N-(Hydroxymethyl)phthalimide
- Product Name
- N-(Hydroxymethyl)phthalimide
- CAS No.
- 118-29-6
- Chemical Name
- N-(Hydroxymethyl)phthalimide
- Synonyms
- AURORA KA-454;N-(HydroxymethyL;AKOS BBS-00004724;PHTHALIMIDOMETHANOL;IFLAB-BB F0777-0575;N-(Hydroxymethyl)ph;oxymethylphthalimide;Phthalimidylmethanol;N-Methylolphthalimide;Oxymethyl phthalimide
- CBNumber
- CB1392676
- Molecular Formula
- C9H7NO3
- Formula Weight
- 177.16
- MOL File
- 118-29-6.mol
N-(Hydroxymethyl)phthalimide Property
- Melting point:
- 147-149 °C (lit.)
- Boiling point:
- 309.06°C (rough estimate)
- Density
- 1.3312 (rough estimate)
- refractive index
- 1.5200 (estimate)
- storage temp.
- Store below +30°C.
- form
- Fine Crystalline Powder
- pka
- 13.17±0.10(Predicted)
- color
- White
- BRN
- 140946
- InChIKey
- MNSGOOCAMMSKGI-UHFFFAOYSA-N
- CAS DataBase Reference
- 118-29-6(CAS DataBase Reference)
- NIST Chemistry Reference
- 1H-isoindole-1,3(2h)-dione, 2-(hydroxymethyl)-(118-29-6)
- EPA Substance Registry System
- N-(Hydroxymethyl)phthalimide (118-29-6)
Safety
- Safety Statements
- 22-24/25
- WGK Germany
- 3
- RTECS
- TI5270000
- TSCA
- Yes
- HS Code
- 29251995
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P405Store locked up.
N-Bromosuccinimide Price
- Product number
- H41803
- Product name
- N-(Hydroxymethyl)phthalimide
- Purity
- 97%
- Packaging
- 100g
- Price
- $219
- Updated
- 2024/03/01
- Product number
- 8.14422
- Product name
- N-(Hydroxymethyl)-phthalimide
- Purity
- for synthesis
- Packaging
- 100g
- Price
- $68.9
- Updated
- 2024/03/01
- Product number
- H0648
- Product name
- N-Hydroxymethylphthalimide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 25g
- Price
- $35
- Updated
- 2024/03/01
- Product number
- H0648
- Product name
- N-Hydroxymethylphthalimide
- Purity
- >98.0%(HPLC)(N)
- Packaging
- 250g
- Price
- $150
- Updated
- 2024/03/01
- Product number
- B21292
- Product name
- N-(Hydroxymethyl)phthalimide, 97%
- Packaging
- 25g
- Price
- $24.65
- Updated
- 2024/03/01
N-(Hydroxymethyl)phthalimide Chemical Properties,Usage,Production
Chemical Properties
white crystalline powder
Uses
N-(Hydroxymethyl)phthalimide is used as a reactant in the synthesis of 5-[(3-aralkyl amido/imidoalkyl)phenyl]-1,2,4-triazolo[3,4-b]-1,3,4-thiadiazines as antiviral agents.
Uses
For amidomethylation of aromatics in triflic acid.
Preparation
To a flask equipped with a mechanical stirrer and condenser is added 511 gm (3.47 moles) of phthalimide, 260 ml of 40% formalin (3.47 moles), and 1750 ml of water. The mixture is refluxed for about 5-10 min or until a clear solution results (if any insoluble material remains, it is first filtered). Then the mixture is cooled for several hours. The resulting product is filtered with suction, washed with cold water, and air-dried to afford 594 gm (96%), m.p. 137-141°C.
NOTE: The product should not be oven-dried since it decomposes with the loss of formaldehyde. Recrystallization of the product from ethanol affords 94% recovery of the original material with the same melting point range.
Definition
ChEBI: A primary alcohol comprising phthalimide carrying an N-hydroxymethyl substituent.
Synthesis Reference(s)
Journal of the American Chemical Society, 77, p. 1913, 1955 DOI: 10.1021/ja01612a068
N-(Hydroxymethyl)phthalimide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from N-(Hydroxymethyl)phthalimide manufacturers
- Product
- N-(Hydroxymethyl)phthalimide 118-29-6
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000kg
- Release date
- 2024-04-16
- Product
- N-(Hydroxymethyl)phthalimide 118-29-6
- Price
- US $90.00-900.00/kg
- Min. Order
- 10kg
- Purity
- 0.99
- Supply Ability
- 20tons
- Release date
- 2023-10-31
- Product
- N-(Hydroxymethyl)phthalimide 118-29-6
- Price
- US $0.00/Kg/Bag
- Min. Order
- 1KG
- Purity
- 99%min
- Supply Ability
- 10000kg
- Release date
- 2021-09-14