ChemicalBook > CAS DataBase List > BOC-GLY-OSU

BOC-GLY-OSU

Product Name
BOC-GLY-OSU
CAS No.
3392-07-2
Chemical Name
BOC-GLY-OSU
Synonyms
BOC-GLY-OSU;Boc-L-Gly-OSu;BOC-GLYCINE-OSU;BOC-GLY-OSU USP/EP/BP;BOC-GLY-OSU;BOC-GLY-OSU;Boc-Gly-OSu >=99.0% (T);N-Boc-glycine N-succinimidyl ester;BOC-GLYCINE-HYDROXYSUCCINIMIDESTER;BOC-GLYCINE HYDROXYSUCCINIMIDE ESTER;Boc glycine-N-hydroxysccinimide ester
CBNumber
CB1233050
Molecular Formula
C11H16N2O6
Formula Weight
272.25
MOL File
3392-07-2.mol
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BOC-GLY-OSU Property

Melting point:
165-167 °C
Density 
1.31±0.1 g/cm3(Predicted)
storage temp. 
-20°C
solubility 
Soluble in Chloroform,Dichloromethane,Ethyl Acetate,DMSO,Acetone,etc.
pka
10.51±0.46(Predicted)
form 
Powder
color 
White
Sensitive 
Hygroscopic
BRN 
1549242
CAS DataBase Reference
3392-07-2(CAS DataBase Reference)
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Safety

Safety Statements 
22-24/25
WGK Germany 
3
3-10-21
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
15423
Product name
Boc-Gly-OSu
Purity
≥99.0% (T)
Packaging
5g
Price
$148
Updated
2025/07/31
Sigma-Aldrich
Product number
15423
Product name
Boc-Gly-OSu
Purity
≥99.0% (T)
Packaging
25g
Price
$537
Updated
2025/07/31
TRC
Product number
B656123
Product name
Boc-Gly-OSu
Packaging
2.5g
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB47806
Product name
Boc-glycine N-hydroxysuccinimide ester
Packaging
50g
Price
$342
Updated
2021/12/16
Activate Scientific
Product number
AS112706
Product name
Boc-Gly-OSu
Purity
97%
Packaging
100g
Price
$383
Updated
2021/12/16
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BOC-GLY-OSU Chemical Properties,Usage,Production

Chemical Properties

White to off-white powder

Uses

peptide synthesis

reaction suitability

reaction type: Boc solid-phase peptide synthesis

Synthesis

4530-20-5

6066-82-6

3392-07-2

Step 2: Synthesis of 2,5-dioxopyrrolidin-1-yl 2-(tert-butoxycarbonylamino) acetate. N-Boc-glycine (7.31 g, 41.7 mmol) was dissolved in 100 mL of dichloromethane (DCM) and the solution was cooled to 15 °C. Subsequently, N-hydroxysuccinimide (5.28 g, 45.9 mmol) was added to the cooled solution. Under vigorous stirring, N,N'-dicyclohexylcarbodiimide (9.47 g, 45.9 mmol) was added to the formed suspension. The reaction mixture transformed into a cloudy white suspension within seconds. The reaction mixture was gradually warmed to room temperature and stirring was continued for 1 hour. Upon completion of the reaction, the insoluble by-products were removed by filtration through diatomaceous earth, the filtrate was washed with 50 mL of saturated sodium bicarbonate solution, dried over anhydrous sodium sulfate, and finally concentrated under vacuum to give the product as a white crystalline powder. Yield: 7.02 g, yield 61.8%. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 1.38 (s, 9H), 2.80 (s, 4H), 4.07 (d, J = 6 Hz, 2H), 7.43 (br s, 1H). Mass spectrum (ESI) m/z 567.2 [2M + Na]+.

References

[1] Chemistry - A European Journal, 2016, vol. 22, # 52, p. 18865 - 18872
[2] Journal of the Chemical Society - Perkin Transactions 1, 1998, # 15, p. 2443 - 2449
[3] Chemical communications (Cambridge, England), 2003, # 23, p. 2870 - 2871
[4] ACS Medicinal Chemistry Letters, 2013, vol. 4, # 4, p. 402 - 407
[5] Helvetica Chimica Acta, 2004, vol. 87, # 5, p. 1077 - 1089

BOC-GLY-OSU Preparation Products And Raw materials

Raw materials

Preparation Products

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BOC-GLY-OSU Suppliers

ChemPep, Inc.
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View Lastest Price from BOC-GLY-OSU manufacturers

Sichuan HongRi Pharma-Tech Co.,Ltd
Product
Boc-Gly-OSu 3392-07-2
Price
US $0.00-0.00/kg
Min. Order
1kg
Purity
95%
Supply Ability
1T+
Release date
2024-02-28
Zhuozhou Wenxi import and Export Co., Ltd
Product
BOC-GLY-OSU 3392-07-2
Price
US $15.00-10.00/KG
Min. Order
1KG
Purity
99%+ HPLC
Supply Ability
Monthly supply of 1 ton
Release date
2021-08-11
Sichuan Jiaying Lai Technology Co.,LTD
Product
Boc-Gly-OSu 3392-07-2
Price
US $1.00/g
Min. Order
1g
Purity
98%
Supply Ability
100KG
Release date
2019-07-21

3392-07-2, BOC-GLY-OSURelated Search:


  • tert-butylN-{2-[(2,5-dioxopyrrolidin-1-yl)oxy]-2-oxoethyl}carbaMate
  • N-Boc-glycine N-hydroxysucciniMide ester, 98%
  • 2,5-Dioxopyrrolidin-1-yl 2-((tert-butoxycarbonyl)aMino)acetate
  • Boc-Gly-OSu >=99.0% (T)
  • BOC-GLY-OSU;BOC-GLY-OSU
  • Boc-glycineN-hydroxysuccinimide ester≥ 97% (HPLC)
  • N-Boc-glycine N-succinimidyl ester
  • N-ALPHA-T-BOC-GLYCINE N-HYDROXYSUCCINIMIDE ESTER
  • BOC-GLY-OSU
  • BOC-GLYCINE 4-HYDROXYSUCCINIMIDE ESTER
  • BOC-GLYCINE HYDROXYSUCCINIMIDE ESTER
  • BOC-GLYCINE N-HYDROXYSUCCINIMIDE ESTER
  • BOC-GLYCINE-OSU
  • (2,5-dioxopyrrolidin-1-yl) 2-[(2-methylpropan-2-yl)oxycarbonylamino]acetate
  • (2,5-dioxopyrrolidin-1-yl) 2-[(2-methylpropan-2-yl)oxycarbonylamino]ethanoate
  • 2-(tert-butoxycarbonylamino)acetic acid succinimido ester
  • tert-butyl [2-[(2,5-dioxo-1-pyrrolidinyl)oxy]-2-oxoethyl]carbamate
  • Boc-L-Glycine 4-Hydroxysuccinimide Ester
  • N-alpha-t-Butyloxycarbonyl-glycine succinimidyl ester
  • BOC-GLYCINE-HYDROXYSUCCINIMIDESTER
  • BOC-L-GLYCINEN-HYDROXYSUCCINIMIDEESTER
  • [(tert-Butoxycarbonyl)amino]acetic acid succinimidyl ester
  • [2-[(2,5-Dioxo-1-pyrrolidinyl)oxy]-2-oxoethyl]carbamic acid 1,1-dimethylethyl ester
  • N-(tert-Butoxycarbonyl)glycine succinimidyl ester
  • N-(tert-Butyloxycarbonyl)glycine 2,5-dioxo-1-pyrrolidinyl ester
  • N-[[N-(tert-Butoxycarbonyl)glycyl]oxy]succinimide
  • 2,5-Dioxopyrrolidin-1-yl N-(tert-butoxycarbonyl)glycinate
  • N-(tert-Butyloxycarbonyl)glycine N-hydroxysuccinimide ester
  • BOC-GLY-OSU USP/EP/BP
  • 2,5-Dioxopyrrolidin-1-yl (tert-butoxycarbonyl)glycinate
  • Boc-L-Gly-OSu
  • Boc glycine-N-hydroxysccinimide ester
  • 3392-07-2
  • 545127
  • Amino Acid Derivatives
  • Specialty Synthesis
  • Peptide Synthesis
  • Amino Acid Derivatives
  • Boc-Amino Acids and Derivative
  • Boc-Amino acid series