N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

Product Name: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
CAS No.: 2842-44-6
Chemical Name: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
Synonyms: FirstCure MHPT;2-(N-Methyl-p-toluidino);HYDROXYETHYL METHYLTOLUIDINE;Hydroxyethyl methyltolylamine;2-(N-methyl-p-toluidino)ethanol;2-(Methyl(p-tolyl)aMino)ethanol;N-methyl-hydroxyethyl-p-toluidine;2-(N-Methyl-N-4-tolylamino)ethanol;2-(N-methyl-N-p-tolylamino)ethanol;2-(Methyl(p-tolyl)amino)ethan-1-ol
CBNumber: CB2158428
Molecular Formula: C10H15NO
Formula Weight: 165.23
MOL File: 2842-44-6.mol

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Property

Boiling point:: 152-154 °C(Press: 10 Torr)
Density: 1.047±0.06 g/cm3(Predicted)
vapor pressure: 0.062-0.115Pa at 20-25℃
storage temp.: Sealed in dry,Room Temperature
form: Liquid:viscous
pka: 14.69±0.10(Predicted)
InChI: InChI=1S/C10H15NO/c1-9-3-5-10(6-4-9)11(2)7-8-12/h3-6,12H,7-8H2,1-2H3
InChIKey: HXCWOOAEAHVMBJ-UHFFFAOYSA-N
SMILES: C(O)CN(C)C1=CC=C(C)C=C1
LogP: 2.2 at 25℃ and pH6
EPA Substance Registry System: Ethanol, 2-[methyl(4-methylphenyl)amino]- (2842-44-6)

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Safety

HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0290557
Product name: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE
Purity: 98.00%
Packaging: 5MG
Price: $502.35
Updated: 2021/12/16

Labseeker

Product number: SC-91423
Product name: 2-(Methyl(p-tolyl)amino)ethanol
Purity: 95
Packaging: 1kg
Price: $700
Updated: 2021/12/16

Crysdot

Product number: CD12088559
Product name: 2-(Methyl(p-tolyl)amino)ethanol
Purity: 95+%
Packaging: 100g
Price: $50
Updated: 2021/12/16

Crysdot

Product number: CD12088559
Product name: 2-(Methyl(p-tolyl)amino)ethanol
Purity: 95+%
Packaging: 500g
Price: $150
Updated: 2021/12/16

Chemenu

Product number: CM274824
Product name: 2-(Methyl(p-tolyl)amino)ethanol
Purity: 95%
Packaging: 1000g
Price: $234
Updated: 2021/12/16

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Chemical Properties,Usage,Production

Uses

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE is an amine organic compound, which can be used as intermediate in organic synthesis.

Synthesis

Add reactant (0.2 mmol, 1.0 equiv), THF (2.0 mL) and CH2Br2 (0.6 mmol, 3.0 equiv) to a flame-dried 10 mL Schlenk tube in a glove box. Seal and take out of the glove box. Cool the reaction mixture to -78°C. Add nBuLi (0.56 mmol, 2.8 equiv) dropwise under N2 atmosphere within 3minutes. Stir the reaction at -78°C for 30 minutes and add ZnCl2 (0.1 mL, 0.5equiv, 1.0 M in Et2O). Allow the mixture to warm to room temperature and stir for 1 hour. Cool the mixture to 0°C. Add a premixture of H2O2 (30% in H2O, 0.5 mL) and NaOH (2.0 M, 1.0 mL). Stir the mixture at room temperature for another 1 hour and dilute with water (20 mL). Extract with DCM (30 mL x 2) and dry over Na2SO4. Filter and concentrate under vacuum. Purify the crude product by silica gel flash column chromatography to obtain product. 1H NMR (CDCl3, 500 MHz) δ 7.08 (d, J = 8.4 Hz, 2H), 6.78 (d, J = 8.4 Hz,2H), 3.80 (t, J = 5.6 Hz, 2H), 3.43 (t, J = 5.4 Hz, 2H), 2.93 (s, 3H), 2.28 (s, 3H), 2.01 (brs, 1H). 13C NMR (CDCl3, 125 MHz) δ 148.3, 129.8, 127.1, 114.0, 60.1, 56.2, 39.1, 20.4.
Fig The synthetic method of N-(2-hydroxyethyl)-N-methyl-4-toluidine

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE Suppliers

China 143 Switzerland 1 United States 4 Global 148

Yancheng Green Chemicals Co.,Ltd.

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View Lastest Price from N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10 mt
Release date: 2021-07-30

Hebei Mojin Biotechnology Co., Ltd

Product: N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE 2842-44-6
Price: US $0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 50000KG/month
Release date: 2023-08-29

2842-44-6, N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINERelated Search:

N-(2-Hydroxyethyl)-N-methylaniline N-Methylaniline 4-Nitro-N-methylphthalimide 2,2'-(P-TOLYLIMINO)DIETHANOL Riboflavin 2-[(2-amino-5-methylph2-[(2-amino-5-methylphenoxy)methyl]-6-methoxy-8-aminoquinoline-n,n,n',n'-tetraacetic acid tetrapotassium saltenoxy)methyl]-6-methoxy-8-aminoquinoline-n,n,n FLAVIN ADENINE DINUCLEOTIDE Riboflavin 5'-Monophosphate Sodium Salt 4-MORPHOLINOACETOPHENONE 3-AMINO-4-(4-MORPHOLINO)BENZOTRIFLUORIDE Fura 2-AM Diisopropanol-p-toluidine N-METHYL-P-TOLUIDINE 4'-MORPHOLINOPROPIOPHENONE 1-(4-MORPHOLINO-3-NITROPHENYL)-1-ETHANONE 4-MORPHOLINOBENZOPHENONE INDO 1-AM INDO 1 PENTAPOTASSIUM SALT

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

2-(N-methyl-p-toluidino)ethanol

N-Methyl-N-hydroxyethyl-P-toluidine

N-(2-Hydroxyethyl)-N-methyl-p-toluidine

2-[Methyl(4-methylphenyl)amino]ethanol

2-(N-Methyl-N-4-tolylamino)ethanol

FirstCure MHPT

N-Methyl-N-(2-hydroxyethyl)-p-toluidine

2-(Methyl(p-tolyl)aMino)ethanol

2-(N-methyl-N-p-tolylamino)ethanol

N-(2-HYDROXYETHYL)-N-METHYL-PARA-TOLUIDINE(MPHT)

N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE(MHPT)

Hydroxyethyl methyltolylamine

(5S,8R,9S,10S,13S,14S,17R)-17-ethynyl-3,3-difluoro-10,13-dimethyl-2,4,5,6,7,8,9,11,12,14,15,16-dodecahydro-1H-cyclopenta[a]phenanthren-17-ol

2-(N-Methyl-p-toluidino)

Ethanol, 2-[methyl(4-methylphenyl)amino]-

N-methyl-hydroxyethyl-p-toluidine

HYDROXYETHYL METHYLTOLUIDINE

2842-44-6 N-(2-HYDROXYETHYL)-N-METHYL-4-TOLUIDINE

2-(Methyl(p-tolyl)amino)ethan-1-ol

2842-44-6

42-44-6