ChemicalBook > CAS DataBase List > 4-BROMO-6-FLUOROINDAN-1-ONE

4-BROMO-6-FLUOROINDAN-1-ONE

Product Name: 4-BROMO-6-FLUOROINDAN-1-ONE
CAS No.: 174603-56-6
Chemical Name: 4-BROMO-6-FLUOROINDAN-1-ONE
Synonyms: 4-BROMO-6-FLUOROINDAN-1-ONE;4-Bromo-6-fluoro-1-indanone;4-bromo-6-fluoro-2,3-dihydroinden-1-one;4-broMo-6-fluoro-2,3-dihydro-1H-inden-1-one;1H-Inden-1-one,4-broMo-6-fluoro-2,3-dihydro-
CBNumber: CB0842154
Molecular Formula: C9H6BrFO
Formula Weight: 229.05
MOL File: 174603-56-6.mol

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4-BROMO-6-FLUOROINDAN-1-ONE Property

Boiling point:: 301.1±42.0 °C(Predicted)
Density: 1.691±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to light brown Solid
InChI: InChI=1S/C9H6BrFO/c10-8-4-5(11)3-7-6(8)1-2-9(7)12/h3-4H,1-2H2
InChIKey: KBBCLUTZUIWTON-UHFFFAOYSA-N
SMILES: C1(=O)C2=C(C(Br)=CC(F)=C2)CC1

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Safety

HS Code: 2914790090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B293365
Product name: 4-Bromo-6-fluoroindan-1-one
Packaging: 50mg
Price: $130
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0036676
Product name: 4-BROMO-6-FLUOROINDAN-1-ONE
Purity: 95.00%
Packaging: 5G
Price: $1437.98
Updated: 2021/12/16

AK Scientific

Product number: W3816
Product name: 4-Bromo-6-fluoroindan-1-one
Packaging: 10g
Price: $2255
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0036676
Product name: 4-BROMO-6-FLUOROINDAN-1-ONE
Purity: 95.00%
Packaging: 25G
Price: $3228.23
Updated: 2021/12/16

AccelPharmtech

Product number: M1064
Product name: 4-bromo-6-fluoro-2,3-dihydroinden-1-one
Purity: 97.00%
Packaging: 25G
Price: $4320
Updated: 2021/12/16

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4-BROMO-6-FLUOROINDAN-1-ONE Chemical Properties,Usage,Production

Synthesis

174603-55-5

174603-56-6

Under argon protection, 3-(2-bromo-4-fluorophenyl)propionic acid (1.2 g) was added to trifluoromethanesulfonic acid (15 mL) in batches and the reaction was carried out at room temperature. Subsequently, the reaction mixture was stirred at 60°C for 2 hours, then warmed to 80°C and continued stirring for 16 hours. After completion of the reaction, it was cooled to room temperature and the mixture was slowly poured into ice water. The aqueous phase was extracted twice with ethyl acetate. The organic phase was combined and washed sequentially with saturated aqueous Na2CO3 and brine. The organic phase was dried over anhydrous MgSO4 and concentrated under reduced pressure to remove the solvent. The resulting residue was stirred with dichloromethane (40 mL), filtered and washed with dichloromethane. The dichloromethane phase was combined and concentrated to give the target compound 4-bromo-6-fluoro-2,3-dihydro-1H-inden-1-one. Yield: 970 mg; liquid chromatography (Method 3): tR = 0.60 min; mass spectrometry (ESI+): m/z = 229 [M + H]+.

References

[1] Journal of Medicinal Chemistry, 2003, vol. 46, # 3, p. 409 - 416
[2] Patent: WO2013/144098, 2013, A1. Location in patent: Page/Page column 114; 115
[3] Patent: WO2015/36759, 2015, A1

4-BROMO-6-FLUOROINDAN-1-ONE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-BROMO-6-FLUOROINDAN-1-ONE manufacturers

Shanghai Rlavie Technology Co ltd

Product: 4-Bromo-6-fluoro-1-indanone 174603-56-6
Price: US $0.00/KG
Min. Order: 1g
Purity: 98%min
Supply Ability: 5kgs/month
Release date: 2021-07-11

Career Henan Chemical Co

Product: 4-BROMO-6-FLUOROINDAN-1-ONE 174603-56-6
Price: US $7.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 1000kg
Release date: 2020-01-13

174603-56-6, 4-BROMO-6-FLUOROINDAN-1-ONERelated Search:

4-Bromo-1-indanone 4-BROMO-7-CHLORO-1-INDANONE 4-broMo-7-fluoro-2,3-dihydroinden-1-one 4-Bromo-7-methoxy-indan-1-one 4-Bromo-5-chloro-2,3-dihydro-1H-inden-1-one 4-Isopropylphenol 1H-Inden-1-one, 6-broMo-5-chloro-2,3-dihydro- 6-Chloro-5-fluoro-2,3-dihydro-1H-inden-1-one 4-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL 4,6-dimethyl-1H-indene 6-Fluoro-1-indanone 4-BROMO-6-FLUORO-7-HYDROXY-3-METHYLINDAN-1-ONE 4-BROMO-6-FLUOROINDAN-1-ONE

4-BROMO-6-FLUOROINDAN-1-ONE

1H-Inden-1-one,4-broMo-6-fluoro-2,3-dihydro-

4-Bromo-6-fluoro-1-indanone

4-broMo-6-fluoro-2,3-dihydro-1H-inden-1-one

4-bromo-6-fluoro-2,3-dihydroinden-1-one

174603-56-6