Methyl 5-bromo-2-chloropyridine-3-carboxylate

Crystal data

Product Name: Methyl 5-bromo-2-chloropyridine-3-carboxylate
CAS No.: 78686-79-0
Chemical Name: Methyl 5-bromo-2-chloropyridine-3-carboxylate
Synonyms: METHYL 5-BROMO-2-CHLORONICOTINATE;methyl 2-chloro-5-bromonicotinate;Methyl5-Bromo-2-chloronicotinate>Methyl 5-bromo-2-chloronicotinate 98%;Methyl 5-broMo-2-chloronicotinate, 95+%;2-Chloro-5-bromonicotinic acid methyl ester;5-BROMO-2-CHLORONICOTINIC ACID METHYL ESTER;Methyl 5-bromo-2-chloropyridine-3-carboxlate;METHYL 5-BROMO-2-CHLOROPYRIDINE-3-CARBOXYLATE;methyl 5-bromo-2-chloro-3-pyridinecarboxylate
CBNumber: CB2150790
Molecular Formula: C7H5BrClNO2
Formula Weight: 250.48
MOL File: 78686-79-0.mol

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Methyl 5-bromo-2-chloropyridine-3-carboxylate Property

Melting point:: 50-52°C
Boiling point:: 275.6±35.0 °C(Predicted)
Density: 1.684±0.06 g/cm3(Predicted)
Flash point:: >110 °C
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: soluble in Methanol
pka: -3.78±0.10(Predicted)
form: Solid
color: White to Light yellow to Light orange
Sensitive: Light, Air & Moisture Sensitive
InChIKey: MOMQDEDQGJAKII-UHFFFAOYSA-N
CAS DataBase Reference: 78686-79-0(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
WGK Germany: 3
HazardClass: IRRITANT
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P330Rinse mouth.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 764477
Product name: Methyl 5-bromo-2-chloropyridine-3-carboxylate
Purity: 97%
Packaging: 1g
Price: $62.7
Updated: 2023/06/20

TCI Chemical

Product number: M2513
Product name: Methyl 5-Bromo-2-chloronicotinate
Purity: >98.0%(GC)
Packaging: 5g
Price: $64
Updated: 2024/03/01

Alfa Aesar

Product number: H64791
Product name: Methyl 5-bromo-2-chloronicotinate, 98%
Packaging: 25g
Price: $98.65
Updated: 2024/03/01

Alfa Aesar

Product number: H64791
Product name: Methyl 5-bromo-2-chloronicotinate, 98%
Packaging: 5g
Price: $24
Updated: 2021/12/16

Alfa Aesar

Product number: H64791
Product name: Methyl 5-bromo-2-chloronicotinate, 98%
Packaging: 100g
Price: $347.65
Updated: 2024/03/01

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Methyl 5-bromo-2-chloropyridine-3-carboxylate Chemical Properties,Usage,Production

Crystal data

The crystal structure data of Methyl 5-bromo-2-chloropyridine-3-carboxylate is shown below:

Synthesis

Methyl 5-bromo-2-chloropyridine-3-carboxylate is prepared by the reaction of 5-Bromo-2-chloronicotinic acid and Methanol. The specific synthesis steps are as follows:
To 0.5 L flask charged with 5-Bromo-2-chloronicotinic acid (25.0 g, 106.4 mmol) in MeOH (250 mL) was added H2SO4(5 mL). The mixture was heated to 60° C., stirred for 1.5 day. LC-MS indicated full conversion of starting material at this time. The reaction was cooled to RT and the volatile components removed in vacuo. The crude residue was dissolved in EtOAc (300 mL), quenched with sat. aqueous Na(HCO3)2(200 mL). The organic layer was separated, washed with brine, dried over MgSO4and concentrated to afford the compound, methyl-5-bromo-2-chloronicotinate, as a while solid (quantitative yield). LC-MS (M+H)=250.1.

Methyl 5-bromo-2-chloropyridine-3-carboxylate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Methyl 5-bromo-2-chloropyridine-3-carboxylate manufacturers

Henan Bao Enluo International TradeCo.，LTD

Product: Methyl 5-bromo-2-chloropyridine-3-carboxylate 78686-79-0
Price: US $10.00/kg
Min. Order: 1kg
Purity: 99.99%
Supply Ability: 50000tons
Release date: 2023-08-09

Dideu Industries Group Limited

Product: Methyl 5-bromo-2-chloropyridine-3-carboxylate 78686-79-0
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-10-25

Zhuozhou Wenxi import and Export Co., Ltd

Product: Methyl 5-bromo-2-chloropyridine-3-carboxylate 78686-79-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-06-27

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Methyl 5-bromo-2-chloropyridine-3-carboxylate ISO 9001：2015 REACH

78686-79-0

C7H5BrClNO2

Esters

Pyridine

blocks

Bromides

Carboxes

Pyridines