ChemicalBook > CAS DataBase List > 2-(4-Morpholine)ethyl bromide
2-(4-Morpholine)ethyl bromide
- Product Name
- 2-(4-Morpholine)ethyl bromide
- CAS No.
- 89583-07-3
- Chemical Name
- 2-(4-Morpholine)ethyl bromide
- Synonyms
- 4-(2-broMoethyl)Morpholine;2-MORPHOLINOETHYL BROMIDE;Morpholine, 4-(2-broMoethyl)-;2-(4-MORPHOLINE)ETHYL BROMIDE;4-(2-Morpholine)ethyl bromide;4-(2-bromoethyl)morpholin-4-ium
- CBNumber
- CB2228761
- Molecular Formula
- C6H12BrNO
- Formula Weight
- 194.07
- MOL File
- 89583-07-3.mol
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2-(4-Morpholine)ethyl bromide Property
- Boiling point:
- 219.9±25.0 °C(Predicted)
- Density
- 1.393±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Store in freezer, under -20°C
- pka
- 5.90±0.10(Predicted)
- Appearance
- Colorless to light yellow Solid-Liquid Mixture
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N-Bromosuccinimide Price
Biosynth Carbosynth
- Product number
- FB139679
- Product name
- 4-(2-Bromoethyl)morpholine
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB139679
- Product name
- 4-(2-Bromoethyl)morpholine
- Packaging
- 1g
- Price
- $150
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB139679
- Product name
- 4-(2-Bromoethyl)morpholine
- Packaging
- 2g
- Price
- $200
- Updated
- 2021/12/16
Biosynth Carbosynth
- Product number
- FB139679
- Product name
- 4-(2-Bromoethyl)morpholine
- Packaging
- 5G
- Price
- $300
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 113723
- Product name
- 2-(4-Morpholine)ethyl bromide
- Purity
- 95%
- Packaging
- 1g
- Price
- $403
- Updated
- 2021/12/16
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2-(4-Morpholine)ethyl bromide Chemical Properties,Usage,Production
Synthesis
622-40-2
89583-07-3
The general procedure for the synthesis of 2-(4-morpholinato)ethyl bromide from 2-morpholine ethanol is as follows: Example 4780: 2-morpholine ethanol (1 g, 7.62 mmol) was dissolved in dichloromethane (76 mL) and cooled to 0°C in an ice bath. Subsequently, dibromotriphenylphosphine (3.86 g, 9.15 mmol) was added to the solution. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, solid impurities were removed by filtration to afford pure 2-(4-morpholinato)ethyl bromide (1.4 g, quantitative yield). The product was characterized by 300 MHz 1H NMR (CD3OD) with chemical shifts δ (ppm) of 4.1 (m, 2H), 3.85 (m, 2H), 3.8 (t, 2H), 3.7 (t, 2H), 3.58 (m, 2H), 3.25 (m, 2H); mass spectrometry (MS) showed a molecular ion peak of 194 (M + 1).
References
[1] Patent: US2008/58315, 2008, A1. Location in patent: Page/Page column 46
[2] Arhiv za Kemiju, 1946, vol. 18, p. 87,92
[3] Chem.Abstr., 1948, p. 3395
[4] Patent: WO2013/33085, 2013, A1. Location in patent: Paragraph 00179
[5] Patent: US2010/160308, 2010, A1. Location in patent: Page/Page column 26
2-(4-Morpholine)ethyl bromide Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-(4-Morpholine)ethyl bromide manufacturers
Career Henan Chemical Co
- Product
- 2-(4-Morpholine)ethyl bromide 89583-07-3
- Price
- US $9.80/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-03
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