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5-METHOXY-2-NITROBENZONITRILE

Product Name
5-METHOXY-2-NITROBENZONITRILE
CAS No.
38469-84-0
Chemical Name
5-METHOXY-2-NITROBENZONITRILE
Synonyms
3-Cyano-4-nitroanisole;5-METHOXY-2-NITROBENZONITRILE;Benzonitrile, 5-methoxy-2-nitro-;3-Cyano-4-nitroanisole, 2-Cyano-4-methoxynitrobenzene
CBNumber
CB32449204
Molecular Formula
C8H6N2O3
Formula Weight
178.14
MOL File
38469-84-0.mol
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5-METHOXY-2-NITROBENZONITRILE Property

Melting point:
96 °C
Boiling point:
352.2±32.0 °C(Predicted)
Density 
1.32±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
Appearance
Light brown to yellow Solid
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Safety

HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
M326988
Product name
5-Methoxy-2-nitrobenzonitrile
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
M326988
Product name
5-Methoxy-2-nitrobenzonitrile
Packaging
500mg
Price
$65
Updated
2021/12/16
AK Scientific
Product number
W5921
Product name
5-Methoxy-2-nitrobenzonitrile
Packaging
1g
Price
$84
Updated
2021/12/16
Matrix Scientific
Product number
073350
Product name
5-Methoxy-2-nitrobenzonitrile
Purity
95+%
Packaging
1g
Price
$231
Updated
2021/12/16
Matrix Scientific
Product number
073350
Product name
5-Methoxy-2-nitrobenzonitrile
Purity
95+%
Packaging
5g
Price
$639
Updated
2021/12/16
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5-METHOXY-2-NITROBENZONITRILE Chemical Properties,Usage,Production

Synthesis

41994-92-7

38469-84-0

Step 2: Synthesis of 5-methoxy-2-nitrobenzonitrile To a 100 mL round bottom flask was added 5-methoxy-2-nitrobenzamide (2.1 g, 0.01 mol), trifluoroacetic anhydride (2.2 mL), triethylamine (2.9 mL) and dichloromethane (30 mL). The reaction mixture was stirred at room temperature for 1 hour. After completion of the reaction, the reaction mixture was washed with distilled water (30 mL × 2). The organic layer was separated and dried over anhydrous sodium sulfate and subsequently concentrated under reduced pressure to give 1.75 g (92% yield) of white solid product. Mass spectrometry (MS) showed m/z: 179 ([M + H]+).

References

[1] Patent: US2010/120741, 2010, A1. Location in patent: Page/Page column 59

5-METHOXY-2-NITROBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-METHOXY-2-NITROBENZONITRILE Suppliers

Alchem Pharmtech,Inc.
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View Lastest Price from 5-METHOXY-2-NITROBENZONITRILE manufacturers

Career Henan Chemical Co
Product
5-METHOXY-2-NITROBENZONITRILE 38469-84-0
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
1000KGS
Release date
2019-12-24