2-IODO-5-NITROANISOLE
Uses- Product Name
- 2-IODO-5-NITROANISOLE
- CAS No.
- 5458-84-4
- Chemical Name
- 2-IODO-5-NITROANISOLE
- Synonyms
- 2-IODO-5-NITROANISOLE;2-IODO-5-NITROANISOLE 97%;2-iodo-5-nitrobenzyl ether;4-Iodo-3-methoxynitrobenzene;I-Iodo-2-Methoxy-4-nitrobenzene;1-Iodo-2-methoxy-4-nitrobenzene;Benzene, 1-iodo-2-methoxy-4-nitro-;2-Iodo-5-nitroanisole【4-Iodo-3-methoxynitrobenzene】;4-Iodo-3-Methoxynitrobenzene[2-Iodo-5-nitroanisole]
- CBNumber
- CB2321488
- Molecular Formula
- C7H6INO3
- Formula Weight
- 279.03
- MOL File
- 5458-84-4.mol
2-IODO-5-NITROANISOLE Property
- Melting point:
- 128-130°C
- Boiling point:
- 341.2±32.0 °C(Predicted)
- Density
- 1.893±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- Appearance
- White to light brown Solid
- CAS DataBase Reference
- 5458-84-4(CAS DataBase Reference)
Safety
- Risk Statements
- 36/37/38
- Safety Statements
- 26-36/37/39
- HS Code
- 29093090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- S362824
- Product name
- 2-IODO-5-NITROANISOLE
- Purity
- Aldrich<sup>CPR</sup>
- Packaging
- 1 unit
- Price
- $185
- Updated
- 2025/07/31
- Product number
- S362824
- Product name
- 2-IODO-5-NITROANISOLE
- Purity
- Aldrich
- Packaging
- 250mg
- Price
- $179
- Updated
- 2024/03/01
- Product number
- I737043
- Product name
- 2-Iodo-5-nitroanisole
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- I737043
- Product name
- 2-Iodo-5-nitroanisole
- Packaging
- 500mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 149002
- Product name
- 2-Iodo-5-nitroanisole
- Purity
- 97%
- Packaging
- 1g
- Price
- $9
- Updated
- 2021/12/16
2-IODO-5-NITROANISOLE Chemical Properties,Usage,Production
Uses
2-Iodo-5-nitrobenzyl ether is a useful research chemical for organic synthesis and other chemical processes.
Synthesis
97-52-9
5458-84-4
General procedure for the synthesis of 2-iodo-5-nitroanisole from 2-methoxy-4-nitroaniline: Potassium iodide (5.0 mmol) and sodium nitrite (3.0 mmol) were sequentially added to an acetic acid solution (30 mL) containing 2-methoxy-4-nitroaniline (2.5 mmol) and camphorsulphonic acid (3.0 mmol) at room temperature. The reaction mixture was stirred continuously for 24 h, during which nitrogen release was observed. Upon completion of the reaction, the reaction endpoint was confirmed by β-naphthol test and thin layer chromatography (TLC), followed by removal of solvent using a rotary evaporator. The resulting solid was washed with water and extracted with dichloromethane (CH2Cl2). The extract was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure to remove the solvent. Finally, the product was purified by column chromatography, and the eluting solvent was a mixed system of hexane/dichloromethane. The physical properties and 1H NMR spectral data of the obtained product were consistent with the commercially available analytically pure sample.
References
[1] Tetrahedron, 2013, vol. 69, # 16, p. 3511 - 3517
[2] Chemical and Pharmaceutical Bulletin, 2014, vol. 62, # 10, p. 979 - 988
[3] Journal of Medicinal Chemistry, 2009, vol. 52, # 15, p. 4869 - 4882
[4] Chem. Zentralbl., 1901, vol. 72, # I, p. 739
[5] Privatmitteilung,
2-IODO-5-NITROANISOLE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-IODO-5-NITROANISOLE manufacturers
- Product
- 2-IODO-5-NITROANISOLE 5458-84-4
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2024-11-26
- Product
- 1-Iodo-2-methoxy-4-nitrobenzene 5458-84-4
- Price
- US $8.00/KG
- Min. Order
- 1KG
- Purity
- ≥98%
- Supply Ability
- kg--ton
- Release date
- 2020-03-08
- Product
- 2-IODO-5-NITROANISOLE 5458-84-4
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg -1000kg
- Release date
- 2020-01-02