ChemicalBook > CAS DataBase List > 4-CHLORO-2,6-DIMETHYLPYRIMIDINE

4-CHLORO-2,6-DIMETHYLPYRIMIDINE

Product Name: 4-CHLORO-2,6-DIMETHYLPYRIMIDINE
CAS No.: 4472-45-1
Chemical Name: 4-CHLORO-2,6-DIMETHYLPYRIMIDINE
Synonyms: Albb-005431;ASISCHEM A63094;TIMTEC-BB SBB010291;6-Chloro-2,4-dimethylpyrimidine;2,4-Dimethyl-6-chloropyrimidine;4-CHLORO-2,6-DIMETHYLPYRIMIDINE;Pyrimidine, 4-chloro-2,6-dimethyl-;4-Chloro-2,6-dimethylpyrimidine95%;4-CHLORO-2,6-DIMETHYLPYRIMIDINE 95%;4-Chloro-2,6-dimethylpyrimidine,97%
CBNumber: CB2489784
Molecular Formula: C6H7ClN2
Formula Weight: 142.59
MOL File: 4472-45-1.mol

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4-CHLORO-2,6-DIMETHYLPYRIMIDINE Property

Melting point:: 39-40 °C
Boiling point:: 180 °C
Density: 1.184±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: liquid
pka: 1.19±0.30(Predicted)
color: Clear, colourless
CAS DataBase Reference: 4472-45-1(CAS DataBase Reference)

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Safety

Hazard Codes: Xi,Xn
Risk Statements: 22
HazardClass: IRRITANT
HS Code: 2933599590

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: C584950
Product name: 4-Chloro-2,6-dimethylpyrimidine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

Apolloscientific

Product number: OR55150
Product name: 4-Chloro-2,6-dimethylpyrimidine
Purity: 99%
Packaging: 1g
Price: $22
Updated: 2021/12/16

Matrix Scientific

Product number: 018781
Product name: 4-Chloro-2,6-dimethyl-pyrimidine
Packaging: 500mg
Price: $24
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H32-5-AE
Product name: 4-Chloro-2,6-dimethylpyrimidine
Packaging: 1g
Price: $24
Updated: 2021/12/16

Matrix Scientific

Product number: 018781
Product name: 4-Chloro-2,6-dimethyl-pyrimidine
Packaging: 1g
Price: $39
Updated: 2021/12/16

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4-CHLORO-2,6-DIMETHYLPYRIMIDINE Chemical Properties,Usage,Production

Synthesis

6622-92-0

4472-45-1

General procedure for the synthesis of 4-chloro-2,6-dimethylpyrimidines from 2,4-dimethyl-6-hydroxypyrimidines: phosphorous trichloride (POCl3, 0.460 g, 3.0 mmol) was added to a solution of 2,4-dimethyl-6-hydroxypyrimidines (1.0 mmol) in toluene (15 mL), and the mixture was stirred for 3 hours under reflux conditions. Upon completion of the reaction, excess phosphorous trichloride was removed by distillation under reduced pressure and the reaction was subsequently quenched by the addition of ice water (10 mL). The pH of the reaction mixture was adjusted to 9-10 with sodium carbonate solution and then extracted with methyl tert-butyl ether (MTBE). The organic phase was dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent to afford the target product 4-chloro-2,6-dimethylpyrimidine (yield: 82%). Mass spectrometry (ESI) showed a molecular ion peak (m/z) [M + H]+ of 143.1.

References

[1] Bioorganic and Medicinal Chemistry Letters, 2018, vol. 28, # 10, p. 1769 - 1775
[2] Tetrahedron Letters, 1999, vol. 40, # 42, p. 7477 - 7478
[3] Patent: US5438058, 1995, A
[4] Patent: US6093718, 2000, A

4-CHLORO-2,6-DIMETHYLPYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

DIETHYL PYRIMIDINE-4,6-DICARBOXYLATE DIMETHYL PYRIMIDINE-4,6-DICARBOXYLATE PYRIMIDINE-4,6-DICARBOXYLIC ACID

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View Lastest Price from 4-CHLORO-2,6-DIMETHYLPYRIMIDINE manufacturers

Dideu Industries Group Limited

Product: 4-CHLORO-2,6-DIMETHYLPYRIMIDINE 4472-45-1
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-06

Career Henan Chemical Co

Product: 4-CHLORO-2,6-DIMETHYLPYRIMIDINE 4472-45-1
Price: US $1.00/kg
Min. Order: 1kg
Purity: 95%-99%
Supply Ability: as request
Release date: 2018-12-24

4472-45-1, 4-CHLORO-2,6-DIMETHYLPYRIMIDINERelated Search:

Pyrimidine 5-Chloro-2,6-dimethylpyrimidine 2-CHLORO-4,6-DIMETHYLPYRIMIDINE,98.0+%(GC),2-CHLORO-4,6-DIMETHYLPYRIMIDINE 5-Bromo-4-chloro-2,6-dimethylpyrimidine 2-Amino-5-chloro-4,6-dimethylpyrimidine,5-Chloro-4,6-dimethylpyrimidine-2-amine 4-AMINO-2-CHLORO-6,7-DIMETHYLPYRIMIDINE,4-AMINO-5-CHLORO-2,6-DIMETHYLPYRIMIDINE 4-Chloro-5-chloro-2,6-dimethylpyrimidine 5-Bromo-2-chloro-4,6-dimethylpyrimidine 6-CHLORO-1,3-DIMETHYLPYRIMIDINE-2,6-1H,3H-DIONE,6-Chloro-1,3-dimethylpyrimidine-2,4-dione,6-CHLORO-1,3-DIMETHYLPYRIMIDINE-2,4(1H,3H)-DIONE 4-chloro-2,5-dimethylpyrimidine 4-CHLORO-5,6-DIMETHYLPYRIMIDINE ETHYL 6-CHLORO-2,5-DIMETHYLPYRIMIDINE-4-CARBOXYLATE

4-CHLORO-2,6-DIMETHYLPYRIMIDINE

TIMTEC-BB SBB010291

Pyrimidine, 4-chloro-2,6-dimethyl- (7CI,8CI,9CI)

4-Chloro-2,6-dimethylpyrimidine95%

ASISCHEM A63094

4-CHLORO-2,6-DIMETHYLPYRIMIDINE 95%

Albb-005431

2,4-Dimethyl-6-chloropyrimidine

6-Chloro-2,4-dimethylpyrimidine

D241 4-Chloro-2,6-dimethyl-pyrimidine

Pyrimidine, 4-chloro-2,6-dimethyl-

4-Chloro-2,6-dimethylpyrimidine,97%

4-CHLORO-2,6-DIMETHYLPYRIMIDINE ISO 9001：2015 REACH

4472-45-1

Heterocycle-Pyrimidine series

alkyl chloride

API intermediates

PYRIMIDINE