ChemicalBook > CAS DataBase List > 4-Chloro-3-nitrobenzenesulfonamide

4-Chloro-3-nitrobenzenesulfonamide

Product Name
4-Chloro-3-nitrobenzenesulfonamide
CAS No.
97-09-6
Chemical Name
4-Chloro-3-nitrobenzenesulfonamide
Synonyms
4-chloro-3-nitrobenzenesulphonamide;YELLOW SULFONE;BUTTPARK 76\07-88;4-Chloro-3-Nitrosulfonamide;4-CHLORO-3-NITROSULFAMYLBENZENE;3-NITRO-4-CHLOROBENZENESULFONAMIDE;2-NITROCHLOROBENZENE-4-SULFONAMIDE;O-NITROCHLOROBENZENE-P-SULFONAMIDE;4-chloro-3-nitro-benzenesulfonamid;4-CHLORO-3-NITROBENZENESULFONAMIDE
CBNumber
CB2243863
Molecular Formula
C6H5ClN2O4S
Formula Weight
236.63
MOL File
97-09-6.mol
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4-Chloro-3-nitrobenzenesulfonamide Property

Melting point:
25-35 °C
Boiling point:
175-176 °C
Density 
1.5966 (rough estimate)
refractive index 
1.6000 (estimate)
storage temp. 
Inert atmosphere,Room Temperature
form 
crystalline powder
pka
9.28±0.60(Predicted)
color 
White to off white
Water Solubility 
224.8mg/L(15 ºC)
CAS DataBase Reference
97-09-6(CAS DataBase Reference)
EPA Substance Registry System
Benzenesulfonamide, 4-chloro-3-nitro- (97-09-6)
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2935909099
Hazardous Substances Data
97-09-6(Hazardous Substances Data)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific
Product number
OR24156
Product name
4-Chloro-3-nitrobenzenesulphonamide
Packaging
5g
Price
$25
Updated
2021/12/16
SynQuest Laboratories
Product number
8669-5-X7
Product name
4-Chloro-3-nitrobenzene-1-sulfonamide
Packaging
5G
Price
$28
Updated
2021/12/16
Matrix Scientific
Product number
098414
Product name
3-Nitro-4-chlorobenzenesulfonamide
Purity
95+%
Packaging
5g
Price
$53
Updated
2021/12/16
Biosynth Carbosynth
Product number
FC146441
Product name
4-Chloro-3-nitrobenzenesulfonamide
Packaging
25g
Price
$80
Updated
2021/12/16
Apolloscientific
Product number
OR24156
Product name
4-Chloro-3-nitrobenzenesulphonamide
Packaging
25g
Price
$83
Updated
2021/12/16
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4-Chloro-3-nitrobenzenesulfonamide Chemical Properties,Usage,Production

Chemical Properties

Light yellow to light brown crystalline powder

Uses

4-Chloro-3-nitrobenzenesulfonamide is used as a chemical intermediate for azo dyes.

Synthesis

Chlorosulphonic acid (450 mL) was slowly added to 2-chloronitrobenzene (100 g). The reaction mass was heated to 100°C and maintained at that temperat ure for 6 hours before cooling to ambient temperature and stirring for an additional 12 hours. The reaction mass was slowly poured into chilled aqueous ammonia (800 mL) and the reaction mixture was stirred for 3 hours at -10°C. The reaction mixture was then warmed to 23°C and stirred for 2 h ours. The reaction mixture was then filtered and the obtained solid was washed three times with water (200 mL x 3). The solid was dissolved in methanol (600 mL) at 60°C, charged with water (200 mL), and was stirred for 1 hour at 60°C. Again, the reaction mixture was charged with water (200 mL) and stirred for 1 hour at 60°C. Once again, the reaction mixtu re was charged with water (200 mL) and stirred for 1 hour. After cooling to room temperature and stirring for 1 hour, the reaction mixture was filtered, and the solid was washed with a 1 :1 mixture of methanol and water (100 mL). The solid was dried under vacuum at 60°C. Crystallization of the residue with toluen e gave the 4-Chloro-3-nitrobenzenesulfonamide(50 g).

4-Chloro-3-nitrobenzenesulfonamide Preparation Products And Raw materials

Raw materials

Sulfuryl chloride

Preparation Products

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4-Chloro-3-nitrobenzenesulfonamide Suppliers

China 141 Germany 1 India 7 Japan 1 Ukraine 3 United Kingdom 7 United States 16 Global 176
Zhejiang Chenhe Biomedicine Co. LTD
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View Lastest Price from 4-Chloro-3-nitrobenzenesulfonamide manufacturers

Career Henan Chemical Co
Product
4-Chloro-3-nitrobenzenesulfonamide 97-09-6
Price
US $1.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
200kg
Release date
2018-12-17

97-09-6, 4-Chloro-3-nitrobenzenesulfonamideRelated Search:

Sodium 3-nitrobenzenesulphonate 4-Nitrophenyl chloroformate Epichlorohydrin 1-Chloro-3-nitrobenzene 2-Nitrochlorobenzene 3,4-Difluoronitrobenzene Sulfanilamide 3-Nitrobenzaldehyde p-Toluenesulfonamide chloronitrobenzene Chloroacetic acid 4-Chloronitrobenzene Difluorochloromethane 1,3-Dinitrobenzene 3-NITRO-4-CHLORO BENZENE SULFONANILIDE 2-NITROCHLOROBENZENE-4-(N,N-DIMETHYL)-SULPHONAMIDE 2-NITROCHLOROBENZENE-4-SULFOMETHYL AMIDE 2-CHLORO-5-NITROBENZENESULFONAMIDE 98%,2-CHLORO-5-NITROBENZENESULFONAMIDE

  • BUTTPARK 76\07-88
  • 3-NITRO-4-CHLOROBENZENESULFONAMIDE
  • 4-CHLORO-3-NITROBENZENE-1-SULFONAMIDE
  • 4-CHLORO-3-NITROBENZENESULFONAMIDE
  • 4-CHLORO-3-NITROSULFAMYLBENZENE
  • YELLOW SULFONE
  • 4-chloro-3-nitro-benzenesulfonamid
  • O-NITROCHLOROBENZENE-P-SULFONAMIDE
  • 2-NITROCHLOROBENZENE-4-SULFONAMIDE
  • 4-chloro-3-nitrobenzenesulphonamide
  • 4-Chloro-3-nitrobenzene-1-sulphonamide
  • 3-Nitro-4-chlorobenzensulfonyl amine
  • Benzenesulfonamide, 4-chloro-3-nitro-
  • 4-Chloro-3-Nitrosulfonamide
  • 97-09-6
  • 1997-09-6
  • 1997-9-6
  • C6H5ClN2O4S
  • ClC6H3NO2SO2NH2
  • C6H3ClNO5S
  • Benzene derivates
  • Intermediates of Dyes and Pigments