TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER

Product Name: TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER
CAS No.: 2434-02-8
Chemical Name: TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER
Synonyms: ethyl 2-(oxolan-2-yl)acetate;ETHYL TETRAHYDROFURAN-2-ACETATE;Tetrahydrofuranaceticacidethylester;Ethyl 2-(tetrahydrofuran-2-yl)acetate;TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER
CBNumber: CB1483073
Molecular Formula: C8H14O3
Formula Weight: 158.2
MOL File: 2434-02-8.mol

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TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER Property

Boiling point:: 98 °C / 13mmHg
Density: 1.03
refractive index: 1.4350-1.4390
storage temp.: 2-8°C
form: clear liquid
color: Colorless to Almost colorless
CAS DataBase Reference: 2434-02-8

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Safety

HS Code: 2932190090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P370+P378In case of fire: Use … for extinction.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: T0957
Product name: Ethyl Tetrahydrofuran-2-acetate
Purity: >98.0%(GC)
Packaging: 5mL
Price: $210
Updated: 2025/07/31

TCI Chemical

Product number: T0957
Product name: Ethyl Tetrahydrofuran-2-acetate
Purity: >98.0%(GC)
Packaging: 25mL
Price: $736
Updated: 2025/07/31

TRC

Product number: T293535
Product name: Tetrahydro-2-furanaceticAcidEthylEster
Packaging: 10g
Price: $1320
Updated: 2021/12/16

Apolloscientific

Product number: OR939909
Product name: Tetrahydrofuran-2-aceticacidethylester
Purity: 95%
Packaging: 1g
Price: $125
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2H23-1-0X
Product name: Tetrahydrofuran-2-aceticacidethylester
Purity: 95%
Packaging: 1g
Price: $200
Updated: 2021/12/16

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TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER Chemical Properties,Usage,Production

Uses

Tetrahydro-2-furanacetic Acid Ethyl Ester is used in organic reactions for the opening of cyclic ethers using dimethylboron bromide.

Synthesis

109-99-9

623-73-4

2434-02-8

General procedure for the synthesis of ethyl tetrahydrofuran-2-acetate from tetrahydrofuran and ethyl diazoacetate: first, methyl phenyl diacetate was prepared by the reaction of methyl phenylacetate with p-acetamidobenzenesulfonyl azide. The dried non-homogeneous catalyst (containing 0.02 mmol Cu) was suspended in anhydrous tetrahydrofuran (10 mL containing 100 mg of n-decane as internal standard) and heated to reflux under inert atmosphere. Anhydrous tetrahydrofuran (10 mL) solution of diazo compounds (1 mmol) was slowly added over a period of 2 hours using a syringe pump. After the addition was completed, the reaction mixture was continued to be stirred under reflux conditions for 30 min. Subsequently, the catalyst was removed by filtration and washed with tetrahydrofuran (5 mL). Yield and stereoselectivity were determined by gas chromatography (GC). After addition of diazo compounds and heating at reflux for 2 h, the presence of active copper substances in solution was detected by analytical tests. After drying the catalyst under vacuum, it can be reused under the same conditions. Enantioselectivity was determined by high performance liquid chromatography (HPLC) when the reaction was carried out in the presence of chiral ligands.

References

[1] Journal of the American Chemical Society, 2002, vol. 124, # 6, p. 896 - 897
[2] Inorganic Chemistry, 2015, vol. 54, # 23, p. 11043 - 11045
[3] Dalton Transactions, 2009, # 2, p. 375 - 382
[4] Journal of Catalysis, 2011, vol. 281, # 2, p. 273 - 278
[5] Chemical Science, 2015, vol. 6, # 2, p. 1510 - 1515

TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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2434-02-8, TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTERRelated Search:

TETRAHYDROFURAN-3-CARBOXALDEHYDE 98 Tetrahydrofuran Cantharidin EXO-7-OXABICYCLO[2.2.1]HEPTANE-2,3-DICARBOXYLIC ANHYDRIDE TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER tetranactin trinactin NSC63925 IKD-8344 NONACTIN 1,2-DIMETHYL-4,10-DIOXATRICYCLO[5.2.1.0(2,6)]DECAN-3-ONE 1-(2-METHYL-3-OXO-4,10-DIOXATRICYCLO[5.2.1.0(2,6)]DEC-1-YL)PROPANE-1,2-DIONE 1,6-DIMETHYL-4,10-DIOXATRICYCLO[5.2.1.0(2,6)]DECANE-3,5-DIONE 5-endo-(Ethoxycarbonyl)endothall anhydride 1,2-DIMETHYL-4,10-DIOXATRICYCLO[5.2.1.0(2,6)]DECANE-3,5-DIONE 5,6-DIBROMO-4-METHYLHEXAHYDRO-4,7-EPOXY-2-BENZOFURAN-1,3-DIONE SPECS AG-650/41069451 exo-cis-7-Oxabicyclo(2.2.1)heptane-2,3-dicarboxylic acid 3,4-methylene dioxybenzyl ester

TETRAHYDROFURAN-2-ACETIC ACID ETHYL ESTER

Ethyl 2-(tetrahydrofuran-2-yl)acetate

ETHYL TETRAHYDROFURAN-2-ACETATE

Tetrahydrofuranaceticacidethylester

ethyl 2-(oxolan-2-yl)acetate

2434-02-8

2434-02-08