6-Bromoquinoline-2-carboxylic acid

Product Name: 6-Bromoquinoline-2-carboxylic acid
CAS No.: 65148-10-9
Chemical Name: 6-Bromoquinoline-2-carboxylic acid
Synonyms: 6-Bromoquinaldic acid;6-BROMO-2-CARBOXYQUINOLINE;6-BroMo-quinolin-2-carboxylic acid;6-BROMO-2-QUINOLINECARBOXYLIC ACID;6-Bromoquinoline-2-carboxylic acid;2-Quinolinecarboxylic acid, 6-bromo-
CBNumber: CB0947486
Molecular Formula: C10H6BrNO2
Formula Weight: 252.06
MOL File: 65148-10-9.mol

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6-Bromoquinoline-2-carboxylic acid Property

Melting point:: 226 °C(Solv: methanol (67-56-1))
Boiling point:: 403.1±30.0 °C(Predicted)
Density: 1.732±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 4.45±0.43(Predicted)
Appearance: Light brown to brown Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B695918
Product name: 6-Bromoquinoline-2-carboxylicacid
Packaging: 25mg
Price: $45
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB44051
Product name: 6-Bromoquinoline-2-carboxylic acid
Packaging: 250mg
Price: $195
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB44051
Product name: 6-Bromoquinoline-2-carboxylic acid
Packaging: 500mg
Price: $300
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB44051
Product name: 6-Bromoquinoline-2-carboxylic acid
Packaging: 1g
Price: $380
Updated: 2021/12/16

AK Scientific

Product number: V0525
Product name: 6-Bromoquinoline-2-carboxylicacid
Packaging: 5g
Price: $591
Updated: 2021/12/16

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6-Bromoquinoline-2-carboxylic acid Chemical Properties,Usage,Production

Synthesis

1020567-35-4

65148-10-9

1b) Synthesis of 6-bromo-2-quinolinecarboxylic acid: Concentrated sulfuric acid (0.75 L) was slowly added to an aqueous (1.75 L) suspension of 6-bromo-2-(tribromomethyl)quinoline (350 g, 0.76 mol) over a period of 15 min under stirring conditions. The reaction mixture was heated at 150 °C (oil bath temperature) for 5 hours. After completion of the reaction, the mixture was cooled, the precipitate was collected by filtration, washed with water and dried to give 6-bromo-2-quinolinecarboxylic acid solid (127.6 g). The filtrate was diluted with water (3 L) to further precipitate a second product (55.7 g) in a combined yield of 183.3 g in 96% yield. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 8.50 (d, J = 9 Hz, 1H), 8.38 (d, J = 2 Hz, 1H), 8.13 (d, J = 9 Hz, 1H), 8.06 (d, J = 9 Hz, 1H), 7.96 (m, 1H). an ES-LCMS assay showed m/z 253 ([M + H] +).

References

[1] Patent: US2008/96921, 2008, A1. Location in patent: Page/Page column 32
[2] Journal of Labelled Compounds and Radiopharmaceuticals, 1998, vol. 41, # 12, p. 1103 - 1126

6-Bromoquinoline-2-carboxylic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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6-Bromoquinoline-2-carboxylic acid Suppliers

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View Lastest Price from 6-Bromoquinoline-2-carboxylic acid manufacturers

Zhuozhou Wenxi import and Export Co., Ltd

Product: 6-BroMo-quinolin-2-carboxylic acid 65148-10-9
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

Career Henan Chemical Co

Product: 6-Bromoquinoline-2-carboxylic acid 65148-10-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-12-31

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65148-10-9