2-Bromo-5-methoxybenzonitrile
- Product Name
- 2-Bromo-5-methoxybenzonitrile
- CAS No.
- 138642-47-4
- Chemical Name
- 2-Bromo-5-methoxybenzonitrile
- Synonyms
- KML-45;4-Bromo-3-cyanoanisole;2-BROMO-5-METHOXYBENZONITRILE;Benzonitrile, 2-bromo-5-methoxy-;2-BroMo-5-Methoxybenzonitrile 97%;4-Bromo-3-cyanoanisole, 6-Bromo-m-anisonitrile
- CBNumber
- CB11484530
- Molecular Formula
- C8H6BrNO
- Formula Weight
- 212.04
- MOL File
- 138642-47-4.mol
2-Bromo-5-methoxybenzonitrile Property
- Melting point:
- 99-102 °C
- Boiling point:
- 292.8±30.0 °C(Predicted)
- Density
- 1.56±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- form
- solid
- color
- peachy
- CAS DataBase Reference
- 138642-47-4
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H312Harmful in contact with skin
H315Causes skin irritation
H319Causes serious eye irritation
H331Toxic if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- 701149
- Product name
- 2-Bromo-5-methoxybenzonitrile
- Purity
- 97%
- Packaging
- 1g
- Price
- $37.8
- Updated
- 2021/12/16
- Product number
- 701149
- Product name
- 2-Bromo-5-methoxybenzonitrile
- Purity
- 97%
- Packaging
- 5g
- Price
- $130
- Updated
- 2021/12/16
- Product number
- H50608
- Product name
- 2-Bromo-5-methoxybenzonitrile, 98%
- Packaging
- 250mg
- Price
- $56.65
- Updated
- 2024/03/01
- Product number
- H50608
- Product name
- 2-Bromo-5-methoxybenzonitrile, 98%
- Packaging
- 1g
- Price
- $171
- Updated
- 2021/12/16
- Product number
- B696600
- Product name
- 2-Bromo-5-methoxybenzonitrile
- Packaging
- 1g
- Price
- $75
- Updated
- 2021/12/16
2-Bromo-5-methoxybenzonitrile Chemical Properties,Usage,Production
Uses
2-Bromo-5-methoxybenzonitrile (10.0 g, 47.2 mmol) was dissolved in dry tetrahydrofuran (100 mL) in a flame-dried flask and cooled in an ice bath. A solution of borane in tetrahydrofuran (75 mL, 75 mmol, 1.0 M) was added dropwise over 30 minutes. The reaction mixture was stirred overnight at rt, then quenched slowly with ice water and Na2CO3 (saturated aqueous solution). After removing THF, the residue was extracted with large amounts of EtOAc three times. The combined organic layers were washed with water, dried, and concentrated to give the crude, which was purified by silica gel column chromatography to give 1-(2-Bromo-5-methoxyphenyl)methanamine as a white powder (3.65 g, 36%).
2-Bromo-5-methoxybenzonitrile Preparation Products And Raw materials
Raw materials
Preparation Products
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