ChemicalBook > CAS DataBase List > 1,3,5-TRIIODOBENZENE

1,3,5-TRIIODOBENZENE

Product Name
1,3,5-TRIIODOBENZENE
CAS No.
626-44-8
Chemical Name
1,3,5-TRIIODOBENZENE
Synonyms
5-Triiodobenzene;2,4,6-Triiodobenzene;1,3,5-TRIIODOBENZENE;Benzene, 1,3,5-triiodo-;1,3,5-TRIIODOBENZENE, 95 %
CBNumber
CB1294914
Molecular Formula
C6H3I3
Formula Weight
455.8
MOL File
626-44-8.mol
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1,3,5-TRIIODOBENZENE Property

Melting point:
184.2°C
Boiling point:
381.91°C (rough estimate)
Density 
2.8493 (rough estimate)
refractive index 
1.8070 (estimate)
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Methanol (Slightly, Heated)
form 
Solid
color 
White to Off-White
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific
Product number
097888
Product name
1,3,5-Triiodobenzene
Purity
95+%
Packaging
250mg
Price
$59
Updated
2021/12/16
AK Scientific
Product number
J54628
Product name
1,3,5-Triiodobenzene
Packaging
250mg
Price
$60
Updated
2021/12/16
Matrix Scientific
Product number
097888
Product name
1,3,5-Triiodobenzene
Purity
95+%
Packaging
500mg
Price
$91
Updated
2021/12/16
Ark Pharm
Product number
AK101088
Product name
1,3,5-Triiodobenzene
Purity
98%
Packaging
10g
Price
$572
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0295342
Product name
1,3,5-TRIIODOBENZENE
Purity
98.00%
Packaging
1G
Price
$1270.5
Updated
2021/12/16
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1,3,5-TRIIODOBENZENE Chemical Properties,Usage,Production

Uses

1,3,5-Triiodobenzene is used in the synthesis of conjugated microporous polymers through cationic cyclization polymerization. It also can be used in optical materials.

Synthesis

1,3,5-Triiodobenzene was synthesized by reacting 2,4,6-triiodoaniline with NaNO2 in the presence of copper(I) oxide.
Experimental procedure: Finely ground NaNO2 (1.95 g, 0.028 mol) was slowly added with stirring to sulfuric acid (3.5 mL). Then a solution of 2,4,6-triiodoaniline(2.90 g, 6.16 mmol) in glacial AcOH (130 mL) was added dropwise with stirring and cooling at such a rate that the temperature of the reaction mixture was kept below 20 °C. Following addition of the amine, the reaction mixture was stirred at ≈20 °C for about 30 min. The resulting solution of the diazonium salt was added dropwise to a suspension of copper(I) oxide (2.52 g) in dry ethanol (70 mL) with vigorous stirring over 15 min. The reaction mixture was brought to boiling and stirred for 30 min until elimination of nitrogen ceased. Then the mixture was cooled, kept for one day, poured into ice water (300 mL), and extracted with benzene (3×50 mL). The benzene extracts were dried with anhydrous Na2SO4 and the solvent was distilled off in vacuo. The residue was repeatedly recrystallized from benzene. The yield was 2.01 g (84%), m.p. 182 °C (cf. lit. data11: m.p. 183 °C). 1H NMR (CDCl3), δ: 8.02 (s, 3 H, CH). 13C NMR (CDCl3), δ: 79; 128.

1,3,5-TRIIODOBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1,3,5-TRIIODOBENZENE manufacturers

Henan Fengda Chemical Co., Ltd
Product
1,3,5-TRIIODOBENZENE 626-44-8
Price
US $101.00-1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-28

626-44-8, 1,3,5-TRIIODOBENZENERelated Search:

Iohexol sodium metrizoate MEGLUMINE DIATRIZOATE Metrizamide ALPHA-ETHYL-3-HYDROXY-2,4,6-TRIIODOHYDROCINNAMIC ACID sodium acetrizoate IODIPAMIDE 2,4,6-Triiodophenol 3-HYDROXY-2,4,6-TRIIODOBENZOIC ACID 3-Amino-2,4,6-triiodobenzoic acid Diatrizoate sodium DIATRIZOIC ACID Acetrizoic acid Iopanoic acid periodobenzene Bunamiodyl disodium 3,3'-[(1,6-dioxo-1,6-hexanediyl)diimino]bis[2,4,6-triiodobenzoate] 2-(2-bromoethoxy)-1,3,5-triiodobenzene

  • Benzene, 1,3,5-triiodo-
  • 1,3,5-TRIIODOBENZENE
  • 2,4,6-Triiodobenzene
  • 1,3,5-TRIIODOBENZENE, 95 %
  • 5-Triiodobenzene
  • 626-44-8
  • C6H3I3