(Diacetoxyiodo)benzene

Product Name: (Diacetoxyiodo)benzene
CAS No.: 3240-34-4
Chemical Name: (Diacetoxyiodo)benzene
Synonyms: PhI(OAc)2;BAIB;IODOBENZENE DIACETATE;DAIB;[Bis(acetoxy)iodo]benzene;PIA;PHENYLIODINE DIACETATE;IODOSOBENZENE DIACETATE;Phenyliodoso diacetate;IODOBENZENE I,I-DIACETATE
CBNumber: CB2222138
Molecular Formula: C10H11IO4
Formula Weight: 322.1
MOL File: 3240-34-4.mol

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(Diacetoxyiodo)benzene Property

Melting point:: 161-163 °C (lit.)
Density: 1.6865 (estimate)
refractive index: n/D 1.444
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: INSOLUBLE
form: Solution
color: Clear to cloudy colorless to yellow
Water Solubility: INSOLUBLE
Sensitive: Light Sensitive
BRN: 1879369
Stability:: Light and Moisture sensitive
InChIKey: ZBIKORITPGTTGI-UHFFFAOYSA-N
CAS DataBase Reference: 3240-34-4(CAS DataBase Reference)
NIST Chemistry Reference: Iodobenzene diacetate(3240-34-4)
EPA Substance Registry System: Iodine, bis(acetato-.kappa.O)phenyl- (3240-34-4)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 22-24/25-37/39-26-36/37/39-27
RIDADR: 1479
WGK Germany: 3
RTECS: DA3525000
F: 4.10-8
Hazard Note: Irritant
TSCA: Yes
HazardClass: 6.1(b)
PackingGroup: III
HS Code: 29310095

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 178721
Product name: (Diacetoxyiodo)benzene
Purity: 98%
Packaging: 5g
Price: $25.2
Updated: 2024/03/01

Sigma-Aldrich

Product number: 178721
Product name: (Diacetoxyiodo)benzene
Purity: 98%
Packaging: 25g
Price: $69.4
Updated: 2024/03/01

TCI Chemical

Product number: I0330
Product name: Iodobenzene Diacetate
Purity: >97.0%(T)
Packaging: 10g
Price: $29
Updated: 2024/03/01

TCI Chemical

Product number: I0330
Product name: Iodobenzene Diacetate
Purity: >97.0%(T)
Packaging: 25g
Price: $55
Updated: 2024/03/01

Alfa Aesar

Product number: B24531
Product name: Iodosobenzene diacetate, 98+%
Packaging: 25g
Price: $64.6
Updated: 2024/03/01

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(Diacetoxyiodo)benzene Chemical Properties,Usage,Production

Chemical Properties

white to light yellow crystal powder

Uses

(Diacetoxyiodo)benzene is a hypervalent iodine reagent that is used in conjunction with catalytic amount of sodium azide in acetonitrile, which enables oxidative decarboxylation of 2-aryl carboxylic acid into the corresponding aldehydes, ketones and nitriles.

Application

(Diacetoxyiodo)benzene, an oxidizing agent, has a wide range of applications. (Diacetoxyiodo)benzene, also known as Diacetoxy Iodobenzene, is used in wide range of medicals industrial applications as well as in human and animal nutrition products such as antiseptics and disinfectants, pharmaceutical intermediates, polarizing films for liquid crystal display [LCD] chemicals.

Origin

This reagent was originally prepared by Conrad Willgerod by reacting iodobenzene with a mixture of acetic acid and peracetic acid：
C6H5I + CH3CO3H + CH3CO2H → C6H5I(O2CCH3)2 + H2O

Purification Methods

The purity of diacetoxyiodobenzene can be checked by treatment with H2SO4 then KI and the liberated I2 is estimated with standard thiosulfate. It has been recrystallised from 5M acetic acid and dried overnight in a vacuum desiccator over CaCl2. The surface of the crystals may become slightly yellow but this does not affect its usefulness. [Sharefkin & Saltzman Org Synth Coll Vol V 600 1973, Beilstein 5 IV 693.]

(Diacetoxyiodo)benzene Preparation Products And Raw materials

Raw materials

Iodobenzene Ethyl 2-(Chlorosulfonyl)acetate Acetic anhydride Hydrogen peroxide Acetic acid

Preparation Products

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(Diacetoxyiodo)benzene Suppliers

Americas 1 Austria 1 Belgium 3 Canada 3 China 496 Europe 4 France 2 Germany 12 India 50 Japan 9 Poland 2 Slovakia 1 South Korea 1 Spain 1 Switzerland 4 Ukraine 1 United Kingdom 23 United States 71 Global 685

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View Lastest Price from (Diacetoxyiodo)benzene manufacturers

HEBEI SHENGSUAN CHEMICAL INDUSTRY CO.,LTD

Product: (Diacetoxyiodo)benzene 3240-34-4
Price: US $999.00-800.00/ton
Min. Order: 1ton
Purity: 99%
Supply Ability: 5000
Release date: 2024-08-21

Hebei Zhuanglai Chemical Trading Co Ltd

Product: (Diacetoxyiodo)benzene 3240-34-4
Price: US $10.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 20 ton
Release date: 2024-11-29

Jinan Finer Chemical Co., Ltd

Product: Iodobenzene diacetate 3240-34-4
Price: US $50.00-80.00/kg
Min. Order: 100kg
Purity: 99%
Supply Ability: 200mt
Release date: 2019-03-15

3240-34-4, (Diacetoxyiodo)benzeneRelated Search:

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PHENYLIODINE DIACETATE

PIA

AURORA KA-6690

(DIACETOXYIODO)BENZENE

DIACETOXYIODOSOBENZENE

DAIB

LABOTEST-BB LT00847235

IODOBENZENE I,I-DIACETATE

IODOBENZENE DIACETATE

IODOSOBENZENE DIACETATE

IODOSOBENZENE I,I-DIACETATE

IODINE, BIS(ACETATO-KO)PHENYL

(Diacetoxyiodo)benzene PIDA

IODOSOBENZENE DIACETATE FOR SYNTHESIS

(Diacetoxyiodo)benze

(Diacetoxyiodo)benzene~DIB~Iodobenzene diacetate~Phenyliodine(III) diacetate

iodosylbenzene di(acetate)

BAIB

2-[2-(carboxylatoMethyl)-3-iodophenyl]acetate

Lodobenzene diacetate

Iodobenzene diacetate, 98% 100GR

Iodobenzene diacetate, 98% 25GR

(diacetoxyiodo)-benzen

(dihydroxyiodo)-benzendiacetate

Benzene, (diacetoxyiodo)-

Benzene, iodoso-, diacetate

Bis(acetato)phenyliodine

bis(acetato-o)phenyl-iodin

Iodine, bis(acetato-O)phenyl-

iodoso-benzendiacetate

phenyliodine(iii)diacetate

Phenyliodo diacetate

phenyliododiacetate

Phenyliodoso acetate

Phenyliodoso diacetate

phenyliodosodiacetate

phenyliodosyldiacetate

Iodobenzene 1,1-diacetate

acetic acid coMpound with iodosylbenzene (2:1)

(Diacetoxyiodo)benzene, Bis(acetoxy)(phenyl)iodane

Iodosobenzene diacetate ,PIDA

Theiodoethyl ester two

acetic acid coMpound with iodobenzene (2:1)

DKFZp686B11164

KIAA1999

mAVO3

MGC39830

Monoclonal Anti-RICTOR antibody produced in mouse

PhI(OAc)2

[acetyloxy(phenyl)-λ3-iodanyl] acetate

[acetyloxy(phenyl)-$l^{3}-iodanyl] acetate

bis(acetyloxy)(phenyl)-lambda~

(Diacetoxyiodo)benzene≥ 99% (HPLC)

[acetyloxy(phenyl)-λ<sup>3</sup>-iodanyl] acetate

-iodanyl acetate

bis(acetato-O)phenyliodine

Ethyl 2-(4-formylphenyl)2-methylpropionatephenyliodine diacetate

(Diacetoxyiodo)benzene=Phenyliodosodiacetate