ChemicalBook > CAS DataBase List > 2-Bromo-6-phenylpyridine

2-Bromo-6-phenylpyridine

Product Name
2-Bromo-6-phenylpyridine
CAS No.
39774-26-0
Chemical Name
2-Bromo-6-phenylpyridine
Synonyms
2-brom-6-phenylpyridin;2-BROMO-6-PHENYLPYRIDINE;6-Bromo-2-phenylpyridine;2-bromine-6-phenypyridine;Pyridine, 2-bromo-6-phenyl-;2-bromo-6-phenylpyridine(SALTDATA: FREE)
CBNumber
CB2305480
Molecular Formula
C11H8BrN
Formula Weight
234.09
MOL File
39774-26-0.mol
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2-Bromo-6-phenylpyridine Property

Melting point:
50.0 to 54.0 °C
Boiling point:
315.1±22.0 °C(Predicted)
Density 
1.426±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
pka
0.00±0.10(Predicted)
form 
powder to lump
color 
White to Yellow
CAS DataBase Reference
39774-26-0(CAS DataBase Reference)
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B5150
Product name
2-Bromo-6-phenylpyridine
Purity
>98.0%(GC)
Packaging
200mg
Price
$58
Updated
2025/07/31
TCI Chemical
Product number
B5150
Product name
2-Bromo-6-phenylpyridine
Purity
>98.0%(GC)
Packaging
1g
Price
$171
Updated
2025/07/31
TRC
Product number
B698565
Product name
2-Bromo-6-phenylpyridine
Packaging
500mg
Price
$155
Updated
2021/12/16
TRC
Product number
B698565
Product name
2-Bromo-6-phenylpyridine
Packaging
1g
Price
$220
Updated
2021/12/16
AK Scientific
Product number
J97222
Product name
2-Bromo-6-phenylpyridine
Packaging
250mg
Price
$58
Updated
2021/12/16
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2-Bromo-6-phenylpyridine Chemical Properties,Usage,Production

Synthesis

626-05-1

98-80-6

39774-26-0

General procedure for the synthesis of 2-bromo-6-phenylpyridine from 2,6-dibromopyridine and phenylboronic acid: 2,6-dibromopyridine (2 g, 8.44 mmol), phenylboronic acid (1.03 g, 8.44 mmol), potassium carbonate (4.67 g, 33.77 mmol), and tetrabutylammonium bromide (TBAB, 271 mg, 0.84 mmol) were mixed in a 1 ,4-dioxane (16 ml) and water (4 ml) in a solvent mixture. The reaction mixture was degassed by blowing in nitrogen for 30 min, followed by addition of dichlorobis(triphenylphosphine)palladium(II) (PdCl2(dppf), 62 mg, 0.084 mmol). The reaction mixture was stirred at 40 °C for 1 h. After completion of the reaction, the reaction was filtered through diatomaceous earth. The filtrate was collected and the solvent was removed by distillation under reduced pressure. The crude product was purified by column chromatography using 100% petroleum ether as eluent to afford the target compound 2-bromo-6-phenylpyridine as a colorless solid (1.85 g, 93% yield).1H NMR (400 MHz, DMSO) δ 8.56 (dd, J = 6.3,2.4 Hz, 1H), 8.36-8.18 (m, 2H). 8.16-8.00 (m, 2H), 7.61-7.53 (m, 2H), 7.53-7.45 (m, 1H).

References

[1] Patent: WO2015/172196, 2015, A1. Location in patent: Paragraph 0033; 00179; 00200
[2] Patent: WO2009/111299, 2009, A2. Location in patent: Page/Page column 23
[3] Patent: JP5832992, 2015, B2. Location in patent: Paragraph 0139; 0140
[4] Patent: KR2015/137230, 2015, A. Location in patent: Paragraph 0113; 0114; 0115
[5] Patent: US2004/171614, 2004, A1

2-Bromo-6-phenylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Bromo-6-phenylpyridine manufacturers

Career Henan Chemical Co
Product
2-Bromo-6-phenylpyridine 39774-26-0
Price
US $1.00/kg
Min. Order
1kg
Purity
98%
Supply Ability
200kg
Release date
2018-12-20

39774-26-0, 2-Bromo-6-phenylpyridineRelated Search:

3-BROMO-4-PHENYLPYRIDINE 2-BROMO-4-PHENYLPYRIDINE 2-(4-Bromomethylphenyl)pyridine 2-BROMO-5-PHENYLPYRIDINE 2-BROMO-3-PHENYLPYRIDINE 4-(6-Bromo-pyridin-2-yl)-3-methyl-benzoicacid 2-Bromo-6-phenylpyridine 3-(6-Bromopyridin-2-yl)benzoic acid 4-(6-Bromo-pyridin-2-yl)-2-methyl-benzoicacid 3-BROMO-5-PHENYLPYRIDINE 5-BROMO-2-PHENYLPYRIDINE 4-BROMO-3-PHENYLPYRIDINE 3-BROMO-2-PHENYLPYRIDINE 4-Bromo-2-phenylpyridine 4-(8-Bromo-[1,7]naphthyridin-6-yl)-benzoic acid 3-AMINO-6-BROMO-2-PHENYLPYRIDINE 4-(6-Bromo-pyridin-2-yl)-benzoic acid 4-(6-BROMOPYRIDIN-2-YL)BENZALDEHYDE

  • Pyridine, 2-bromo-6-phenyl-
  • 6-Bromo-2-phenylpyridine
  • 2-bromo-6-phenylpyridine(SALTDATA: FREE)
  • 2-BROMO-6-PHENYLPYRIDINE
  • 2-brom-6-phenylpyridin
  • 2-bromine-6-phenypyridine
  • 39774-26-0