9-Anthracenylmethyl methacrylate
- Product Name
- 9-Anthracenylmethyl methacrylate
- CAS No.
- 31645-35-9
- Chemical Name
- 9-Anthracenylmethyl methacrylate
- Synonyms
- Anthracen-9-ylmethyl methacrylate;ANMA;AMMA;DK738;POLYFLUOR(R) 407;(9-ANTHRYL) METHACRYLATE;9-Anthrylmethyl Methacrylate;9-ANTHRACENYLMETHYL METHACRYLATE;9-ANTHRACENE METHYL METHACRYLATE;9-Anthrylmethyl Methacrylate >
- CBNumber
- CB3192708
- Molecular Formula
- C19H16O2
- Formula Weight
- 276.33
- MOL File
- 31645-35-9.mol
9-Anthracenylmethyl methacrylate Property
- Melting point:
- 80-85 °C (lit.)
- Boiling point:
- 443.0±14.0 °C(Predicted)
- Density
- 1.159±0.06 g/cm3(Predicted)
- storage temp.
- Keep Cold
- solubility
- Acetone, Chloroform, Dichloromethane, hot Ethanol, Ethyl Acetate,
- form
- Solid
- color
- Pale Yellow
- InChIKey
- MJYSISMEPNOHEG-UHFFFAOYSA-N
- CAS DataBase Reference
- 31645-35-9(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,F
- Risk Statements
- 41
- Safety Statements
- 25-26-36/39
- WGK Germany
- 3
- HS Code
- 29161290
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H318Causes serious eye damage
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 579017
- Product name
- Poly(9-anthracenylmethyl methacrylate)
- Packaging
- 100mg
- Price
- $252
- Updated
- 2023/06/20
- Product number
- 578207
- Product name
- 9-Anthracenylmethyl methacrylate
- Purity
- 95%
- Packaging
- 100mg
- Price
- $326
- Updated
- 2023/06/20
- Product number
- A2645
- Product name
- 9-Anthrylmethyl Methacrylate
- Purity
- >98.0%(HPLC)
- Packaging
- 1g
- Price
- $286
- Updated
- 2024/03/01
- Product number
- 002786
- Product name
- 9-Anthryl Methacrylate
- Packaging
- 1g
- Price
- $403
- Updated
- 2021/12/16
- Product number
- A685000
- Product name
- 9-Anthrylmethyl Methacrylate
- Packaging
- 2.5g
- Price
- $1320
- Updated
- 2021/12/16
9-Anthracenylmethyl methacrylate Chemical Properties,Usage,Production
Description
9-Anthrylmethyl Methacrylate is a fluorescent copolymer used as an optic fiber sensor for determination of Tetracycline.
Chemical Properties
Pale Yellow Crystals
Uses
A fluorescent copolymer as optic fiber sensor for determination of Tetracycline.
Synthesis
9-Anthracenylmethyl methacrylate (9-AMM)is generally synthesized by reacting 9-Anthracene-methanol with methylene chloride and methacryloyl chloride in the presence of a base triethylamine.
Experimental procedrure: 9-Anthracene-methanol 9.3g (45mmol), methylene chloride 60ml and methacryloyl chloride 8g (77mmol) were charged into a 300ml three-necked flask equipped with a stirrer and thermometer. Methylene chloride 10ml solution of triethylamine 6.0g (59mmol) was added dropwise while cooling the slurry with ice water. After completion of the dropwise addition, the slurry became a homogeneous solution. Then allowed to stand overnight while cooling in ice water. The hydrochloride salt of triethylamine floating on the liquid surface and water 30ml were sufficiently added. Further stirred to dissolve. Again washed with water 30ml, the obtained methylene chloride solution was dried over anhydrous sodium sulfate. Further methanol was added to the filtered methylene chloride solution 100ml, stored in the refrigerator and recrystallized. After 2 days, the precipitated crystals were suction filtered and dried. Pale yellow microcrystals 7.1g were obtained. Analysis results of the obtained substance are as shown below, this compound was confirmed to be 9-Anthracenylmethyl methacrylate by 1H-NMR, IR. Yield 58mol%. Melting point: 59-60 ° CIR (KBr, cm-1): 1715, 1624, 1450, 1320, 1296, 1164, 1150, 1060, 1008, 964, 946, 892, 740, 700, 640, 600, 568, 500. 1H-NMR (CDCl3, ppm): δ1.92 (s, 3H, methyl), 5.50 (s, 1H, vinyl), 6.05 (s, 1H, vinyl), 6.22 (s, 2H, methylene group), 7.44-7.60 (m, 4H, anthracene ring), 8.03 (d, J = 10Hz, 2H, anthracene ring), 8, 38 (d, J = 10Hz, 2H, anthracene ring), 8.51 (s, 1H, anthracene ring).
9-Anthracenylmethyl methacrylate Preparation Products And Raw materials
Raw materials
Preparation Products
9-Anthracenylmethyl methacrylate Suppliers
View Lastest Price from 9-Anthracenylmethyl methacrylate manufacturers
- Product
- 9-Anthracenylmethyl methacrylate 31645-35-9
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%+
- Supply Ability
- 10000kgs per Month
- Release date
- 2022-10-11
- Product
- 9-Anthracenylmethyl methacrylate 31645-35-9
- Price
- US $0.00/L
- Min. Order
- 1L
- Purity
- 98%
- Supply Ability
- According to customer requirements
- Release date
- 2022-12-16
- Product
- 9-Anthracenylmethyl methacrylate 31645-35-9
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2018-08-09