1-Acetylpiperazine

Product Name: 1-Acetylpiperazine
CAS No.: 13889-98-0
Chemical Name: 1-Acetylpiperazine
Synonyms: N-ACETYLPIPERAZINE;1-AcetyL;AKOS BB-5737;acetylpiperazine;N-aetylpiperazine;N-ACETY PIPERAZINE;1-ACETYLPIPERAZINE;n-acetyl ptperazine;1-Piperazinoethanone;Olaparib Impurity 61
CBNumber: CB1717961
Molecular Formula: C6H12N2O
Formula Weight: 128.17
MOL File: 13889-98-0.mol

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1-Acetylpiperazine Property

Melting point:: 31-34 °C (lit.)
Boiling point:: 127 °C
Density: 1.0754 (rough estimate)
refractive index: 1.4880 (estimate)
Flash point:: >230 °F
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: methanol: soluble1g/10 mL, clear, colorless to faintly greenish-yellow
pka: 8.50±0.10(Predicted)
form: Liquid After Melting
color: Clear light yellow
Water Solubility: Soluble in water 210 g/L (20°C).
Sensitive: Hygroscopic
BRN: 112220
CAS DataBase Reference: 13889-98-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
Risk Statements: 36/38-36/37/38
Safety Statements: 26-36-37/39
WGK Germany: 3
F: 3-10-34
Hazard Note: Irritant
HS Code: 29339900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H334May cause allergy or asthma symptoms or breathing difficulties if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P342+P311IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 359513
Product name: 1-Acetylpiperazine
Purity: 99%
Packaging: 5g
Price: $57.9
Updated: 2024/03/01

Sigma-Aldrich

Product number: 359513
Product name: 1-Acetylpiperazine
Purity: 99%
Packaging: 25g
Price: $162
Updated: 2024/03/01

TCI Chemical

Product number: A1399
Product name: 1-Acetylpiperazine
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $16
Updated: 2024/03/01

TCI Chemical

Product number: A1399
Product name: 1-Acetylpiperazine
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $38
Updated: 2024/03/01

Alfa Aesar

Product number: B20200
Product name: 1-Acetylpiperazine, 99%
Packaging: 5g
Price: $41.65
Updated: 2024/03/01

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1-Acetylpiperazine Chemical Properties,Usage,Production

Chemical Properties

clear light yellow liquid after melting

Uses

1-Acetylpiperazine may be used in the synthesis of series of 7-alkoxyl substituted indolizinoquinoline-5,12-dione derivatives and 2-substituted-N-(naphth-1-ylmethyl)-pyrimidin-4-amines and 2-substituted-N-benzhydrylpyrimidin-4-amines.

Definition

ChEBI: 1-Acetylpiperazine is a member of phytanoyl-CoAs.

General Description

Infrared and Raman spectra of 1-acetylpiperazine have been recorded in the region of 4000-40cm^-1.

Purification Methods

Purify 1-acetylpiperazine by recrystallisation from 40% aqueous EtOH or from EtOH/Et2O. It is an irritant, and is hygroscopic. The hydrochloride has m 191o (from EtOH), and the tosylate salt has m 148-149o (from EtOH/EtOAc, 1:16). The free base, however, cannot be isolated by basifying the tosylate salt and extraction with CH2Cl2. [Jacobi Chem Ber 66 113 1933, Mosher et al. J Am Chem Soc 75 4949 1953, Hall J Am Chem Soc 78 2570 1956, Beilstein 23 IV 1786.]

1-Acetylpiperazine Preparation Products And Raw materials

Raw materials

Silica gel PIPERAZINE HEXAHYDRATE Acetic anhydride Sodium sulfate Acetyl chloride Potassium carbonate Triethylamine Chloroform Piperazine Tetrahydrofuran Dichloromethane Acetic acid Methanol Sodium hydroxide Magnesium sulfate PETROLEUM ETHER

Preparation Products

(4-ACETYL-PIPERAZIN-1-YL)-ACETIC ACID

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1-Acetylpiperazine Suppliers

Americas 1 Belgium 3 China 222 Europe 4 France 1 Germany 8 India 32 Japan 9 Slovakia 1 South Korea 1 Switzerland 2 United Kingdom 19 United States 49 Global 352

New Energy Chemicals

Tel: 0515-82159088 13770142076
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Creasyn Finechem(Tianjin) Co., Ltd.

Tel: 022-022-83946278 13820372920
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Shanghai Biobond Pharmaceutical Co.,Ltd.

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Email: sales@sh-biobond.cn
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J & K SCIENTIFIC LTD.

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INTATRADE GmbH

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future industrial shanghai co., ltd

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Alfa Aesar

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TAIYUAN RHF CO.,LTD.

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View Lastest Price from 1-Acetylpiperazine manufacturers

Hebei Mojin Biotechnology Co., Ltd

Product: 1-Acetylpiperazine 13889-98-0
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-08-16

Shaanxi Didu New Materials Co. Ltd

Product: 1-Acetylpiperazine 13889-98-0
Price: US $1.50/g
Min. Order: 1g
Purity: 99.0% Min
Supply Ability: 100 Tons
Release date: 2022-09-20

Hebei Guanlang Biotechnology Co., Ltd.

Product: 1-Acetylpiperazine 13889-98-0
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5tons
Release date: 2021-11-09

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1-acetylpiperazine 13889-98-0

1-ACETYLPIPERAZINE For Synthesis

13889-98-0

13889-88-0

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Piperidines, Piperidones, Piperazines