMINE 5-IODO-PYRIDIN-3-YLAMINE 2-Chloro-5-iodopyridine 5-CHLORO-3-IODO-PYRIDIN-2-YLAMINE 2-Chloro-5-iodo-3-nitropyridine 2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE 4-CHLORO-3-IODO-PYRIDIN-2-YLAMINE

2-Chloro-5-iodopyridin-3-aMine

2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE

3-PyridinaMine, 2-chloro-5-iodo-

3-AMINO-2-CHLORO-5-IODOPYRIDINE

2-chloro-5-iodo-3-pyridinamine

2-Chloro-3-amino--5-iodopyridine

2-CHLORO-5-IODO-PYRIDIN-3-YLAMINE ISO 9001：2015 REACH

426463-09-4

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