2-Chloro-N,N-dimethylacetamide

Product Name: 2-Chloro-N,N-dimethylacetamide
CAS No.: 2675-89-0
Chemical Name: 2-Chloro-N,N-dimethylacetamide
Synonyms: EOS-61825;AKOS BBS-00000943;2-Chloro-N,N-dimethy;CHLOROACETYLDIMETHYLAMINE;N,N-DIMETHYLCHOROACETAMIDE;N,N-DIMETHYLCHLOROACETAMIDE;N-DiMethyl-2-chloroacetaMide;N,N-DIMETHYL-2-CHLOROACETAMIDE;2-CHLORO-N,N-DIMETHYLACETAMIDE;2-CHLORO-N,N-DIMETHYL ACETAMINE
CBNumber: CB2343589
Molecular Formula: C4H8ClNO
Formula Weight: 121.57
MOL File: 2675-89-0.mol

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2-Chloro-N,N-dimethylacetamide Property

Melting point:: 15-16 °C
Boiling point:: 98-100°C/11mm
Density: 1.182 g/mL at 20 °C (lit.)
refractive index: n20/D 1.479
Flash point:: 98-100°C/11mm
storage temp.: Store below +30°C.
solubility: Chloroform (Slightly), Hexane (Slightly), Methanol (Slightly)
pka: -0.95±0.70(Predicted)
form: Liquid
color: Clear colorless to pale yellow
BRN: 969568
InChIKey: XBPPLECAZBTMMK-UHFFFAOYSA-N
CAS DataBase Reference: 2675-89-0(CAS DataBase Reference)

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Safety

Hazard Codes: C
Risk Statements: 22-34
Safety Statements: 26-36/37/39-45
RIDADR: UN 3265 8/PG 3
WGK Germany: 3
HS Code: 29241990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

Precautionary statements

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 24350
Product name: 2-Chloro-N,N-dimethylacetamide
Purity: ≥97.0% (GC)
Packaging: 25mL
Price: $138
Updated: 2024/03/01

TCI Chemical

Product number: C3011
Product name: 2-Chloro-N,N-dimethylacetamide
Packaging: 5G
Price: $44
Updated: 2024/03/01

TCI Chemical

Product number: C3011
Product name: 2-Chloro-N,N-dimethylacetamide
Packaging: 25G
Price: $150
Updated: 2024/03/01

Alfa Aesar

Product number: H50229
Product name: 2-Chloro-N,N-dimethylacetamide, 97%
Packaging: 250mg
Price: $69.65
Updated: 2024/03/01

Alfa Aesar

Product number: H50229
Product name: 2-Chloro-N,N-dimethylacetamide, 97%
Packaging: 1g
Price: $226.65
Updated: 2024/03/01

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2-Chloro-N,N-dimethylacetamide Chemical Properties,Usage,Production

Uses

2-Chloro-N,N-dimethylacetamide is N,M-dialkyl amide used as an organic catalyst in the preparation of phosphorylated thiosemicarbazide.

Uses

2-Chloro-N,N-dimethylacetamide (N,N-dimethylchloroacetamide) was used in the synthesis of (S)-carbinoxamine.

Synthesis

In a 500 mL four-necked flask, sodium hydrogen carbonate 126.0 g (1.50 mol) and 146.8 g of toluene were added, and the mixture was stirred while cooling. The internal temperature was maintained below 5 ° C, 112.9 g (1.00 mol) of chloroacetyl chloride was added dropwise over 4 hours, and 49.6 g (1.10 mol) of dimethylamine gas was blown over 4 hours. After stirring at -2 to 1 ° C. for 1 hour, the reaction solution was filtrated under reduced pressure to remove inorganic salt crystals by filtration. The crystals were washed with 100 g of toluene, and the filtrate and washings were combined. After separating and removing the aqueous layer in the filtrate washings, the toluene layer was concentrated under reduced pressure to obtain 113.2 g (0.93 mol) of oily 2-chloro-N, N-dimethylacetamide. The yield was 93.1%.

2-Chloro-N,N-dimethylacetamide Preparation Products And Raw materials

Raw materials

Dimethylamine hydrochloride Chloroacetyl chloride Sodium bicarbonate Dichloromethane Sodium hydroxide Dimethylamine

Preparation Products

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2-Chloro-N,N-dimethylacetamide Suppliers

Americas 1 Canada 2 China 195 Europe 2 Germany 10 Hungary 1 India 12 Israel 1 Japan 3 South Korea 1 Switzerland 4 Ukraine 1 United Kingdom 10 United States 34 Global 277

Carbosynth

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NiCHe Materials Ltd.

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Apollo Scientific Ltd

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Biosynth Carbosynth

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Manchester Organics

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Apollo Scientific Ltd.

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Leancare Ltd.

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CARBONE SCIENTIFIC CO.,LTD

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Eurolabs Limited

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Fulcrum Scientific Ltd.

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View Lastest Price from 2-Chloro-N,N-dimethylacetamide manufacturers

Hebei Weibang Biotechnology Co., Ltd

Product: 2-Chloro-N,N-dimethylacetamide 2675-89-0
Price: US $0.00-0.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20 mt
Release date: 2024-11-26

Henan Aochuang Chemical Co.,Ltd.

Product: 2-Chloro-N,N-dimethylacetamide 2675-89-0
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1Ton
Release date: 2022-10-17

Zhuozhou Wenxi import and Export Co., Ltd

Product: N,N-Dimethyl-2-chloroacetamide 2675-89-0
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-11

2675-89-0, 2-Chloro-N,N-dimethylacetamideRelated Search:

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AKOS BBS-00000943

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2-Chloro-N,N-dimethy

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2-CHLORO-N,N-DIMETHYL ACETAMINE

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2-CHLORO-N N-DIMETHYLACETAMIDE 98 %

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2-Chloro-N,N-dimethylacetamide >=97.0% (GC)

EOS-61825

2675-89-0 C4H8ClNO 2-Chloro-N,N-dimethylacetamide

2-Chloro-N,N-dimethylacetamide, 97%,

2675-89-0

ClCH2CONCH32

Carbonyl Compounds

Building Blocks

Amides

Organic Building Blocks

2675-89-0