3-(4-BROMO-PHENYL)-PROPIONALDEHYDE

Product Name: 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
CAS No.: 80793-25-5
Chemical Name: 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
Synonyms: 4-Bromophenylpropanal;4-(4-broMophenyl)butanal;Benzenepropanal, 4-broMo-;3-(4-BROMO-PHENYL)-PROPIOLDEHYDE;3-(4-BROMO-PHENYL)-PROPIONALDEHYDE
CBNumber: CB2779182
Molecular Formula: C9H9BrO
Formula Weight: 213.07
MOL File: 80793-25-5.mol

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3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Property

Boiling point:: 267.8±15.0 °C(Predicted)
Density: 1.399±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
Appearance: Colorless to light yellow Liquid

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Safety

HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H227Combustible liquid

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth

Product number: FB151387
Product name: 3-(4-Bromo-phenyl)-propionaldehyde
Packaging: 25mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151387
Product name: 3-(4-Bromo-phenyl)-propionaldehyde
Packaging: 50mg
Price: $100
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151387
Product name: 3-(4-Bromo-phenyl)-propionaldehyde
Packaging: 100mg
Price: $150
Updated: 2021/12/16

AK Scientific

Product number: 2565AC
Product name: 3-(4-Bromophenyl)propionaldehyde
Packaging: 1g
Price: $177
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB151387
Product name: 3-(4-Bromo-phenyl)-propionaldehyde
Packaging: 250mg
Price: $250
Updated: 2021/12/16

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3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Chemical Properties,Usage,Production

Synthesis

25574-11-2

80793-25-5

GENERAL STEPS: Example A.4: Synthesis of 3-(4-bromophenyl)propanal (10×) 4-Bromophenylpropanol (4.71 g, 21.8 mmol) was dissolved in dichloromethane (DCM), Dess-Martin periodinane (9.71 g, 20.9 mmol) was added, and the reaction was carried out for 2 hours at room temperature. Upon completion of the reaction, the reaction was quenched with 2 M NaOH solution and the organic and aqueous phases were separated and the aqueous phase was extracted with DCM. The organic phases were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated under reduced pressure. The crude product was purified by rapid chromatography on silica gel, the eluent being a gradient solution of DCM in cyclohexane (cHex) to afford the target product 3-(4-bromophenyl)propionaldehyde (10×) (4.46 g, 96% yield) as a colorless liquid. 1H NMR (400 MHz, CDCl3) δ 9.81 (s, 1H), 7.41 (d, J = 8.4 Hz, 2H), 7.07 (d, J = 8.4 Hz, 2H), 2.91 (t, J = 7.6 Hz, 2H), 2.79-2.74 (m, 2H). MS (ES) C9H9BrO calculated value: 211/213, ([M-H]-) not detected, 100% purity.

References

[1] Patent: WO2015/181272, 2015, A1. Location in patent: Page/Page column 30
[2] Patent: EP3239143, 2017, A2. Location in patent: Paragraph 0120
[3] Patent: WO2015/66413, 2015, A1. Location in patent: Page/Page column 176; 177
[4] Patent: US2017/253554, 2017, A1. Location in patent: Paragraph 0425; 0426
[5] Chemical Communications, 2011, vol. 47, # 27, p. 7875 - 7877

3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-(4-BROMO-PHENYL)-PROPIONALDEHYDE Suppliers

China 54 Germany 2 India 1 Ukraine 1 United Kingdom 1 United States 5 Global 64

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View Lastest Price from 3-(4-BROMO-PHENYL)-PROPIONALDEHYDE manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: 3-(4-Bromophenyl)propanal 80793-25-5
Price: US $0.00-0.00/KG
Min. Order: 10mg
Purity: 99%HPLC
Supply Ability: 2000tons
Release date: 2020-01-15

80793-25-5, 3-(4-BROMO-PHENYL)-PROPIONALDEHYDERelated Search:

(S)-N-Fmoc-3-Bromophenylalanine (S)-N-BOC-4-Bromophenylalanine 3-(4-BROMO-PHENYL)-3-OXO-PROPIONIC ACID ETHYL ESTER 4-BROMO-DL-PHENYLALANINE (R)-N-Fmoc-4-Bromophenylalanine 4-Bromo-1,8-naphthalic anhydride AC-P-BROMO-DL-PHE-OH (RS)-beta-Amino-beta-(4-bromophenyl)propionic acid 2-(4-BROMO-BENZYL)-MALONIC ACID DIETHYL ESTER N-ACETYL-2-(4-BROMOPHENYL)-DL-BETA-ALANINE 3-[(AMINOCARBONYL)AMINO]-3-(4-BROMOPHENYL)PROPANOIC ACID 2-(4-BROMOBENZYLIDENE)-1-BENZOSUBERONE EPOXIDE METHYL 2-AMINO-4-(4-BROMOPHENYL)-7,7-DIMETHYL-5-OXO-4,6,7,8-TETRAHYDRO2H-CHROMENE-3-CARBOXYLATE 2-(4-BENZYLIDENE)-1-INDANONEEPOXIDE 2-(4-BROMOBENZYLIDENE)-1-TETRALONE EPOXIDE [2-(BENZYLOXY)PHENYL][3-(4-BROMOPHENYL)OXIRAN-2-YL]METHANONE 1-[2-(BENZYLOXY)PHENYL]-2,3-DIBROMO-3-(4-BROMOPHENYL)PROPAN-1-ONE ethyl 3-amino-3-(4-bromophenyl)propanoate

3-(4-BROMO-PHENYL)-PROPIONALDEHYDE

3-(4-BROMO-PHENYL)-PROPIOLDEHYDE

4-(4-broMophenyl)butanal

Benzenepropanal, 4-broMo-

4-Bromophenylpropanal

80793-25-5