ChemicalBook > CAS DataBase List > 3-Chloro-2-nitroaniline

3-Chloro-2-nitroaniline

Product Name: 3-Chloro-2-nitroaniline
CAS No.: 59483-54-4
Chemical Name: 3-Chloro-2-nitroaniline
Synonyms: TIMTEC-BB SBB008617;2-Nitro-3-chloroaniline;3-CHLORO-2-NITROANILINE;3-Chloro-2-nitroaniline 98%;2-Amino-6-chloronitrobenzene;3-CHLORO-2-NITRO-PHENYLAMINE;3-Chloro-2-nitroaniline, 95+%;Benzenamine, 3-chloro-2-nitro-;3-Chloro-2-nitroaniline, CAS 59483-54-4;3-Chloro-2-nitroaniline ISO 9001：2015 REACH
CBNumber: CB0733270
Molecular Formula: C6H5ClN2O2
Formula Weight: 172.57
MOL File: 59483-54-4.mol

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3-Chloro-2-nitroaniline Property

Melting point:: 107-108°C
Boiling point:: 327.1±22.0 °C(Predicted)
Density: 1.494±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
pka: -1.29±0.10(Predicted)
Appearance: Orange to red Solid
InChI: InChI=1S/C6H5ClN2O2/c7-4-2-1-3-5(8)6(4)9(10)11/h1-3H,8H2
InChIKey: YADOEPHJIBKBCN-UHFFFAOYSA-N
SMILES: C1(N)=CC=CC(Cl)=C1[N+]([O-])=O
CAS DataBase Reference: 59483-54-4(CAS DataBase Reference)

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Safety

Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 072902
Product name: 3-Chloro-2-nitroaniline
Purity: 95+%
Packaging: 5g
Price: $25
Updated: 2021/12/16

Oakwood

Product number: 011628
Product name: 3-Chloro-2-nitroaniline
Packaging: 5g
Price: $25
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC32786
Product name: 3-Chloro-2-nitroaniline
Packaging: 5G
Price: $30
Updated: 2021/12/16

AK Scientific

Product number: A974
Product name: 3-Chloro-2-nitroaniline
Packaging: 5g
Price: $41
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC32786
Product name: 3-Chloro-2-nitroaniline
Packaging: 10g
Price: $50
Updated: 2021/12/16

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3-Chloro-2-nitroaniline Chemical Properties,Usage,Production

Chemical Properties

red powder

Synthesis

4771-47-5

59483-54-4

General procedure for the synthesis of 3-chloro-2-nitroaniline from 3-chloro-2-nitrobenzoic acid: 3-chloro-2-nitrobenzoic acid (20 g, 99 mmol) and triethylamine (Et3N, 20.74 mL, 149 mmol) were dissolved in N,N-dimethylformamide (DMF, 100 mL), followed by the addition of diphenylphosphonium chloride (32.8 g, 119 mmol). The reaction mixture was stirred at room temperature for 3 hours. Next, water (200 mL) was added to the reaction mixture and heated at 100 °C for 1 hour. After the reaction was completed, the solution was cooled to room temperature. The device was short range distillation head and DMF was removed by high vacuum distillation. the remaining solid was dissolved in ethyl acetate (EtOAc) and washed with saturated sodium bicarbonate (NaHCO3) solution. The organic phase was filtered through diatomaceous earth, the filtrate was washed sequentially with water (3 times) and brine, dried over anhydrous sodium sulfate (Na2SO4), filtered, and concentrated under reduced pressure to afford the target product 3-chloro-2-nitroaniline 10 g in 53.4% yield. m/z 173.1 (M + H)+ with retention time of 1.67 min by LC-MS.

References

[1] Patent: WO2015/92713, 2015, A1. Location in patent: Page/Page column 273
[2] Journal of Organic Chemistry, 1977, vol. 42, # 1, p. 166 - 169
[3] Journal of Medicinal Chemistry, 1993, vol. 36, # 11, p. 1630 - 1640
[4] Journal of Medicinal Chemistry, 1992, vol. 35, # 23, p. 4455 - 4463
[5] Patent: US6358946, 2002, B1. Location in patent: Page column 5

3-Chloro-2-nitroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-Chloro-2-nitroaniline manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 3-Chloro-2-nitroaniline 59483-54-4
Price: US $1.10-9.90/KG
Min. Order: 1KG
Purity: 99%min
Supply Ability: 100KG
Release date: 2025-08-20

Dideu Industries Group Limited

Product: 3-Chloro-2-nitroaniline 59483-54-4
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-26

Zhuozhou Wenxi import and Export Co., Ltd

Product: 3-Chloro-2-nitroaniline 59483-54-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-08-11

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3-Chloro-2-nitroaniline, CAS 59483-54-4

59483-54-4

59483-54-0

C6H5CIN2O2

Amines

blocks

NitroCompounds

Pyridines

Anilines, Aromatic Amines and Nitro Compounds