4-Iodobenzaldehyde
- Product Name
- 4-Iodobenzaldehyde
- CAS No.
- 15164-44-0
- Chemical Name
- 4-Iodobenzaldehyde
- Synonyms
- NSC 84301;P-IODOBENZALDEHYDE;4-IODOBENZALDEHYDE;4-Iodobenzaldehyde>Benzaldehyde, 4-iodo-;4-Iodobenzaldehyde 96%;Benzaldehyde of iodine;4-IODOBENZALDEHYDE 98+%;4-IODOBENZALDEHYDE, 97+%;TIANFUCHEM-- 15164-44-0--High purity 4-IODOBENZALDEHYDE in stock
- CBNumber
- CB2265151
- Molecular Formula
- C7H5IO
- Formula Weight
- 232.02
- MOL File
- 15164-44-0.mol
4-Iodobenzaldehyde Property
- Melting point:
- 78-82 °C (lit.)
- Boiling point:
- 265°C(lit.)
- Density
- 1.8576 (estimate)
- storage temp.
- 2-8°C
- form
- Crystals
- color
- Yellow
- Water Solubility
- Insoluble in water.
- Sensitive
- Air & Light Sensitive
- BRN
- 636101
- InChI
- InChI=1S/C7H5IO/c8-7-3-1-6(5-9)2-4-7/h1-5H
- InChIKey
- NIEBHDXUIJSHSL-UHFFFAOYSA-N
- SMILES
- C(=O)C1=CC=C(I)C=C1
- CAS DataBase Reference
- 15164-44-0(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 263826
- Product name
- 4-Iodobenzaldehyde
- Purity
- 96%
- Packaging
- 1g
- Price
- $114
- Updated
- 2024/03/01
- Product number
- I0612
- Product name
- 4-Iodobenzaldehyde
- Purity
- >96.0%(GC)
- Packaging
- 1g
- Price
- $64
- Updated
- 2024/03/01
- Product number
- I0612
- Product name
- 4-Iodobenzaldehyde
- Purity
- >96.0%(GC)
- Packaging
- 5g
- Price
- $225
- Updated
- 2024/03/01
- Product number
- L17448
- Product name
- 4-Iodobenzaldehyde, 98+%
- Packaging
- 1g
- Price
- $100.65
- Updated
- 2024/03/01
- Product number
- L17448
- Product name
- 4-Iodobenzaldehyde, 98+%
- Packaging
- 5g
- Price
- $334.65
- Updated
- 2024/03/01
4-Iodobenzaldehyde Chemical Properties,Usage,Production
Chemical Properties
Yellow crystals
Uses
4-Iodobenzaldehyde is used in synthesis of 4-[2-(trimethylsilyl)ethynyl]benzaldehyde, 5,15-dimesityl-10-(3-[2-(trimethylsilyl)ethynyi]phenyl}-20-(4-iodophenyl)porphyrin, and 5,15-dimesityl-10-[3,5-bis{2-[4-(N,N?-difluoroboryl-1,9-dimethyidipyrrin-5-yl)-phenyl]ethynyl}phenyl]-20-(4-iodophenyl)porphyrin.
Uses
4-Iodobenzaldehyde has been used in the preparation of:
- benzaldimine monolayers
- 4-[2-(trimethylsilyl)ethynyl]benzaldehyde
- 5,15-dimesityl-10-(3-[2-(trimethylsilyl)ethynyi]phenyl}-20-(4-iodophenyl)porphyrin
- 5,15-dimesityl-10-[3,5-bis{2-[4-(N,N′-difluoroboryl-1,9-dimethyidipyrrin-5-yl)-phenyl]ethynyl}phenyl]-20-(4-iodophenyl)porphyrin, multipigment building block
Synthesis
A mixture of 10.0g p-bromobenzaldehyde (54mmol), 81.1gKI (488mmol, 9.0eq), 31.7gCuI (166mmol, 3.1eq) and 150ml freshly distilled DMI was placed in a 500ml three-neck flask. The mixture was purged with nitrogen and heated at 200°C with vigorous stirring for 6 hours. After cooling to room temperature, add salt water and ice. The reaction vessel was placed in an ice bath for several hours and precipitated inorganic salts were removed by filtration. After the filtrate was extracted with diethyl ether, the extracts were combined and washed with brine. Removal of the solvent under reduced pressure gave the product 4-Iodobenzaldehyde.
4-Iodobenzaldehyde Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-Iodobenzaldehyde manufacturers
- Product
- 4-Iodobenzaldehyde 15164-44-0
- Price
- US $0.00-0.00/KG
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-15
- Product
- 4-iodobenzaldehyde 15164-44-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 97.3%
- Supply Ability
- 100 tons
- Release date
- 2022-02-08
- Product
- 4-IODOBENZALDEHYDE 15164-44-0
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-01