ChemicalBook > CAS DataBase List > 3-Methyl-4-nitroaniline

3-Methyl-4-nitroaniline

Product Name
3-Methyl-4-nitroaniline
CAS No.
611-05-2
Chemical Name
3-Methyl-4-nitroaniline
Synonyms
NSC 17041;4-NITRO-M-TOLUIDINE;5-AMINO-2-NITROTOLUENE;3-Amino-6-nitrotoluene;6-Nitro-3-aMinotoluene;4-nitro-3-methylaniline;3-METHYL-4-NITROANILINE;3-Mehtyl-4-nitroaniline;3-Methyl-4-nitroaniline>3-METHYL-4-NITROANILINE 99%
CBNumber
CB2665283
Molecular Formula
C7H8N2O2
Formula Weight
152.15
MOL File
611-05-2.mol
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3-Methyl-4-nitroaniline Property

Melting point:
136-137°C
Boiling point:
330.0±22.0 °C(Predicted)
Density 
1.269±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
Methanol
form 
Solid
pka
1.12±0.10(Predicted)
color 
Brown Crystalline
BRN 
2209112
CAS DataBase Reference
611-05-2(CAS DataBase Reference)
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Safety

Hazard Codes 
T
Risk Statements 
23/24/25-33-51/53
Safety Statements 
28-36/37-45-61
RIDADR 
2660
HazardClass 
6.1
PackingGroup 
III
HS Code 
2921420090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H301Toxic if swalloed

H311Toxic in contact with skin

H331Toxic if inhaled

H373May cause damage to organs through prolonged or repeated exposure

H401Toxic to aquatic life

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P309IF exposed or if you feel unwell:

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TCI Chemical
Product number
M1677
Product name
3-Methyl-4-nitroaniline
Purity
>97.0%(GC)
Packaging
5g
Price
$37
Updated
2025/07/31
TCI Chemical
Product number
M1677
Product name
3-Methyl-4-nitroaniline
Purity
>97.0%(GC)
Packaging
25g
Price
$186
Updated
2025/07/31
TRC
Product number
M323580
Product name
3-Methyl-4-nitrobenzeneamine
Packaging
250mg
Price
$105
Updated
2021/12/16
AK Scientific
Product number
9147AB
Product name
3-Methyl-4-nitroaniline
Packaging
1g
Price
$68
Updated
2021/12/16
AK Scientific
Product number
9147AB
Product name
3-Methyl-4-nitroaniline
Packaging
25g
Price
$277
Updated
2021/12/16
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3-Methyl-4-nitroaniline Chemical Properties,Usage,Production

Chemical Properties

Brown Crystalline Solid

Uses

3-Methyl-4-nitrobenzeneamine (cas# 611-05-2) is a compound useful in organic synthesis.

Synthesis Reference(s)

Synthetic Communications, 18, p. 2161, 1988 DOI: 10.1080/00397918808068287

Synthesis

99584-85-7

611-05-2

General procedure for the synthesis of 3-methyl-4-nitroaniline (20-2) from 3-methyl-4-nitrobenzamide (20-1, 40 g, 222 mmol): 20-1 was dissolved in 400 mL of methanol/water (v/v=1/1) mixed solvent and cooled to 0 °C. Subsequently, sodium hydroxide (35.6 g, 888 mmol) was added to the solution and stirred for 0.5 hours. Sodium hypochlorite solution (380 g, 556 mmol) was added slowly and dropwise at 0°C. The reaction mixture was gradually warmed up to room temperature (20°C) and stirring was continued for 18 hours. After that, the mixture was further warmed up to 35°C and stirred for 1 hour, then warmed up to 75°C and stirred for 0.5 hours. After completion of the reaction, the mixture was cooled to room temperature. The pH was adjusted to 6.0 with hydrochloric acid, at which time a brown precipitate was produced. The precipitate was collected by filtration and washed twice with 200 mL of water to give the final 20-2 (29 g, 86% yield) as a tan powder.

References

[1] Patent: US9138427, 2015, B2. Location in patent: Page/Page column 297

3-Methyl-4-nitroaniline Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Methyl-4-nitroaniline Suppliers

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View Lastest Price from 3-Methyl-4-nitroaniline manufacturers

Honest Joy Holdings Limited
Product
3-Methyl-4-nitroaniline 611-05-2
Price
US $0.00/KG
Min. Order
1KG
Purity
99.0%
Supply Ability
100 tons
Release date
2022-02-21
Career Henan Chemical Co
Product
3-Methyl-4-nitroaniline 611-05-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100kg
Release date
2019-07-12

611-05-2, 3-Methyl-4-nitroanilineRelated Search:

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