ChemicalBook > CAS DataBase List > 2-Iodoxybenzoic acid

2-Iodoxybenzoic acid

Product Name: 2-Iodoxybenzoic acid
CAS No.: 61717-82-6
Chemical Name: 2-Iodoxybenzoic acid
Synonyms: IBX;1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;1-HYDROXY-1,2-BENZIODOXOL-3(1H)-ONE 1-OXIDE;BX;1-hydroxy-1-oxo-3H-1$l^{5},2-benziodaoxol-3-one;39.0%(T);TRILON®TRILON®BX;Iodoxybenzoic aci;2-IodoxybenzoicAci
CBNumber: CB3194863
Molecular Formula: C7H5IO4
Formula Weight: 280.02
MOL File: 61717-82-6.mol

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2-Iodoxybenzoic acid Property

Melting point:: 280 °C
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
solubility: DMSO (Very Slightly, Heated)
form: powder to crystal
color: White to Almost white
Merck: 14,5048
InChI: InChI=1S/C7H5IO4/c9-7(10)5-3-1-2-4-6(5)8(11)12/h1-4H,(H,9,10)
InChIKey: CQMJEZQEVXQEJB-UHFFFAOYSA-N
SMILES: C1(C(=O)O)C=CC=CC=1I(=O)=O
CAS DataBase Reference: 61717-82-6(CAS DataBase Reference)

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Safety

Hazard Codes: C,Xi,Xn
Risk Statements: 22-34-44-42/43-36/37/38-20/21/22-37-35-1
Safety Statements: 26-36/37/39-45-22-35
RIDADR: UN 1759 8/PG 2
WGK Germany: 3
HazardClass: 8
PackingGroup: Ⅱ
HS Code: 29163990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H314Causes severe skin burns and eye damage

H335May cause respiratory irritation

H372Causes damage to organs through prolonged or repeated exposure

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P314Get medical advice/attention if you feel unwell.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 661384
Product name: 2-Iodoxybenzoic acid
Purity: contains stabilizer, 45wt. % (IBX)
Packaging: 1g
Price: $55.76
Updated: 2025/07/31

Sigma-Aldrich

Product number: 661384
Product name: 2-Iodoxybenzoic acid
Purity: contains stabilizer, 45wt. % (IBX)
Packaging: 10g
Price: $193
Updated: 2025/07/31

TCI Chemical

Product number: I0791
Product name: 2-Iodoxybenzoic Acid (stabilized with Benzoic Acid + Isophthalic Acid)
Purity: >39.0%(T)
Packaging: 5g
Price: $73
Updated: 2025/07/31

TCI Chemical

Product number: I0791
Product name: 2-Iodoxybenzoic Acid (stabilized with Benzoic Acid + Isophthalic Acid)
Purity: >39.0%(T)
Packaging: 25g
Price: $227
Updated: 2025/07/31

Sigma-Aldrich

Product number: 661384
Product name: 2-Iodoxybenzoic acid
Purity: contains stabilizer, 45wt. % (IBX)
Packaging: 50g
Price: $758
Updated: 2025/07/31

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2-Iodoxybenzoic acid Chemical Properties,Usage,Production

Chemical Properties

White to off-white powder, prills or agglomerates

Uses

Stabilized 2-Iodoxybenzoic Acid (SIBX)

Uses

2-Iodoxybenzoic Acid is used in the oxidation of alcohols in organic synthesis. It is also frequently used in the preparation of Dess-Martin periodinane.

Definition

ChEBI: A benziodoxole compound having hydroxy and oxo substituents at the 1-position and an oxo substituent at the 3-position.

Synthesis Reference(s)

The Journal of Organic Chemistry, 48, p. 4155, 1983 DOI: 10.1021/jo00170a070

reaction suitability

reagent type: oxidant

Synthesis

88-67-5

61717-82-6

General procedure for the synthesis of 2-iodobenzoic acid from 2-iodobenzoic acid: note: IBX may explode when subjected to shock or heated to over 200 °C. IBX was prepared with reference to the method described by Sputore and coworkers.In a 500 mL round bottom flask equipped with a mechanical stirrer, 2-iodobenzoic acid (12.5 g, 50.4 mmol) was added to a solution of Oxone (40.281 g, 65.5 mmol) in deionized water (163 mL). The reaction mixture was heated to 73 °C and stirred vigorously at this temperature for 3 hours. Subsequently, the reaction mixture was cooled to 0 °C and continued to stir slowly for 1.5 hours. The mixture was filtered through a porous glass funnel and the resulting white solid was washed sequentially with deionized water (730 mL) and acetone (235 mL). Finally, the product was dried under high vacuum for 2 days to afford 2-iodoylbenzoic acid as a white solid in 84% yield (11.848 g, 42.3 mmol).

References

[1] European Journal of Organic Chemistry, 2012, # 7, p. 1439 - 1447
[2] Journal of Organic Chemistry, 1983, vol. 48, # 22, p. 4155 - 4156
[3] Journal of the American Chemical Society, 1991, vol. 113, # 19, p. 7277 - 7287
[4] Journal of Organic Chemistry, 2005, vol. 70, # 17, p. 6991 - 6994
[5] Tetrahedron, 2002, vol. 58, # 23, p. 4573 - 4587

2-Iodoxybenzoic acid Preparation Products And Raw materials

Raw materials

2-Iodobenzoic acid Isophthalic acid Potassium bromate Benzoic acid Sulfuric acid

Preparation Products

Dess-Martin periodinane (5-BROMOTHIOPHEN-3-YL)METHANESULFONYL CHLORIDE

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View Lastest Price from 2-Iodoxybenzoic acid manufacturers

Watson Biotechnology Co.,Ltd

Product: 2-Iodoxybenzoic acid 61717-82-6
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 20MT
Release date: 2024-08-16

Shaanxi Haibo Biotechnology Co., Ltd

Product: 2-Iodoxybenzoic acid 61717-82-6
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 2000ton
Release date: 2023-09-06

Zhuozhou Wenxi import and Export Co., Ltd

Product: 2-Iodoxybenzoic Acid 61717-82-6
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

61717-82-6, 2-Iodoxybenzoic acidRelated Search:

2-Iodobenzoic acid Citric acid Ethyl 2-(Chlorosulfonyl)acetate Sodium lauroylglutamate Sodium lauroylsarcosinate Folic acid Ascoric Acid 2-Iodosobenzoic acid 2-IODOBENZALDEHYDE 2-Iodobenzyl alcohol O-IODOXYBENZOIC ACID, 97% 2-Iodotoluene Iodosobenzene 1-HYDROXY-1,3-DIOXO-1,3-DIHYDRO-1L5-BENZO[D][1,2]IODOXOLE-4-CARBOXYLIC ACID Iodoxybenzene 2-Iodoxybenzoic acid 2-IODOXYBENZOIC ACID STABILIZED MIXTURE (DESS MART STABILIZED 2-IODOXYBENZOIC ACID (SIBIX) MIXTURE

1-hydroxy-1-oxo-3H-1$l^{5},2-benziodaoxol-3-one

2-Iodoxybenzoic Acid Stabilized (SIBX)

2-Iodoxybenzoic Acid (stabilized with Benzoic Acid + Isophthalic Acid)

1-Hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide 97%, 45 wt. % IBX

SIBX, 1,3-Dihydro-1,3-dioxo-1-hydroxy-1,2-benziodoxole stabilised

Iodoxybenzoic aci

2-Iodoxybenzoic acid contains stabilizer, 45 wt. % (IBX)

TRILON&reg

TRILON&REG;BX

2-IODOXYBENZOIC ACID (IBX) 1M SOLUTION IN DMSO

1-Hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide (mixture of isomers)

1,2-BENZIODOXOL-3(1H)-ONE, 1-HYDROXY, 1-OXIDE

1-HYDROXY-1,2-BENZIODOXOL-3(1H)-ONE 1-OXIDE

1-HYDROXY-1,2-BENZIODOXOL-3(H)-ONE 1-OXIDE

2-IODOXYBENZOIC ACID, STABILIZED (45 WT&

IbxO-IodoxybenzoicAcid

2-Iodoxybenzoic acid, stabilized

2-Iodoxybenzoic acid

IBX(1-HYDROXY-1,2-BENZIODOXOL-3(1H)-ONE-1-OXIDE)

SIBX, Stabilized IBX

2-Iodoxybenzoic acid ,39-50% [Stabilizer：Benzoic acid 23%，Isophtalic acid 30%]

1-Hydroxy-1,3-dioxo-3H-benz[d][1,2]iodoxol

1-Hydroxy-3H-benz[d][1,2]iodoxol-1,3-dione

2-Iodoxybenzoic acidDess Martin analogueSIBX

1-Hydroxy-1,2-benziodoxy-3-(1h)-one-1-xoide

2-Iodoxybenzoic Acid Stabilized (SIBX), 46 wt% IBX

1-Hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide 97%

IBX, 1,3-Dihydro-1,3-dioxo-1-hydroxy-1,2-benziodoxole

1-hydroxy-1,3-dioxobenziodoxole

IBX

1-hydroxy-1-oxo-1$l^{5},2-benziodoxol-3-one

2-Iodoxybenzoic acid (mixture of isomers)

2-Iodoxybenzoic acid, stabilized (45 wt.% IBX)

2-Iodoxybenzoic acid(IBX)

2-IodoxybenzoicAcid(stabilizedwithBenzoicAcid+IsophthalicAcid)&gt

39.0%(T)

2-Iodoxybenzoic Acid,>95%

2-Iodoxybenzoic acid (Stabilised)

2-IodoxybenzoicAci

2-Iodoxybenzoic acid, contains stabilizer, 0.45wt (IBX)

1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione

2-Iodoxybenzoic acid contains stabilizer

1-hydroxy-1-oxo-3H-1λ?,2-benziodaoxol-3-one

Stabilised IBX [Stabilised iodoxy benzoic acid}

1-hydroxy-1-oxo-3H-1lambda5,2-benziodaoxol-3-one

IBX,contains stabilizer, 45-47wt%

2-Iodoacylbenzoic acid

1-Hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide, 45 wt. % IBX

61717-82-6

C7H5IO4

Hypervalent Iodine

Oxidation

Synthetic Reagents

Fused Ring Systems

pharmacetical

API intermediates

Iodylbenzoic acid