1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

Uses

Product Name: 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
CAS No.: 41481-63-4
Chemical Name: 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
Synonyms: Diallyl Ether Bisphenol-S;BIS(4-ALLYLOXYPHENYL)SULFONE;Bis(p-allyloxyphenyl) sulfone;4,4'-Sulfonylbis((allyloxy)benzene);4,4'-Sulfonylbis((allyloxy)benzene);Bis-[4-(2propenyloxy)-phenyl]-sulfone;1-(benzenesulfonyl)-4-prop-2-enoxybenzene;Sulfonylbis(4,1-phenylene)bis(allyl ether);1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER;1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene]
CBNumber: CB0696083
Molecular Formula: C18H18O4S
Formula Weight: 330.4
MOL File: 41481-63-4.mol

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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Property

Melting point:: 141-142 °C(Solv: ethanol (64-17-5))
Boiling point:: 500.7±45.0 °C(Predicted)
Density: 1.171±0.06 g/cm3(Predicted)
storage temp.: -20°C Freezer, Under inert atmosphere
solubility: DMSO (Slightly), Methanol (Slightly)
form: Solid
color: White to Off-White
CAS DataBase Reference: 41481-63-4(CAS DataBase Reference)

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: A614508
Product name: bis(4-Allyloxyphenyl)sulfone
Packaging: 10g
Price: $245
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB147064
Product name: Bis(4-allyloxyphenyl)sulfone
Packaging: 100g
Price: $376
Updated: 2021/12/16

AK Scientific

Product number: P143
Product name: 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene]
Packaging: 100g
Price: $557
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB147064
Product name: Bis(4-allyloxyphenyl)sulfone
Packaging: 250g
Price: $752.5
Updated: 2021/12/16

AK Scientific

Product number: P143
Product name: 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene]
Packaging: 250g
Price: $1065
Updated: 2021/12/16

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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Chemical Properties,Usage,Production

Uses

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is a useful research chemical.

Chemical Properties

White crystalline powder

Preparation

The preparation of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is as follows:2400g water, 216g caustic soda lye of 48% strength, 600g 4,4'-dihydroxydiphenyl sulfone and 204g Allyl chloride were mixed and the reaction was carried out at 55-60°C and autogenously generated pressure of 0.8-1. Okg/cm2 for 8 hours. 204g caustic soda lye of 48% strength was added in the reaction mixture, and maintained for 1 hour at 80°C thereafter filtered at 80°C to remove 4,4'-diallyloxydiphenyl sulfone. Further, the filtrate solution was treated with 5g activated carbon and 5g sequestering agent at 85- 90°C. The pH of filtrated solution was adjusted to 8.9 with 20% sulfuric acid and cooled to 35°C. The precipitate was separated by filtration and slurred in water. The pH was adjusted to 4.94 with 20% sulfuric acid and the precipitate was separated by filtration, and washed with water and dried to obtain 615g the product 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity. The yield was 93.5% with respect to 4,4'-dihydroxydiphenyl sulfone. The wet cake of 4,4'-diallyloxydiphenyl sulfone was slurred in 100g of 5%w/v aqueous solution of sodium hydroxide and refluxed for 1 hour, then cooled to 80°C. The precipitate was filtered, washed with water and dried to obtain 45g of 4,4'-diallyloxy diphenyl sulfone of 91.9% purity. The yield was 6% with respect to 4,4'-dihydroxydiphenyl sulfone. pH of the mother liquor obtained after separation of 4-allyloxy 4'-hydroxydiphenyl sulfone, was adjusted to 4.5 with 20% sulfuric acid. The precipitate was separated by filtration, washed with water and dried to obtain 33g of 4,4'-dihydroxydiphenyl sulfone of 87.9% purity. The conversion of 4,4'-dihydroxydiphenyl sulfone was 94.50%.; 595g of 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity was dissolved in 230g of 48% strength caustic soda lye and 1000g water, treated with 5g activated carbon and 5g sequestering agent at 85-90°C. The slurry was filtered and pH of the filtrate was adjusted to 8.95 with 20% sulfuric acid and then cooled to 35°C. The precipitate was separated by filtration, slurried in water and the pH was adjusted to 5.0 with 20% sulfuric acid. The slurry was filtrated and the precipitate was washed with water and dried to obtain 563g of 4- allyloxy 4'-hydroxydiphenyl sulfone of 99.273% purity.

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Preparation Products And Raw materials

Raw materials

Preparation Products

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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Suppliers

China 71 Europe 2 Germany 2 United Kingdom 5 United States 15 Global 95

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View Lastest Price from 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene 41481-63-4
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-09-19

Zhuozhou Wenxi import and Export Co., Ltd

Product: 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene 41481-63-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

Career Henan Chemical Co

Product: 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene 41481-63-4
Price: US $2.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: ask
Release date: 2018-12-22

41481-63-4, 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzeneRelated Search:

Sulfuryl chloride 3-(METHOXYMETHOXY)BENZALDEHYDE p-Anisaldehyde Xylene m-Anisyl alcohol Benzene Anisole 2-Phenoxyethanol (Trifluoromethoxy)benzene o-Anisaldehyde 4-Methoxybenzoic acid Allyl ether Bis(4-hydroxyphenyl) Sulfone 4,4'-Thiobis-phenol Bis(4-methoxyphenyl) sulfoxide 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene 4-((3,5-DIMETHYL-4-[(2,3,3-TRICHLOROACRYLOYL)OXY]PHENYL)SULFONYL)-2,6-DIMETHYLPHENYL 2,3,3-TRICHLOROACRYLATE 4-((4-[(2,3,3-TRICHLOROACRYLOYL)OXY]PHENYL)SULFONYL)PHENYL 2,3,3-TRICHLOROACRYLATE

1-(benzenesulfonyl)-4-prop-2-enoxybenzene

1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene]

1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER

1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether

Bis-[4-(2propenyloxy)-phenyl]-sulfone

Bis(p-allyloxyphenyl) sulfone

Sulfonylbis(4,1-phenylene)bis(allyl ether)

1-allyloxy-4-(4-allyloxyphenyl)sulfonyl-benzene

1-prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene

BIS(4-ALLYLOXYPHENYL)SULFONE

Diallyl Ether Bisphenol-S

Benzene, 1,1'-sulfonylbis[4-(2-propen-1-yloxy)-

4,4'-Sulfonylbis((allyloxy)benzene)

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

4,4'-Sulfonylbis((allyloxy)benzene)

41481-63-4

C18H18O4S

Industrial/Fine Chemicals

Aromatics