Methyl 3-amino-4-chlorobenzoate

Product Name: Methyl 3-amino-4-chlorobenzoate
CAS No.: 40872-87-5
Chemical Name: Methyl 3-amino-4-chlorobenzoate
Synonyms: Intedanib Impurity 5;Methyl 3-Amino-4-chlorobenzene;METHYL 3-AMINO-4-CHLOROBENZOATE;METHYL, 4-CHLORO-3-AMINOBENZOATE;Methyl3-Amino-4-chlorobenzoate>3-amino-4-chloro-2-methylbenzoate;Amino chlorobenzoic acid methyl ester;3-AMINO-4-CHLOROBENZOIC ACID METHYL ESTER;Methyl 3-AMino-4-chlorobenzoate, 98.0%(GC&T;Benzoic acid, 3-aMino-4-chloro-, Methyl ester
CBNumber: CB3211933
Molecular Formula: C8H8ClNO2
Formula Weight: 185.61
MOL File: 40872-87-5.mol

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Methyl 3-amino-4-chlorobenzoate Property

Melting point:: 83 °C
Boiling point:: 292.1±20.0 °C(Predicted)
Density: 1.311±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
form: crystalline powder
pka: 1.51±0.10(Predicted)
color: Pale lemon/gold
CAS DataBase Reference: 40872-87-5(CAS DataBase Reference)

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Safety

Hazard Codes: Xi
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: M1778
Product name: Methyl 3-Amino-4-chlorobenzoate
Purity: >98.0%(GC)(T)
Packaging: 5g
Price: $54
Updated: 2024/03/01

TCI Chemical

Product number: M1778
Product name: Methyl 3-Amino-4-chlorobenzoate
Purity: >98.0%(GC)(T)
Packaging: 25g
Price: $181
Updated: 2024/03/01

TRC

Product number: M328668
Product name: Methyl 3-Amino-4-chlorobenzoate
Packaging: 500mg
Price: $65
Updated: 2021/12/16

Apolloscientific

Product number: OR2041
Product name: Methyl 3-Amino-4-chlorobenzoate
Packaging: 25g
Price: $58
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4658-5-X6
Product name: Methyl 3-amino-4-chlorobenzoate
Packaging: 25g
Price: $64
Updated: 2021/12/16

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Methyl 3-amino-4-chlorobenzoate Chemical Properties,Usage,Production

Synthesis

To a solution of 3-amino-4-chlorobenzoic acid (15.0 g, 88.0 mmol) in methanol (90.0 mL), thionyl chloride (13.0 mL) was added drop-wise at 0 °C. The resulting mixture was refluxed for 12h. After completion of the reaction, the reaction mixture was concentrated under reduced pressure. The residue was diluted with water (150 mL) and extracted with ethyl acetate. The organic layer was washed with sodium bicarbonate (50 mL) and brine solution (50 mL) and dried over sodium sulfate. The organic layer was removed under a rotary evaporator to yield Methyl 3-amino-4-chlorobenzoate (15.0 g, 92.5 per cent) as an off-white solid. 1H NMR (400 MHz, CDC13) δ 3.88 (s, 3H), 4.26 (brs, 2H), 7.29 (d, J = 8.2 Hz, 1H), 7.34-7.37 (dd, J = 1.9, 8.2 Hz, 1H), 7.45 (d, J = 1.9 Hz, 1H).

Methyl 3-amino-4-chlorobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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Methyl 3-amino-4-chlorobenzoate Suppliers

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View Lastest Price from Methyl 3-amino-4-chlorobenzoate manufacturers

Career Henan Chemical Co

Product: methyl 3-amino-4-chlorobenzoate 40872-87-5
Price: US $7.00/kg
Min. Order: 1kg
Purity: 99%
Supply Ability: 100kg
Release date: 2018-12-25

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3-AMINO-4-CHLOROBENZOIC ACID METHYL ESTER

METHYL 3-AMINO-4-CHLOROBENZOATE

METHYL, 4-CHLORO-3-AMINOBENZOATE

Amino chlorobenzoic acid methyl ester

Methyl 3-Amino-4-chlorobenzene

Benzoic acid, 3-aMino-4-chloro-, Methyl ester

Methyl 3-AMino-4-chlorobenzoate, 98.0%(GC&T

Intedanib Impurity 5

3-amino-4-chloro-2-methylbenzoate

Methyl3-Amino-4-chlorobenzoate&gt

Benzoic acid, 3-amino-4-chloro-, methyl ester (9CI, ACI)

3-amino-4-chloro-Benzoic acid methyl ester (9CI ACI)

40872-87-5

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