Synthesis
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Pentafluoropyridine

Synthesis
Product Name
Pentafluoropyridine
CAS No.
700-16-3
Chemical Name
Pentafluoropyridine
Synonyms
PERFLUOROPYRIDINE;PENTAFLUOROPYRIDINE;Pentafluoropyridine>Pentafluoropyridine 99%;5-Chloro-2-caynopyridine;PENTAFLUOROPYRIDINE, 99+%;2,3,4,5,6-Perfluoropyridine;2,3,4,5,6-PENTAFLUOROPYRIDINE;Pentafluoropyridine, 99+% 5GR;Pyridine, 2,3,4,5,6-pentafluoro-
CBNumber
CB2344607
Molecular Formula
C5F5N
Formula Weight
169.05
MOL File
700-16-3.mol
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Pentafluoropyridine Property

Melting point:
-42
Boiling point:
83-85 °C
Density 
1.54 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.386(lit.)
Flash point:
75 °F
storage temp. 
Inert atmosphere,2-8°C
form 
Liquid
pka
-12.08±0.28(Predicted)
color 
Clear colorless
Specific Gravity
1.62
Water Solubility 
Not miscible or difficult to mix in water.
BRN 
1427064
InChIKey
XTGOWLIKIQLYRG-UHFFFAOYSA-N
CAS DataBase Reference
700-16-3(CAS DataBase Reference)
NIST Chemistry Reference
Pyridine, pentafluoro-(700-16-3)
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Safety

Hazard Codes 
Xn,F,Xi
Risk Statements 
10-20/21/22-36/37/38
Safety Statements 
26-28-24/25-16
RIDADR 
UN 1993 3/PG 3
WGK Germany 
3
Hazard Note 
Flammable/Irritant
HazardClass 
3
PackingGroup 
III
HS Code 
29333990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H226Flammable liquid and vapour

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P233Keep container tightly closed.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
158798
Product name
Pentafluoropyridine
Purity
≥99%
Packaging
25g
Price
$157
Updated
2024/03/01
TCI Chemical
Product number
P0926
Product name
Pentafluoropyridine
Purity
>98.0%(GC)
Packaging
5g
Price
$66
Updated
2024/03/01
TCI Chemical
Product number
P0926
Product name
Pentafluoropyridine
Purity
>98.0%(GC)
Packaging
25g
Price
$210
Updated
2024/03/01
Alfa Aesar
Product number
A19656
Product name
Pentafluoropyridine, 99%
Packaging
5g
Price
$42.65
Updated
2024/03/01
Alfa Aesar
Product number
A19656
Product name
Pentafluoropyridine, 99%
Packaging
25g
Price
$146
Updated
2024/03/01
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Pentafluoropyridine Chemical Properties,Usage,Production

Synthesis

Historically, potassium fluoride has been used with solvents to perform the Halex reaction and Finger and Kruse established the use of polar aprotic solvents in the Halex reaction, with DMSO and DMF being used for the conversion of pentachloropyridine to pentafluoropyridine.

Chemical Properties

CLEAR COLOURLESS LIQUID

Uses

Pentafluoropyridine was used in the preparation of η2-C,C coordinated pentafluoropyridine complex. It was also used in the preparation of polyfluorinated coupling products via Pd(0)-catalyzed cross-coupling reaction with diarylzinc compounds. It was also used as derivatizing reagent in the sensitive GC-MS method for determination of the four endocrine disrupting chemicals.

General Description

The reactions of pentafluoropyridine with cobalt(0) complex, Co(PMe3)4 was investigated.

Purification Methods

Distil it through a concentric tube column; it has in cyclohexane at 256.8nm. [Chambers et al. J Chem Soc 3573 1964, NMR: Bell et al. J Fluorine Chem 1 51 1971.] The hexafluoroantimonate has m 98-102o(dec) after crystallisation from liquid SO2. [Beilstein 20/5 V 401.]

Pentafluoropyridine Preparation Products And Raw materials

Raw materials

Preparation Products

3,5-Difluoropyridine 3,5-DIFLUORO-PYRIDIN-4-YLAMINE 3,5-DIFLUOROPYRIDINE-4-CARBALDEHYDE
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Pentafluoropyridine Suppliers

Americas 1 Belgium 2 China 171 Europe 1 France 1 Germany 10 India 6 Italy 1 Japan 5 Jordan 1 Russia 2 Switzerland 3 The Netherlands 1 United Kingdom 16 United States 36 Global 257
Ark Pharm, Inc.
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Pure Chemistry Scientific Inc.
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Accela ChemBio Inc.
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Matrix Scientific
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View Lastest Price from Pentafluoropyridine manufacturers

Hebei Weibang Biotechnology Co., Ltd
Product
Pentafluoropyridine 700-16-3
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
500000kg
Release date
2024-10-31
Hebei Yanxi Chemical Co., Ltd.
Product
Pentafluoropyridine 700-16-3
Price
US $20.00-8.00/kg
Min. Order
1kg
Purity
0.99
Supply Ability
20 tons
Release date
2023-10-07
Shaanxi Dideu Medichem Co. Ltd
Product
Pentafluoropyridine 700-16-3
Price
US $1.10/g
Min. Order
1g
Purity
99.0% min
Supply Ability
100 tons min
Release date
2021-05-26

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  • Pentafluoropyridine 99%
  • PENTAFLUOROPYRIDINE
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  • 2,3,4,5,6-Pentafluoropyridine 99%
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  • 5-Chloro-2-caynopyridine
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  • Pentafluoropyridine ISO 9001：2015 REACH
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  • 700-16-3
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