ChemicalBook > CAS DataBase List > (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol

(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol

Product Name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
CAS No.
103755-58-4
Chemical Name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Synonyms
1-Phenyl-1H-1,2,3-Triazol-4-yl;1H-1,2,3-Triazole-4-methanol, 1-phenyl-;(1-PHENYL-1H-1,2,3-TRIAZOL-4-YL)METHANOL;(1-phenyl-1H-1,2,3-triazole-4-yl)methanol;1-Phenyl-1H-1,2,3-triazole-4-methanol, 97%
CBNumber
CB2409760
Molecular Formula
C9H9N3O
Formula Weight
175.19
MOL File
103755-58-4.mol
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(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Property

Melting point:
114-116°C
Boiling point:
379.9±34.0 °C(Predicted)
Density 
1.27±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
12.96±0.10(Predicted)
CAS DataBase Reference
103755-58-4(CAS DataBase Reference)
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Safety

HazardClass 
IRRITANT
HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC
Product number
P337388
Product name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Packaging
250mg
Price
$90
Updated
2021/12/16
AK Scientific
Product number
V0637
Product name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Packaging
250mg
Price
$99
Updated
2021/12/16
AK Scientific
Product number
V0637
Product name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Packaging
1g
Price
$143
Updated
2021/12/16
Apolloscientific
Product number
OR32719
Product name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Packaging
1g
Price
$163
Updated
2021/12/16
Matrix Scientific
Product number
044400
Product name
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol
Purity
>95%
Packaging
5g
Price
$210
Updated
2021/12/16
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(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Chemical Properties,Usage,Production

Synthesis

107-19-7

622-37-7

103755-58-4

General procedure: Azidobenzene (1 eq.), 2-propyn-1-ol (1.5 eq.) and copper sulfate pentahydrate (0.1 eq.) were dissolved in a solvent mixture of water and acetonitrile (12 mL, water:acetonitrile = 2:1, v/v) at room temperature. Hydrazine hydrate (1 eq.) was added dropwise to the above solution under vigorous stirring. The reaction mixture gradually changed to light yellow or light green color. The progress of the reaction is monitored by thin layer chromatography (TLC) and the reaction is usually completed within a few minutes (see Table 3 for specific times). Upon completion of the reaction, the product usually precipitates as a colorless solid (unless otherwise noted). The reaction mixture is diluted with excess water and subsequently filtered. The collected solid product is washed with water and dried. The resulting solid may be crystallized by dissolution in a suitable solvent or filtered through a pad of diatomaceous earth to obtain analytically pure 1-phenyl-1hydro-4-methanolyl-1,2,3-triazole.

References

[1] New Journal of Chemistry, 2006, vol. 30, # 8, p. 1137 - 1139
[2] Green Chemistry, 2012, vol. 14, # 5, p. 1298 - 1301
[3] Applied Catalysis A: General, 2013, vol. 453, p. 151 - 158
[4] Archiv der Pharmazie, 2015, vol. 348, # 11, p. 796 - 807
[5] New Journal of Chemistry, 2015, vol. 39, # 8, p. 5902 - 5907

(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (1-Phenyl-1H-1,2,3-triazol-4-yl)methanol manufacturers

Career Henan Chemical Co
Product
(1-Phenyl-1H-1,2,3-triazol-4-yl)methanol 103755-58-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg;10kg;100kg
Release date
2019-08-29

103755-58-4, (1-Phenyl-1H-1,2,3-triazol-4-yl)methanolRelated Search:

Diphenyl ether 2-Phenylphenol Triphenylphosphine oxide Triton X-100 PHENYL VALERATE Methanol Triphenylphosphine Phenyl salicylate PHENYL RESIN [1-(4-Chlorophenyl)-1H-1,2,3-triazol-4-yl]methanol Phenylacetone Phenylacetic acid 5-METHYL-1-[3-(TRIFLUOROMETHYL)PHENYL]-1H-1,2,3-TRIAZOLE-4-CARBOXYLIC ACID (5-METHYL-2-PHENYL-2H-1,2,3-TRIAZOL-4-YL)METHANOL METHYL 5-(2-METHOXY-2-OXOETHYL)-1-(4-METHOXYPHENYL)-1H-1,2,3-TRIAZOLE-4-CARBOXYLATE METHYL 1-(2,4-DICHLOROPHENYL)-5-(2-METHOXY-2-OXOETHYL)-1H-1,2,3-TRIAZOLE-4-CARBOXYLATE METHYL 1-(4-CHLOROPHENYL)-5-(2-METHOXY-2-OXOETHYL)-1H-1,2,3-TRIAZOLE-4-CARBOXYLATE METHYL 5-(2-METHOXY-2-OXOETHYL)-1-[3-(TRIFLUOROMETHYL)PHENYL]-1H-1,2,3-TRIAZOLE-4-CARBOXYLATE

  • (1-PHENYL-1H-1,2,3-TRIAZOL-4-YL)METHANOL
  • 1-Phenyl-1H-1,2,3-Triazol-4-yl
  • (1-phenyl-1H-1,2,3-triazole-4-yl)methanol
  • 1H-1,2,3-Triazole-4-methanol, 1-phenyl-
  • 1-Phenyl-1H-1,2,3-triazole-4-methanol, 97%
  • 103755-58-4
  • API intermediates
  • Pyrrodiazole
  • Heterocyclic Series