2-(4-Morpholine)ethyl bromide

Product Name: 2-(4-Morpholine)ethyl bromide
CAS No.: 89583-07-3
Chemical Name: 2-(4-Morpholine)ethyl bromide
Synonyms: 4-(2-broMoethyl)Morpholine;2-MORPHOLINOETHYL BROMIDE;Morpholine, 4-(2-broMoethyl)-;2-(4-MORPHOLINE)ETHYL BROMIDE;4-(2-Morpholine)ethyl bromide;4-(2-bromoethyl)morpholin-4-ium
CBNumber: CB2228761
Molecular Formula: C6H12BrNO
Formula Weight: 194.07
MOL File: 89583-07-3.mol

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2-(4-Morpholine)ethyl bromide Property

Boiling point:: 219.9±25.0 °C(Predicted)
Density: 1.393±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Store in freezer, under -20°C
pka: 5.90±0.10(Predicted)
Appearance: Colorless to light yellow Solid-Liquid Mixture

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB139679
Product name: 4-(2-Bromoethyl)morpholine
Packaging: 5G
Price: $300
Updated: 2021/12/16

Matrix Scientific

Product number: 113723
Product name: 2-(4-Morpholine)ethyl bromide
Purity: 95%
Packaging: 1g
Price: $403
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139679
Product name: 4-(2-Bromoethyl)morpholine
Packaging: 500mg
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139679
Product name: 4-(2-Bromoethyl)morpholine
Packaging: 1g
Price: $150
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB139679
Product name: 4-(2-Bromoethyl)morpholine
Packaging: 2g
Price: $200
Updated: 2021/12/16

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2-(4-Morpholine)ethyl bromide Chemical Properties,Usage,Production

Synthesis

622-40-2

89583-07-3

The general procedure for the synthesis of 2-(4-morpholinato)ethyl bromide from 2-morpholine ethanol is as follows: Example 4780: 2-morpholine ethanol (1 g, 7.62 mmol) was dissolved in dichloromethane (76 mL) and cooled to 0°C in an ice bath. Subsequently, dibromotriphenylphosphine (3.86 g, 9.15 mmol) was added to the solution. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, solid impurities were removed by filtration to afford pure 2-(4-morpholinato)ethyl bromide (1.4 g, quantitative yield). The product was characterized by 300 MHz 1H NMR (CD3OD) with chemical shifts δ (ppm) of 4.1 (m, 2H), 3.85 (m, 2H), 3.8 (t, 2H), 3.7 (t, 2H), 3.58 (m, 2H), 3.25 (m, 2H); mass spectrometry (MS) showed a molecular ion peak of 194 (M + 1).

References

[1] Patent: US2008/58315, 2008, A1. Location in patent: Page/Page column 46
[2] Arhiv za Kemiju, 1946, vol. 18, p. 87,92
[3] Chem.Abstr., 1948, p. 3395
[4] Patent: WO2013/33085, 2013, A1. Location in patent: Paragraph 00179
[5] Patent: US2010/160308, 2010, A1. Location in patent: Page/Page column 26

2-(4-Morpholine)ethyl bromide Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(4-Morpholine)ethyl bromide Suppliers

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View Lastest Price from 2-(4-Morpholine)ethyl bromide manufacturers

Career Henan Chemical Co

Product: 2-(4-Morpholine)ethyl bromide 89583-07-3
Price: US $9.80/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-03

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2-(4-MORPHOLINE)ETHYL BROMIDE

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4-(2-Morpholine)ethyl bromide

89583-07-3

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